POWDERS AND GRANULES AND PROCESS FOR MAKING SUCH POWDERS AND GRANULES

    公开(公告)号:US20230062299A1

    公开(公告)日:2023-03-02

    申请号:US17786303

    申请日:2020-12-04

    申请人: BASF SE

    摘要: The present invention is directed towards a process for making a powder or granule containing (A) at least one alkali metal salt of citric acid, and at least one additive selected from (B) at least one (co)polymer containing carboxylic acid groups, partially neutralized with alkali, in a weight ratio of (A):(B) of from 5:1 up to 100:1, wherein said powder or granule contains at least 75% by weight of citrate (A), said process comprising the steps of (a) mixing the at least one alkali metal salt of citric acid (A) and the at least one (co)polymer (B) in the presence of water, (b) removing most of said water by spray-drying or spray granulation using a gas with an inlet temperature of at least 125° C.

    Detergent additive
    2.
    发明授权

    公开(公告)号:US11421190B2

    公开(公告)日:2022-08-23

    申请号:US16630870

    申请日:2018-07-10

    发明人: Liang Chen Xue Chen

    摘要: A detergent additive comprising an active, the active comprising one or both of tetraacetylethylenediamine and triacetylethylenediamine; and polyvinyl butyral. A method of preparing a detergent additive comprising providing a solvent to a reaction mixture; providing polyvinyl butyral to the reaction mixture; providing an active to the reaction mixture, the active comprising one or both of tetraacetylethylenediamine and triacetylethylenediamine; mixing the reaction mixture; and spray-drying the reaction mixture.

    Process for manufacturing granules

    公开(公告)号:US10975334B2

    公开(公告)日:2021-04-13

    申请号:US16060148

    申请日:2016-12-01

    申请人: BASF SE

    摘要: Process for manufacturing granules of at least one alkali metal salt of aminopolycarboxylic acid (A), comprising the steps of (a) providing an aqueous slurry of alkali metal salt of aminopolycarboxylic acid (A), (b) maintaining said aqueous slurry at a temperature in the range of from 50 to 90° C. over a period of time in the range of from 2 to 180 hours, (c) spray granulating said slurry with a gas inlet temperature of at least 150° C.