Dewatering and purification of crude pyrrolidine
    2.
    发明授权
    Dewatering and purification of crude pyrrolidine 有权
    脱水和纯化粗吡咯烷

    公开(公告)号:US06353118B1

    公开(公告)日:2002-03-05

    申请号:US09716835

    申请日:2000-11-20

    IPC分类号: C07O295023

    CPC分类号: C07D295/023

    摘要: In a process for purifying crude pyrrolidine to give a pyrrolidine composition comprising more than 99% (m/m) of pyrrolidine and less than 0.3% (m/m) of water, crude pyrrolidine comprising from 40 to 98% (m/m) of pyrrolidine and having a water content of more than 2% (m/m) is subjected to continuous distillation at a pressure at the top of less than 950 hPa in a column having a stripping section and a rectifying section.

    摘要翻译: 在纯化粗制吡咯烷的方法中,得到包含大于99%(m / m)的吡咯烷和小于0.3%(m / m)的水的吡咯烷组合物,包含40-98%(m / m) 的吡咯烷并且具有大于2%(m / m)的水含量的混合物在具有汽提段和精馏段的塔中在小于950hPa的顶部的压力下进行连续蒸馏。

    Plant-treatment agents
    3.
    发明授权
    Plant-treatment agents 失效
    植物处理剂

    公开(公告)号:US06191071B1

    公开(公告)日:2001-02-20

    申请号:US09297628

    申请日:1999-05-04

    IPC分类号: A01N2510

    CPC分类号: A01N25/10

    摘要: The invention concerns novel plant-treatment agents comprising: at least one thermoplastically processable biodegradable polyester amide, optionally in a mixture with one or a plurality of further thermoplastically processable, biodegradable polymer components; at least one agrochemical substance; and optionally additives. The invention further concerns a process for preparing these agents, and their use in the application of agrochemical substances.

    摘要翻译: 本发明涉及新颖的植物处理剂,其包括:至少一种热塑性可加工的可生物降解的聚酯酰胺,任选地与一种或多种另外的热塑性可加工的可生物降解的聚合物组分的混合物; 至少一种农用化学物质; 和任选的添加剂。 本发明还涉及制备这些试剂的方法及其在应用农药物质中的应用。

    Preparation of pyrroles
    4.
    发明授权
    Preparation of pyrroles 有权
    吡咯的制备

    公开(公告)号:US6162928A

    公开(公告)日:2000-12-19

    申请号:US553254

    申请日:2000-04-20

    摘要: A process for preparing pyrroles of the formula I: ##STR1## where R.sub.1, R.sup.2, R.sup.3 and R.sup.4 are identical or different and are hydrogen atoms, alkyl groups having from 1 to 12 carbon atoms or cycloalkyl groups having from 3 to 12 carbon atoms, by dehydrogenation of pyrrolidines of the formula II: ##STR2## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are as defined above, in the presence of a supported noble metal catalyst is described. In this process, the dehydrogenation is carried out at from 150 to 300.degree. C. and pressures of from 0.01 to 50 bar and the noble metal catalyst comprises from 30 to 100% by weight of:a) palladium on an oxide of a rare earth or an oxide of an element of the 4.sup.th group (transition group IV) of the Periodic Table, orb) a platinum/palladium mixture on aluminum oxide, an oxide of a rare earth or an oxide of an element of the 4.sup.th groupand from 0 to 70% by weight of alkali metal oxide or alkaline earth metal oxide.

    摘要翻译: 制备式I的吡咯的方法:其中R 1,R 2,R 3和R 4相同或不同,为氢原子,具有1至12个碳原子的烷基或具有3至12个碳原子的环烷基,通过脱氢 描述了在负载的贵金属催化剂的存在下,式II的吡咯烷(其中R 1,R 2,R 3和R 4如上定义)。 在该方法中,脱氢在150-300℃,压力为0.01至50巴,贵金属催化剂包含30-100重量%的:a)在稀土氧化物上的钯 或元素周期表第4族元素(过渡组IV)的氧化物,或b)在氧化铝上的铂/钯混合物,稀土的氧化物或第4族元素的氧化物, 0〜70重量%的碱金属氧化物或碱土金属氧化物。

    Apparatus for developing photographic material
    8.
    发明授权
    Apparatus for developing photographic material 失效
    照相材料显影装置

