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    METHODS OF MAKING GLASS-CRYSTALLINE PARTICLES INCLUDING A GLASS COMPONENT AND A CRYSTALLINE COMPONENT
    3.
    发明申请
    METHODS OF MAKING GLASS-CRYSTALLINE PARTICLES INCLUDING A GLASS COMPONENT AND A CRYSTALLINE COMPONENT 失效
    制造玻璃晶粒的方法，包括玻璃组分和晶体组分

    公开(公告)号：US20110233486A1

    公开(公告)日：2011-09-29

    申请号：US12891244

    申请日：2010-09-27

    Applicant: Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    Inventor： Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    IPC: H01B1/20 ,  C03B19/10

    CPC classification number: C03B19/1065

    Abstract: Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.

    Abstract translation: 公开了一种制造包含玻璃组分和结晶组分的玻璃晶粒的方法，包括以下步骤：a）提供包含溶剂，玻璃组分组合物和结晶组分组合物的前体溶液; b）形成包含前体溶液的细碎液滴的气溶胶，其中液滴浓度低于液滴的碰撞和随后的聚结导致液滴浓度降低10％的浓度; c）加热气溶胶，其中在加热时形成玻璃晶体颗粒，其中所述玻璃晶体颗粒包含玻璃组分和结晶组分，并且其中所述结晶组分包含一种或多种金属氧化物; 和d）分离玻璃晶粒。

    Methods of making glass-crystalline particles including a glass component and a crystalline component
    4.
    发明授权
    Methods of making glass-crystalline particles including a glass component and a crystalline component 失效
    制造玻璃成分和结晶成分的玻璃结晶粒子的方法

    公开(公告)号：US08545733B2

    公开(公告)日：2013-10-01

    申请号：US12891244

    申请日：2010-09-27

    Applicant: Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    Inventor： Eric Lee Brantley ,  John T. Chaplinsky ,  Howard David Glicksman ,  James J. Krajewski ,  Brian J. Laughlin ,  Kurt Richard Mikeska ,  Lawrence V. Triboletti

    IPC: H01B1/12

    CPC classification number: C03B19/1065

    Abstract: Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.

    Abstract translation: 公开了一种制造包含玻璃组分和结晶组分的玻璃晶粒的方法，包括以下步骤：a）提供包含溶剂，玻璃组分组合物和结晶组分组合物的前体溶液; b）形成包含前体溶液的细碎液滴的气溶胶，其中液滴浓度低于液滴的碰撞和随后的聚结导致液滴浓度降低10％的浓度; c）加热气溶胶，其中在加热时形成玻璃晶体颗粒，其中所述玻璃晶体颗粒包含玻璃组分和结晶组分，并且其中所述结晶组分包含一种或多种金属氧化物; 和d）分离玻璃晶粒。

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