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    Asymmetric dioxazine compounds and use thereof as fiber reactive dyes
    1.
    发明授权
    Asymmetric dioxazine compounds and use thereof as fiber reactive dyes 失效
    不对称二恶嗪化合物及其作为纤维活性染料的用途

    公开(公告)号：US5650507A

    公开(公告)日：1997-07-22

    申请号：US579645

    申请日：1995-12-27

    申请人： Kingo Akahori ,  Junya Hada ,  Takashi Omura ,  Shigeru Kawabata ,  Naoki Harada

    发明人： Kingo Akahori ,  Junya Hada ,  Takashi Omura ,  Shigeru Kawabata ,  Naoki Harada

    IPC分类号： C09B62/503 ,  D06P1/384 ,  C07D498/04

    CPC分类号： C09B62/5033

    摘要： An asymmetric dioxazine compound of the following formula: ##STR1## wherein R is sulfo, halogeno, alkoxy, alkyl or carboxy; R.sub.1 and R.sub.2 are each hydrogen or alkyl; R.sub.3 is hydrogen, alkyl or acyl; X.sub.1 and X.sub.2 are each hydrogen, halogeno, alkyl, alkoxy or phenoxy; Y is aliphatic amino having a vinylsulfonyl or .beta.-substituted ethylsulfonyl fiber-reactive group; and Q is unsubstitued, substituted or cyclic amino; is useful for dyeing or printing fiber materials blue with excellence in build-up properties and various fastness properties.

    摘要翻译： 下式的不对称二恶嗪化合物：其中R是磺基，卤代，烷氧基，烷基或羧基; R1和R2各自为氢或烷基; R3是氢，烷基或酰基; X1和X2各自为氢，卤代，烷基，烷氧基或苯氧基; Y是具有乙烯基磺酰基或β-取代的乙基磺酰基纤维反应性基团的脂族氨基; Q是未取代的，取代的或环状的氨基; 用于染色或印刷纤维材料蓝色，具有优异的聚集性能和各种牢度性能。

    Bisazo compounds and use thereof as fiber reactive dyes
    2.
    发明授权
    Bisazo compounds and use thereof as fiber reactive dyes 失效
    双偶氮化合物及其作为纤维活性染料的用途

    公开(公告)号：US5637705A

    公开(公告)日：1997-06-10

    申请号：US532510

    申请日：1995-09-22

    申请人： Sigeru Sasaki ,  Kingo Akahori ,  Takeshi Washimi ,  Takashi Omura ,  Toshiyuki Araki ,  Atsushi Inoue

    发明人： Sigeru Sasaki ,  Kingo Akahori ,  Takeshi Washimi ,  Takashi Omura ,  Toshiyuki Araki ,  Atsushi Inoue

    IPC分类号： C09B62/513 ,  C07D251/52 ,  C07D251/54

    CPC分类号： C09B62/513

    摘要： A bisazo compound of the following formula: ##STR1## wherein R.sup.1 and R.sup.3 are each hydrogen or alkyl; D is phenylene or naphthylene; one of X.sup.1 and X.sup.2 is NH.sub.2 and the other is OH; Z.sup.1 and Z.sup.2 are each --CH.dbd.CH.sub.2 or --CH.dbd.CH.sub.2 Z' in which Z' is a splittable group; B is monosulfophenylene, monosulfophenylene-methylene or mono- or di-sulfonaphthylene-methylene; U is phenylene or an aliphatic bridging group; and J is an amono-derivative group or, J may be alkoxy when X.sup.1 is OH and U is phenylene, and J may be alkoxy or phenoxy when X.sup.1 is OH and U is the aliphatic bridging group. This compound is useful for dyeing or printing fiber materials and gives a dyed or printed product having a color superior in various fastness properties with superior build-up property.

    摘要翻译： 下式的双偶氮化合物：其中R 1和R 3各自为氢或烷基; D是亚苯基或亚萘基; X1和X2之一是NH2，另一个是OH; Z 1和Z 2各自为-CH = CH 2或-CH = CH 2 Z'，其中Z'为可裂组; B是单磺酰亚砜，单磺酰亚苯基 - 亚甲基或单 - 或二 - 磺基亚乙基 - 亚甲基; U是亚苯基或脂族桥基; 并且J是氨基衍生基团，或者当X1是OH且U是亚苯基时，J可以是烷氧基，当X 1是OH且U是脂族桥基时，J可以是烷氧基或苯氧基。 该化合物可用于染色或印刷纤维材料，并提供具有优异的各种牢度性能的优异的成色性能的染色或印刷产品。

