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    Dental compositions comprising ethylenically unsaturated addition-fragmentation agent
    1.
    发明授权
    Dental compositions comprising ethylenically unsaturated addition-fragmentation agent 有权
    含有烯键式不饱和加成断裂剂的牙科组合物

    公开(公告)号：US09056043B2

    公开(公告)日：2015-06-16

    申请号：US13978557

    申请日：2012-02-08

    申请人： Guy D. Joly ,  Larry R. Krepski ,  Babu N. Gaddam ,  Ahmed S. Abuelyaman ,  Bradley D. Craig ,  Timothy D. Dunbar ,  Chuntao Cao ,  Joel D. Oxman ,  Afshin Falsafi ,  William H. Moser ,  Hoa T. Bui

    发明人： Guy D. Joly ,  Larry R. Krepski ,  Babu N. Gaddam ,  Ahmed S. Abuelyaman ,  Bradley D. Craig ,  Timothy D. Dunbar ,  Chuntao Cao ,  Joel D. Oxman ,  Afshin Falsafi ,  William H. Moser ,  Hoa T. Bui

    IPC分类号： A61K6/083 ,  A61K6/00

    CPC分类号： A61K6/083 ,  A61K6/0023 ,  A61K6/0029 ,  A61K6/005 ,  C08L33/10

    摘要： Dental compositions are described comprising an addition-fragmentation agent comprising at least one ethylenically unsaturated terminal group and a backbone unit comprising an α,β-unsaturated carbonyl; at least one monomer comprising at least two ethylenically unsaturated group; and inorganic oxide filler. The addition-fragmentation agent is preferably free-radically cleavable. The addition-fragmentation agent preferably comprises at least two ethylenically unsaturated terminal groups, such as (meth)acTylate groups. In some embodiments, the addition-fragmentation agent has the formula: wherein R1, R2 and R3 are each independently Zm, -Q-, a (hetero)alkyl group or a (hetero)aryl group with the proviso that at least one of R1, R2 and R3 is Zm-Q-; Q is a linking group have a valence of m+1; Z is an ethylenically unsaturated polymerizable group; m is 1 to 6; each X1 is independently —O— or —NR4—, where R4 is H or C1-C4 alkyl; and n is 0 or 1. Also described are dental articles prepared from a dental composition comprising an addition-fragmentation agent and methods of treating a tooth surface.

    摘要翻译： 描述了牙科组合物，其包含包含至少一个烯属不饱和末端基团的加成断裂剂和包含α，β-不饱和羰基的主链单元; 至少一种包含至少两个烯属不饱和基团的单体; 和无机氧化物填料。 加成裂解剂优选是可自由基切割的。 加成断裂剂优选包含至少两个烯键式不饱和端基，例如（甲基）丙烯酸酯基团。 在一些实施方案中，加成断裂剂具有下式：其中R 1，R 2和R 3各自独立地为Z m，-Q-，（杂）烷基或（杂）芳基，条件是R 1 ，R2和R3是Zm-Q-; Q是连接基团，其价态为m + 1; Z是烯属不饱和可聚合基团; m为1〜6; 每个X 1独立地是-O-或-NR 4 - ，其中R 4是H或C 1 -C 4烷基; 并且n为0或1.还描述了由包含加成碎裂剂的牙科组合物制备的牙科用品和治疗牙齿表面的方法。

    DENTAL COMPOSITIONS COMPRISING ETHYLENICALLY UNSATURATED ADDITION-FRAGMENTATION AGENT
    3.
    发明申请
    DENTAL COMPOSITIONS COMPRISING ETHYLENICALLY UNSATURATED ADDITION-FRAGMENTATION AGENT 有权
    包含乙烯不饱和添加剂分散剂的牙科组合物

    公开(公告)号：US20130316307A1

    公开(公告)日：2013-11-28

    申请号：US13978557

    申请日：2012-02-08

    申请人： Guy D. Joly ,  Larry R. Krepski ,  Babu N. Gaddam ,  Ahmed S. Abuelyaman ,  Bradley D. Craig ,  Timothy D. Dunbar ,  Chuntao Cao ,  Joel D. Oxman ,  Afshin Falsafi ,  William H. Moser ,  Hoa T. Bui

