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公开(公告)号：US4265406A
公开(公告)日：1981-05-05
申请号：US44161
申请日：1979-05-31
Applicant: Derek A. Palgrave , Frederick A. Waite , James D. Birchall , John Cooper , James A. Enever
Inventor： Derek A. Palgrave , Frederick A. Waite , James D. Birchall , John Cooper , James A. Enever
CPC classification number: C05C1/02 , B02C23/06 , Y10S149/112
Abstract: A process is described for the comminution of a solid material in the presence of a saturated solution of the solid in a liquid in which the solid has a solubility greater than 1%, and also in the presence of an additive dissolved in the saturated solution which can at least partially inhibit regrowth at crystal surfaces of the solid material. The process is of particular interest for the comminution of water-soluble salts in the presence of their saturated aqueous solutions and may be employed to make, inter alia, improved slurry explosives and fluid fertilizer compositions.
Abstract translation: 描述了一种在固体在固体溶解度大于1％的液体中的固体的饱和溶液存在下粉碎固体材料的方法，以及溶解在饱和溶液中的添加剂的存在下， 可以至少部分地抑制固体材料的晶体表面的再生长。 该方法在其饱和水溶液存在下粉碎水溶性盐是特别有意义的，并且可用于特别改进的浆料炸药和流体肥料组合物。
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公开(公告)号：US4482372A
公开(公告)日：1984-11-13
申请号：US452497
申请日：1982-12-23
Applicant: Derek A. Palgrave , Frederick A. Waite , James D. Birchall , John Cooper , James A. Enever
Inventor： Derek A. Palgrave , Frederick A. Waite , James D. Birchall , John Cooper , James A. Enever
CPC classification number: C05C1/02 , B02C23/06 , Y10S149/112
Abstract: A fluid fertilizer composition based essentially on potassium chloride and an ammonium phosphate prepared by a process which comprises comminuting a solid substance containing potassium chloride and ammonium phosphate by grinding in the presence of a saturated solution of solid in a liquid in which the solid has a solubility greater than 1% by weight, the mixture of the solution and the solid being in fluid condition with the solid being a separate phase during grinding and the solution having dissolved therein an additive which is a crystal growth inhibitor for the solid whereby crystal growth is inhibited at both existing crystal surfaces and new crystal surfaces created by the breaking down of relatively coarse particles.
Abstract translation: 一种基本上基于氯化钾和一种磷酸铵的流体肥料组合物，其通过以下方法制备，所述方法包括在固体在其中具有溶解度的液体中的固体的饱和溶液存在下，研磨含有氯化钾和磷酸铵的固体物质 大于1重量％，溶液和固体的混合物处于流体状态，固体在研磨期间是分离相，并且溶液中溶解有作为固体的晶体生长抑制剂的添加剂，从而晶体生长被抑制 在现有的晶体表面和通过相对粗糙的颗粒的分解产生的新的晶体表面。
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Patent Agency Ranking
公开(公告)号：US4384903A
公开(公告)日：1983-05-24
申请号：US201972
申请日：1980-10-29
Applicant: James A. Enever
Inventor： James A. Enever
CPC classification number: C06B47/14 , F02B3/06 , Y10S149/112
Abstract: An aqueous slurry explosive blasting composition comprising an aqueous suspension of water-soluble crystalline oxidizing salt consisting predominantly of ammonium nitrate, which salt has been comminuted in a saturated aqueous solution in the presence of a water-soluble crystal-growth inhibiting surfactant having a hydrophobic portion and a hydrophilic portion in its molecule, in intimate admixture with liquid water-immiscible hydrocarbon fuel sensitizer. The surfactant maintains the oxidizer salt in a finely divided state and also ensures that the liquid hydrocarbon remains uniformly distributed throughout the explosive mass as a stable coating of droplets on the salt particles thereby enhancing the explosive sensitivity of the composition. The preferred fuel is diesel oil and preferred surfactants include sodium carboxymethyl cellulose, long chain aliphatic amines, polyacrylic acids, sulphonated nuclear aromatic compounds, sulphonated dyes, sulphonated polymers and long chain alcohol sulphonates and phosphonates.
Abstract translation: 一种含水浆料爆炸性组合物，其包含主要由硝酸铵组成的水溶性结晶氧化盐的水性悬浮液，该盐在具有疏水部分的水溶性晶体生长抑制性表面活性剂存在下在饱和水溶液中粉碎 和分子中的亲水部分，与液态水不混溶烃燃料敏化剂紧密混合。 表面活性剂将氧化剂盐保持在细分的状态，并且还确保液体烃保持均匀分布在整个爆炸物质中，作为在盐颗粒上的稳定的液滴涂层，从而增强组合物的爆炸敏感性。 优选的燃料是柴油，优选的表面活性剂包括羧甲基纤维素钠，长链脂族胺，聚丙烯酸，磺化核芳烃化合物，磺化染料，磺化聚合物和长链醇磺酸盐和膦酸盐。
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4.发明授权
公开(公告)号：US4367104A
公开(公告)日：1983-01-04
申请号：US181344
申请日：1980-08-26
Applicant: Hugh S. Paton , James A. Enever
Inventor： Hugh S. Paton , James A. Enever
Abstract: Water-soluble crystalline material which has been comminuted in a saturated aqueous solution of the material in the presence of a water-soluble crystal-growth inhibitor having a hydrophobic portion and a hydrophilic portion in its molecular structure is mixed with a deflocculant which inhibits the interaction of the hydrophobic molecular portions whenever the comminuted solid is suspended in water. The viscosity of aqueous suspensions of comminuted solid is thereby stabilized.The invention is especially beneficial in the preparation of aqueous suspensions of finely comminuted ammonium nitrate for use in slurry blasting explosives.With crystal-growth inhibitors such as water-soluble polysaccharide derivatives, long chain aliphatic amines, polyacrylic acids, sulphonated nuclear aromatic compounds, sulphonated dyes or sulphonated polymers the preferred deflocculant, which should be different from the crystal-growth inhibitor, may include water-soluble polysaccharide derivatives, polyacrylic acid, polyvinyl pyrrolidone, sodium lignosulphonate and/or a salt of a condensate of naphthalene sulphonic acid with formaldehyde.