    Monoazo compounds having vinylsulfone type fiber reactive group and method for dyeing or printing fiber materials using the same
    5.
    发明授权
    Monoazo compounds having vinylsulfone type fiber reactive group and method for dyeing or printing fiber materials using the same 失效
    具有乙烯基砜型纤维反应性基团的单偶氮化合物和使用其的纤维材料的染色或印花方法

    公开(公告)号：US5488098A

    公开(公告)日：1996-01-30

    申请号：US193646

    申请日：1994-02-07

    申请人： Masayuki Miki ,  Kingo Akahori ,  Yutaka Kayane ,  Takeshi Washimi

    发明人： Masayuki Miki ,  Kingo Akahori ,  Yutaka Kayane ,  Takeshi Washimi

    IPC分类号： C09B62/085 ,  C09B62/44 ,  C09B62/51 ,  D06P1/384

    CPC分类号： C09B62/4413 ,  C09B62/51

    摘要： A monoazo compound of the following formula, ##STR1## wherein D is phenylene or naphthylene; X is halogeno, pyridinio or ##STR2## B is --OR.sub.3, --SR.sub.4, ##STR3## in which R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, r is 0 or 1, and E is O, SO, SO.sub.2, CH.sub.2 or NR.sub.8, in which R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl; R, R.sub.1, R.sub.2 and R.sub.7 are each hydrogen or alkyl; A.sub.1, A.sub.2 and A.sub.3 are each phenylene, naphthylene or alkylene; Z.sub.1, Z.sub.2 and Z.sub.3 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a splittable group; and p is 0 or 1; which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.

    摘要翻译： 下式的单偶氮化合物，其中D是亚苯基或亚萘基; X是卤素，吡啶鎓或B是-OR 3，-SR 4，其中R 3，R 4，R 5和R 6各自是氢，烷基，苯基，萘基或苄基，r是0或1，E是 O，SO，SO 2，CH 2或NR 8，其中R 8是氢或C 1 -C 4烷基; R，R 1，R 2和R 7各自为氢或烷基; A1，A2和A3各自为亚苯基，亚萘基或亚烷基; Z 1，Z 2和Z 3各自为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可裂解基团; p为0或1; 该化合物可用于染色或印刷纤维材料以获得染色或印刷成具有优异的各种牢度性能的颜色的产品，具有优异的聚集性能。

    Monoazo compounds having naphthylazonaphtylamino group and use therefor for dyeing or printing fiber materials
    6.
    发明授权
    Monoazo compounds having naphthylazonaphtylamino group and use therefor for dyeing or printing fiber materials 失效
    具有萘氮杂萘基氨基的单偶氮化合物，用于染色或印刷纤维材料

    公开(公告)号：US5359040A

    公开(公告)日：1994-10-25

    申请号：US963553

    申请日：1992-10-20

    申请人： Kingo Akahori ,  Masayuki Miki ,  Takeshi Washimi ,  Yutaka Kayane

    发明人： Kingo Akahori ,  Masayuki Miki ,  Takeshi Washimi ,  Yutaka Kayane

    IPC分类号： C07D251/54 ,  C09B62/085 ,  C09B62/51 ,  D06P1/384

    CPC分类号： C09B62/51

    摘要： A monoazo compound represented by the following formula (I) in the free acid form: ##STR1## wherein X is an alkylamino, C.sub.5 -C.sub.7 cycloalkylamino, piperidino, pyrrolidino or morpholino group which is unsubstituted or substituted with a substituent other than sulfo, R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 alkyl, R.sub.1 and R.sub.2 independently of one another are each hydrogen, methoxy, ethoxy, methyl, ethyl, chloro, bromo, nitro, carboxy or sulfo, Z is vinyl or -CH.sub.2 CH.sub.2 Y in which Y is a group which is split by the action of an alkali and p is 0 or 1. This compound is a reactive dye suitable for dyeing or printing fiber materials containing hydroxyl group and/or amide group in red color. This compound is high in dissolvability and can give dyed or printed products excellent in dyeability such as build-up property and various fastnesses.