    发明人： Guy D. Joly ,  Larry R. Krepski ,  Babu N. Gaddam ,  Ahmed S. Abuelyaman ,  Bradley D. Craig ,  Timothy D. Dunbar ,  Chuntao Cao ,  Joel D. Oxman ,  Afshin Falsafi ,  William H. Moser ,  Hoa T. Bui

    IPC分类号： A61K6/00

    CPC分类号： A61K6/083 ,  A61K6/0023 ,  A61K6/0029 ,  A61K6/005 ,  C08L33/10

    摘要： Dental compositions are described comprising an addition-fragmentation agent comprising at least one ethylenically unsaturated terminal group and a backbone unit comprising an α,β-unsaturated carbonyl; at least one monomer comprising at least two ethylenically unsaturated group; and inorganic oxide filler. The addition-fragmentation agent is preferably free-radically cleavable. The addition-fragmentation agent preferably comprises at least two ethylenically unsaturated terminal groups, such as (meth)acTylate groups. In some embodiments, the addition-fragmentation agent has the formula: wherein R1, R2 and R3 are each independently Zm, -Q-, a (hetero)alkyl group or a (hetero)aryl group with the proviso that at least one of R1, R2 and R3 is Zm-Q-; Q is a linking group have a valence of m+1; Z is an ethylenically unsaturated polymerizable group; m is 1 to 6; each X1 is independently —O— or —NR4—, where R4 is H or C1-C4 alkyl; and n is 0 or 1. Also described are dental articles prepared from a dental composition comprising an addition-fragmentation agent and methods of treating a tooth surface.

    摘要翻译： 描述了牙科组合物，其包含包含至少一个烯属不饱和末端基团的加成断裂剂和包含α，β-不饱和羰基的主链单元; 至少一种包含至少两个烯属不饱和基团的单体; 和无机氧化物填料。 加成裂解剂优选是可自由基切割的。 加成断裂剂优选包含至少两个烯键式不饱和端基，例如（甲基）丙烯酸酯基团。 在一些实施方案中，加成断裂剂具有下式：其中R 1，R 2和R 3各自独立地为Z m，-Q-，（杂）烷基或（杂）芳基，条件是R 1 ，R2和R3是Zm-Q-; Q是连接基团，其价态为m + 1; Z是烯属不饱和可聚合基团; m为1〜6; 每个X 1独立地是-O-或-NR 4 - ，其中R 4是H或C 1 -C 4烷基; 并且n为0或1.还描述了由包含加成碎裂剂的牙科组合物制备的牙科用品和治疗牙齿表面的方法。

    DENTAL AUTO-MIXING METHOD, DEVICE, AND COMPOSITION FOR TEMPORARY CEMENTS
    4.
    发明申请
    DENTAL AUTO-MIXING METHOD, DEVICE, AND COMPOSITION FOR TEMPORARY CEMENTS 审中-公开
    牙科自动混合方法，装置和组合物用于临时试验

    公开(公告)号：US20120258424A1

    公开(公告)日：2012-10-11

    申请号：US13513879

    申请日：2010-12-16

    申请人： Afshin Falsafi ,  Joel D. Oxman ,  Hoa T. Bui ,  Anupa N. Patel

    发明人： Afshin Falsafi ,  Joel D. Oxman ,  Hoa T. Bui ,  Anupa N. Patel

    IPC分类号： A61K6/083 ,  A61C13/263 ,  A61C5/06 ,  A61C13/23

    CPC分类号： A61K6/083 ,  A61C5/62 ,  A61C5/64 ,  A61K6/0017 ,  A61K6/0023 ,  A61K6/0835 ,  C08L33/00

    摘要： The abstract has been amended as follows: A method of dispensing a hardenable dental composition, which can form a temporary bond, comprising 1) providing multi-part hardenable dental composition comprising part (A) in the form of a paste comprising acid-reactive glass particles and a liquid selected from the group consisting of water, a monomer having at least one ethylenically 10 unsaturated group per monomer molecule, and a combination thereof; and part (B) comprising a water soluble polyacid and a liquid selected from the group consisting of water, a monomer having at least one ethylenically unsaturated group per monomer molecule, and a combination thereof; and 2) extruding the composition through a static mixer in fluid communication with a first reservoir containing the part (A) and a second reservoir 20 containing the part (B); wherein a plunger is positioned in each reservoir for simultaneously forcing part (A) and part (B) into the static mixer.

