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    PREPARATION OF MESO-POROUS POLYMER BASED NANO-POLYMERIZED COMPOSITE MATERIAL
    2.
    发明申请
    PREPARATION OF MESO-POROUS POLYMER BASED NANO-POLYMERIZED COMPOSITE MATERIAL 失效
    基于多孔聚合物的纳米聚合复合材料的制备

    公开(公告)号：US20110172084A1

    公开(公告)日：2011-07-14

    申请号：US13120281

    申请日：2009-09-15

    申请人： Hyun Tae Jang ,  Wang Seog Cha ,  Ji Yun Lee ,  Bhagiyalakshmi Markandan ,  Anuradha Ramani ,  Hwa Young Lee ,  Joo Boo Lee ,  Sung Yong Lee

    发明人： Hyun Tae Jang ,  Wang Seog Cha ,  Ji Yun Lee ,  Bhagiyalakshmi Markandan ,  Anuradha Ramani ,  Hwa Young Lee ,  Joo Boo Lee ,  Sung Yong Lee

    IPC分类号： B01J37/34 ,  B05D3/00 ,  B05D3/12 ,  B01J20/32 ,  B82Y40/00 ,  B82Y30/00

    CPC分类号： B01J20/20 ,  B01D53/02 ,  B01D2253/202 ,  B01D2257/504 ,  B01J20/02 ,  B01J20/0211 ,  B01J20/06 ,  B01J20/08 ,  B01J20/103 ,  B01J20/18 ,  B01J20/205 ,  B01J20/261 ,  B01J20/262 ,  B01J20/28057 ,  B01J20/28083 ,  B01J20/3204 ,  B01J20/327 ,  B01J20/3272 ,  B01J2220/46 ,  B82Y30/00 ,  B82Y40/00 ,  Y02C10/08

    摘要： Disclosed herein is a method for preparation of a mesoporous polymer nano-composite material, more particularly, a method for preparation of a meso-porous polymer nano-polymerized composite material which includes: drying a solid material having pores under vacuum at ambient temperature and pressure; adding a first organic solvent to the vacuum dried solid material in the reactor and dispersing the first organic solvent in pores of the solid material by an ultrasonicator to remove air while wetting a surface of the solid material with acetonitrile; adding a constant amount of a material having radicals or functional groups relative to weight of the mixture containing the solid material and the first organic solvent in a reactor, which was prepared in the above step, and agitating the mixture; introducing a polymerization initiator into the reactor containing the mixture prepared in the above step, in order to initiate polymerization of the mixture in the reactor; using a second organic solvent to filter and wash the reaction product after completion of the polymerization, in order to remove the unreacted material having radicals or functional groups as well as the polymerization initiator from the product; and drying the treated product to eliminate the second organic solvent from the same after removal of the unreacted material having radicals or functional groups as well as the polymerization initiator from the product.

    摘要翻译： 本文公开了一种制备介孔聚合物纳米复合材料的方法，更具体地说，涉及一种制备中孔多孔聚合物纳米复合材料的方法，该方法包括：在环境温度和压力下干燥具有真空孔的固体材料 ; 向反应器中的真空干燥的固体材料中加入第一有机溶剂，并通过超声波分散器将第一有机溶剂分散在固体材料的孔中，以除去空气，同时用乙腈润湿固体物质的表面; 在上述步骤中制备的反应器中加入恒定量的相对于含有固体物质和第一有机溶剂的混合物重量的自由基或官能团的材料，并搅拌该混合物; 在含有上述步骤中制备的混合物的反应器中引入聚合引发剂，以引发混合物在反应器中的聚合反应; 使用第二有机溶剂在聚合完成后过滤和洗涤反应产物，以从产物中除去具有自由基或官能团的未反应物质以及聚合引发剂; 并且从产物中除去具有自由基或官能团的未反应物质以及聚合引发剂后，干燥经处理的产物以从其中除去第二有机溶剂。