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    Preparation of bis(2-morpholinoethyl) ether
    5.
    发明授权
    Preparation of bis(2-morpholinoethyl) ether 有权
    双（2-吗啉代乙基）醚的制备

    公开(公告)号：US6111100A

    公开(公告)日：2000-08-29

    申请号：US474906

    申请日：1999-12-30

    申请人： Hartmut Riechers ,  Joachim Simon ,  Andreas Henne ,  Arthur Hohn

    发明人： Hartmut Riechers ,  Joachim Simon ,  Andreas Henne ,  Arthur Hohn

    IPC分类号： C07D295/08 ,  B01J23/72 ,  C07D295/088 ,  C07D413/12

    CPC分类号： C07D295/088

    摘要： In a process for preparing bis(2-morpholinoethyl) ether by reacting diethylene glycol with ammonia under superatmospheric pressure and at elevated temperature in the presence of hydrogen and a hydrogenation catalyst, the catalytically active composition of the catalyst prior to reduction with hydrogen comprisesfrom 20 to 85% by weight of aluminum oxide (Al.sub.2 O.sub.3), zirconium dioxide (ZrO.sub.2), titanium dioxide (TiO.sub.2) and/or silicon dioxide (SiO.sub.2),from 1 to 70% by weight of oxygen-containing compounds of copper, calculated as CuO,from 0 to 50% by weight of oxygen-containing compounds of magnesium, calculated as MgO, oxygen-containing compounds of chromium, calculated as Cr.sub.2 O.sub.3, oxygen-containing compounds of zinc, calculated as ZnO, oxygen-containing compounds of barium, calculated as BaO, and/or oxygen-containing compounds of calcium, calculated as CaO, andless than 20% by weight of oxygen-containing compounds of nickel, calculated as NiO, based on the oxygen-containing compounds of copper, calculated as CuO.

    摘要翻译： 在氢气和氢化催化剂的存在下，在二氧化乙烯与氨在超大气压和升高的温度下反应制备双（2-吗啉代乙基）醚的方法中，用氢还原之前的催化剂催化活性组合物包括20 至85重量％的氧化铝（Al 2 O 3），二氧化锆（ZrO 2），二氧化钛（TiO 2）和/或二氧化硅（SiO 2），1至70重量％的含氧化合物的铜，以CuO ，0〜50重量％的以氧化镁计的含氧化合物的镁，以Cr 2 O 3计算的含氧化合物的铬，以ZnO计的氧的含氧化合物，钡的含氧化合物，计算值 作为BaO，和/或以CaO计的钙的含氧化合物，以NiO计，基于含氧化合物的铜，小于20重量％的含氧化合物的镍 ，以CuO计算。