    摘要翻译： 摘要已经被修改如下：一种分配可以形成临时结合的可硬化牙科组合物的方法，包括：1）提供多部分可硬化牙科用组合物，其包含含有酸反应性玻璃的浆料形式的部分（A） 颗粒和选自水，每单体分子具有至少一个烯键式10不饱和基团的单体及其组合的液体; 和部分（B），其包含水溶性多酸和选自水，每单体分子具有至少一个烯属不饱和基团的单体及其组合的液体; 和2）通过与包含所述部分（A）的第一储存器和包含所述部分（B）的第二储存器20流体连通的静态混合器挤出所述组合物; 其中柱塞位于每个储存器中，用于同时迫使部分（A）和部分（B）进入静态混合器。

    Dental fillers, pastes, and compositions prepared therefrom
    6.
    发明授权
    Dental fillers, pastes, and compositions prepared therefrom 有权
    牙科填料，糊剂和由其制备的组合物

    公开(公告)号：US07091259B2

    公开(公告)日：2006-08-15

    申请号：US10190321

    申请日：2002-07-03

    申请人： Hoa T. Bui ,  Brant U. Kolb ,  Sumita B. Mitra

    发明人： Hoa T. Bui ,  Brant U. Kolb ,  Sumita B. Mitra

    IPC分类号： A61K6/083 ,  C08K9/06 ,  A61C5/00

    CPC分类号： A61K6/083 ,  A61K6/0017 ,  A61K6/0023 ,  A61K6/0091 ,  A61K6/087 ,  Y10T428/2995 ,  C08L33/04 ,  C08L63/00

    摘要： The present invention provides a dental paste, methods of making and using the dental paste, and compositions prepared therefrom. The dental paste includes (a) a filler including porous, non-pyrogenic silica having a silane treated surface and being substantially free of heavy metals and (b) a filler including non-agregated primary silica particles, with the fillers being dispersed in a hardenable resin. Fillers including porous, non-pyrogenic silica, and methods of making and using the fillers, are also provided.

    摘要翻译： 本发明提供牙膏，制造和使用牙膏的方法以及由其制备的组合物。 牙膏包括可硬化树脂和设置在树脂中的酸反应性填料。 酸反应性填料包括硅烷处理的表面，其中硅烷包括含聚氧化烯烃基的硅烷。

    Broadband protective optical window coating
    7.
    发明授权
    Broadband protective optical window coating 失效
    宽带保护光学窗口涂层

    公开(公告)号：US5993981A

    公开(公告)日：1999-11-30

    申请号：US844715

    申请日：1997-04-18

    申请人： Joel Askinazi ,  Authi A. Narayanan ,  Hoa T. Bui ,  Joseph A. Vigil ,  John J. Vajo

    发明人： Joel Askinazi ,  Authi A. Narayanan ,  Hoa T. Bui ,  Joseph A. Vigil ,  John J. Vajo

    IPC分类号： G02B1/11 ,  B32B9/00 ,  G02B1/10

    CPC分类号： G02B1/115

    摘要： The present invention provides a broadband transmitting protective coating (10) including an AlGaP protective layer (14) deposited on an optical substrate (12) and an anti-reflection film (16) deposited on the AlGaP protective layer (14). The coating (10) is suitable for use with typical infrared and broadband optical substrate materials such as germanium or multi-spectral ZnS. In the case of a germanium substrate (12), the anti-reflection film (16), (16a) preferably consists of a single layer of hard carbon or alternating layers of hard carbon and silicon. In the case of a multi-spectral ZnS substrate (12a), the anti-reflection film (16b) preferably consists of layered Al.sub.2 O.sub.3 /TaO.sub.5 /LaF.sub.3 /MgF.sub.2. The protective coating (10) is preferably deposited on the optical substrate (12) by a metal organic chemical vapor deposition process wherein an initial layer of AlP is nucleated on the substrate (12) at a temperature of approximately 400.degree. C. The temperature of the substrate (12) is then raised to approximately 600.degree. C. and a layer of AlGaP (14) is grown on the substrate (12) to a preselected thickness. The AlGaP coated optical substrate (12) is then polished to a desired smoothness. The anti-reflection film (16) is then deposited on the AlGaP layer (14) using an RF chemical vapor deposition process or a thermal evaporation process.