Abstract translation: 在具有疏水部分和分子结构中的亲水部分的水溶性晶体生长抑制剂存在下，在饱和水溶液中粉碎的水溶性晶体材料与抑制相互作用的抗絮凝剂混合 的疏水分子部分，只要粉碎的固体悬浮在水中。 粉碎固体的水性悬浮液的粘度由此稳定。 本发明特别有益于制备用于浆料爆破炸药的细粉碎硝酸铵的水悬浮液。 使用结晶生长抑制剂如水溶性多糖衍生物，长链脂族胺，聚丙烯酸，磺化核芳烃化合物，磺化染料或磺化聚合物，应该与结晶生长抑制剂不同的优选的抗絮凝剂可以包括水 - 可溶性多糖衍生物，聚丙烯酸，聚乙烯吡咯烷酮，木素磺酸钠和/或萘磺酸与甲醛的缩合物的盐。
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公开(公告)号：US4331490A
公开(公告)日：1982-05-25
申请号：US227413
申请日：1981-01-22
Applicant: Derek A. Palgrave , Frederick A. Waite , James D. Birchall , John Cooper , James A. Enever
Inventor： Derek A. Palgrave , Frederick A. Waite , James D. Birchall , John Cooper , James A. Enever
CPC classification number: C05C1/02 , B02C23/06 , Y10S149/112
Abstract: A slurry composition based essentially on ammonium nitrate, prepared by a process which comprises comminuting solid substance containing ammonium nitrate by grinding in the presence of a saturated solution of solid in a liquid in which the solid has a solubility greater than 1% by weight, the mixture of the solution and the solid being in fluid condition with the solid being a separate phase during grinding and the solution having dissolved therein an additive which is a crystal growth inhibitor for the solid whereby crystal growth is inhibited at both existing crystal surfaces and new crystal surfaces created by the breaking down of relatively coarse particles.
Abstract translation: 基于硝酸铵的浆料组合物，其通过以下方法制备，该方法包括在固体溶解度大于1重量％的液体中的固体饱和溶液存在下研磨，粉碎含有硝酸铵的固体物质， 溶液和固体的混合物处于流体状态，固体在研磨过程中是分离相，溶液中溶解有作为固体的晶体生长抑制剂的添加剂，从而在现有晶体表面和新晶体上晶体生长被抑制 通过破碎比较粗糙的颗粒产生的表面。
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公开(公告)号：US4367103A
公开(公告)日：1983-01-04
申请号：US123076
申请日：1980-02-20
Applicant: James A. Enever
Inventor： James A. Enever
CPC classification number: C06B47/14
Abstract: A powder explosive composition comprising particulate inorganic oxidizing salt, finely divided metal sensitizer and, optionally additional fuel consisting of discrete granules containing oxidizing salt and sensitizing metal coated with a tough, cohesive, resilient gelled solution of the oxidizing salt, the amount of the coating being insufficient to form a continuous gelled phase. The composition is more water resistant, less dusty and less sensitive to friction and impact than the metal sensitized powder compositions of the prior art.
Abstract translation: 一种粉末炸药组合物，其包含颗粒状无机氧化盐，细碎金属敏化剂和任选的附加燃料，其由含有氧化盐的分散颗粒和涂覆有所述氧化盐的韧性，粘性的弹性胶凝溶液的敏化金属组成，所述涂层的量为 不足以形成连续凝胶相。 该组合物比现有技术的金属敏化粉末组合物更耐水，更少的粉尘和对摩擦和冲击的敏感性较低。
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公开(公告)号：US3943090A
公开(公告)日：1976-03-09
申请号：US266873
申请日：1972-06-28
Applicant: James A. Enever
Inventor： James A. Enever
Abstract: A method of forming a composite carbon fibres and synthetic plastics material by embodying the fibres in a matrix of the synthetic plastics material. In the interfacial region of the carbon fibres and synthetic plastics material an elastomeric resin is provided which is compatible with the synthetic plastics material used for the matrix to minimise the tendency for cracks to initiate at the interface.
Abstract translation: 通过将纤维体现在合成塑料材料的基质中来形成复合碳纤维和合成塑料材料的方法。 在碳纤维和合成塑料材料的界面区域中，提供了与用于基体的合成塑料材料相容的弹性体树脂，以最小化裂缝在界面处发生的趋势。
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