    公开(公告)号:US5870646A

    公开(公告)日:1999-02-09

    申请号:US926480

    申请日:1997-09-10

    申请人: Joachim Simon

    发明人: Joachim Simon

    IPC分类号: G03D3/13 G03D3/02 G03D3/08

    CPC分类号: G03D3/132

    摘要: An apparatus for developing photographic material having a delivery device and a removal device for developing fluid as well as an inlet and an outlet for the material to be developed with a narrow conduit that extends from the inlet to the outlet. A transport mechanism for transporting the photographic material to be developed from the inlet through the conduit to the outlet wherein the material to be developed comes into contact with the developing fluid as it is transported through the conduit and is developed. Two half shells are connectable to one another, with each half shell having two plates joined to make the half shell. The apparatus also has a central positive displacement element, which together with the inner wall of the half shells, defines the conduit in which the photographic material is developed. The conduit extends between the positive displacement element and the respective inner wall of the half shell. The inner wall of the positive displacement element is embodied substantially as a flat face, while the outer wall reinforces the inner wall in order to prevent deformation of the inner wall by the high pressure of the developing fluid.

    摘要翻译: 一种用于显影照相材料的设备,其具有用于显影流体的输送装置和去除装置,以及用于从入口延伸到出口的窄导管的待显影材料的入口和出口。 一种运送机构,用于将待开发的照相材料从入口通过导管传送至出口,其中待显影的材料在显影液体通过导管输送时与显影液体接触并显影。 两个半壳可以彼此连接,每个半壳有两个连接的板制成半壳。 该设备还具有中心的正位移元件,其与半壳体的内壁一起限定了照相材料在其中显影的导管。 导管在正位移元件和半壳的相应内壁之间延伸。 正位移元件的内壁基本上被实施为平坦表面,而外壁加强了内壁,以防止内壁由于显影液的高压而变形。

    Ethylene urea displaying lasting powder flow
    9.
    发明授权
    Ethylene urea displaying lasting powder flow 有权
    乙烯尿素显示持久的粉末流动

    公开(公告)号:US08303872B2

    公开(公告)日:2012-11-06

    申请号:US12747313

    申请日:2008-12-10

    IPC分类号: B29B9/00 C07D233/34

    CPC分类号: C07D233/34 Y10T428/2982

    摘要: The present invention relates to a process for preparing ethylene urea in solid form, in which a water-comprising product melt of ethylene urea is cooled on a breaking-up apparatus and the water content of the solid obtained is from 5 to 15% by weight. Furthermore, the invention relates to ethylene urea as solid prepared by a process according to the invention, wherein the water content of the solid is from 5 to 15% by weight and the solid displays lasting powder flow.

    摘要翻译: 本发明涉及一种制备固体形式的亚乙基脲的方法,其中将乙烯脲的含水产物熔体在破碎装置上冷却,所得固体的水含量为5至15重量% 。 此外,本发明涉及通过根据本发明的方法制备的固体的乙烯脲,其中固体的水含量为5至15重量%,并且固体显示持续的粉末流动。

    ETHYLENE UREA DISPLAYING LASTING POWDER FLOW
    10.
    发明申请
    ETHYLENE UREA DISPLAYING LASTING POWDER FLOW 有权
    乙烯尿素显示激光粉

    公开(公告)号:US20100261015A1

    公开(公告)日:2010-10-14

    申请号:US12747313

    申请日:2008-12-10

    CPC分类号: C07D233/34 Y10T428/2982

    摘要: The present invention relates to a process for preparing ethylene urea in solid form, in which a water-comprising product melt of ethylene urea is cooled on a breaking-up apparatus and the water content of the solid obtained is from 5 to 15% by weight. Furthermore, the invention relates to ethylene urea as solid prepared by a process according to the invention, wherein the water content of the solid is from 5 to 15% by weight and the solid displays lasting powder flow.

    摘要翻译: 本发明涉及一种制备固体形式的亚乙基脲的方法,其中将乙烯脲的含水产物熔体在破碎装置上冷却,所得固体的水含量为5至15重量% 。 此外,本发明涉及通过根据本发明的方法制备的固体的乙烯脲,其中固体的水含量为5至15重量%,并且固体显示持续的粉末流动。