    摘要翻译： 本发明提供了一种宽带传输保护涂层（10），其包括沉积在AlGaP保护层（14）上的沉积在光学基片（12）上的AlGaP保护层（14）和抗反射膜（16）。 涂层（10）适用于典型的红外和宽带光学基板材料，如锗或多光谱ZnS。 在锗基板（12）的情况下，防反射膜（16），（16a）优选由单层硬碳或硬碳和硅的交替层组成。 在多光谱ZnS衬底（12a）的情况下，抗反射膜（16b）优选由层状Al 2 O 3 / TaO 5 / LaF 3 / MgF 2组成。 保护涂层（10）优选通过金属有机化学气相沉积方法沉积在光学基底（12）上，其中初始的AlP层在基底（12）上在约400℃的温度下成核。 然后将衬底（12）升高至约600℃，并且在衬底（12）上生长一层AlGaP（14）至预定厚度。 然后将AlGaP涂覆的光学基板（12）抛光至所需的平滑度。 然后使用RF化学气相沉积工艺或热蒸发工艺将抗反射膜（16）沉积在AlGaP层（14）上。

    Process for treating hard tissues
    8.
    发明授权
    Process for treating hard tissues 失效

    公开(公告)号：US5980253A

    公开(公告)日：1999-11-09

    申请号：US5885

    申请日：1998-01-12

    申请人： Joel D. Oxman ,  Hoa T. Bui ,  Dwight W. Jacobs

    发明人： Joel D. Oxman ,  Hoa T. Bui ,  Dwight W. Jacobs

    IPC分类号： A61K6/00 ,  A61K6/083 ,  A61K6/087 ,  A61B17/06 ,  A61C5/00 ,  A61K6/08 ,  C08L63/00

    CPC分类号： A61K6/0023 ,  Y10S522/908

    摘要： In a first aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a composition that includes a cationically active functional group, a free radically active functional group, and a polymerization initiator capable of initiating free radical polymerization, where the number of moles of cationically active functional groups per gram of composition is no greater than about 0.0075; and (b) exposing the composition to polymerization conditions to form an adhesive bonded to the hard tissue.In a second aspect, a method for treating hard tissue that includes: (a) applying to hard tissue a first polymerizable composition that includes a free radically active functional group and a polymerization initiator capable of initiating free radical polymerization, but is essentially free of polymerizable components having cationically active functional groups and is capable of forming an adhesive bonded to the hard tissue upon exposure to polymerization conditions; (b) applying a second polymerizable composition; and (c) exposing the second composition to polymerization conditions to form a hardened composition adhered to the hard tissue. The second composition includes (i) a cationically active functional group and (ii) an polymerization initiator capable of initiating cationic polymerization.

    Dental material including fatty acid, dimer thereof, or trimer thereof
    10.
    发明授权
    Dental material including fatty acid, dimer thereof, or trimer thereof 有权
    牙科材料包括脂肪酸，二聚体或其三聚体

    公开(公告)号：US06613812B2

    公开(公告)日：2003-09-02

    申请号：US09753945

    申请日：2001-01-03

    申请人： Hoa T. Bui ,  Brant U. Kolb ,  Sumita B. Mitra

    发明人： Hoa T. Bui ,  Brant U. Kolb ,  Sumita B. Mitra

    IPC分类号： A61K6083

    CPC分类号： A61K6/0017 ,  A61K6/0023 ,  A61K6/0038 ,  A61K6/0835 ,  C08L43/00 ,  C08L33/00

    摘要： A dental composition is provided comprising (a) a part A comprising fluoroaluminosilicate glass that has been surface treated with agents selected from the group consisting of silane, silanol and combinations thereof, and at least one fatty acid, dimer thereof, or trimer thereof; and (b) a part B comprising at least one polyacid. The composition further comprises resin that can be curable or non-curable and at least one initiator. The composition exhibits adhesion to dentin, and the treated FAS glass contained therein does not settle out with time.

    摘要翻译： 提供了一种牙科用组合物，其包含（a）包含氟铝硅酸盐玻璃的部分A，其已经用选自硅烷，硅烷醇及其组合的物质以及至少一种脂肪酸，二聚体或其三聚体进行表面处理; 和（b）包含至少一种多酸的部分B. 组合物还包含可固化或不可固化的树脂和至少一种引发剂。 该组合物表现出对牙本质的粘附性，并且其中所含的经处理的FAS玻璃不随时间而沉降。