    摘要翻译： 由游离酸形式的下式（I）表示的单偶氮化合物：其中X是未被取代或被取代基以外的取代基取代的烷基氨基，C 5 -C 7环烷基氨基，哌啶子基，吡咯烷子基或吗啉代基 磺基，R为氢或未取代或取代的C 1 -C 4烷基，R 1和R 2各自独立地为氢，甲氧基，乙氧基，甲基，乙基，氯，溴，硝基，羧基或磺基，Z为乙烯基或-CH2CH2Y Y是通过碱的作用而分裂的基团，p是0或1.该化合物是适用于染色或印刷含有红色的羟基和/或酰胺基的纤维材料的活性染料。 该化合物的溶解性高，可以赋予染色性，印染性等优异的染色性，例如聚集性和各种坚牢度。

    Bisazo compounds having sulfophenylazonaphtylazophenylamino-s-triazinyl group and use thereof for dyeing or printing fiber materials
    7.
    发明授权
    Bisazo compounds having sulfophenylazonaphtylazophenylamino-s-triazinyl group and use thereof for dyeing or printing fiber materials 失效
    具有磺基苯基偶氮萘基偶氮苯基氨基-s-三嗪基的双偶氮化合物及其用于染色或印刷纤维材料的用途

    公开(公告)号：US5306814A

    公开(公告)日：1994-04-26

    申请号：US993713

    申请日：1992-12-17

    申请人： Kingo Akahori ,  Takeshi Washimi ,  Takashi Omura ,  Mahito Fujita

    发明人： Kingo Akahori ,  Takeshi Washimi ,  Takashi Omura ,  Mahito Fujita

    IPC分类号： C09B62/09 ,  C09B62/513 ,  D06P1/384

    CPC分类号： C09B62/513 ,  C09B62/09

    摘要： A bisazo compound represented by the following formula (I) in the free acid form: ##STR1## wherein R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 alkyl; A is an unsubstituted or substituted phenylene or naphthylene group; Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a group capable of being split by the action of an alkali; X is --NR.sub.1 R.sub.2, C.sub.5 -C.sub.7 cycloalkylamino or ##STR2## in which Q is --CH.sub.2 --, --O--, --SO.sub.2 --, --SO-- or --NR.sub.3 -- in which R.sub.3 is hydrogen or C.sub.1 -C.sub.4 alkyl; and n is 1 or 2; R.sub.1 is hydrogen or unsubstituted or substituted alkyl; R.sub.2 is hydrogen or an unsubstituted or substituted alkyl or phenyl group; and m is 1 or 2, provided that when m is 2, X is ##STR3## This compound is suitable for dyeing and printing cellulose fiber, natural and synthetic polyamide fibers, polyurethane fiber, leather and mixed yarns thereof, to obtain dyed or printed products of a color fast to light and wetness with superior build-up property.

    摘要翻译： 由游离酸形式的下式（I）表示的双偶氮化合物：（*化学结构*）（I）（*化学结构*）其中R为氢或未取代或取代的C 1 -C 4烷基; A是未取代或取代的亚苯基或亚萘基; Z是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y是能够通过碱的作用而分裂的基团; X是-NR 1 R 2，C 5 -C 7环烷基氨基或（*化学结构*）其中Q是-CH 2 - ， - O - ， - SO 2 - ， - SO-或-NR 3 - ，其中R 3是氢或C 1 -C 4烷基; n为1或2; R1是氢或未取代或取代的烷基; R2是氢或未取代或取代的烷基或苯基; m为1或2，条件是当m为2时，X为（*化学结构*）该化合物适用于染色和印刷纤维素纤维，天然和合成聚酰胺纤维，聚氨酯纤维，皮革及其混纺纱线，以获得 染色或印刷的产品，颜色快速，轻盈，具有优异的积聚性能。

    1-aminoanthraquinone dye compound having fiber reactive group through sulfur or oxygen atom at 4-position and imparting red color
    8.
    发明授权
    1-aminoanthraquinone dye compound having fiber reactive group through sulfur or oxygen atom at 4-position and imparting red color 失效
    具有纤维反应性基团的1-氨基蒽醌染料化合物，通过硫或氧原子在4位上赋予红色

    公开(公告)号：US5266696A

    公开(公告)日：1993-11-30

    申请号：US836825

    申请日：1992-02-19

    申请人： Kingo Akahori ,  Naoki Harada ,  Yutaka Kayane ,  Takashi Omura

    发明人： Kingo Akahori ,  Naoki Harada ,  Yutaka Kayane ,  Takashi Omura

    IPC分类号： C09B62/024 ,  C09B62/44 ,  C09B62/505 ,  C07D251/70 ,  C09B62/06 ,  D06P1/382 ,  D06P1/384

    CPC分类号： C09B62/024 ,  C09B62/4409 ,  C09B62/505

    摘要： Anthraquinone compounds of the formula, ##STR1## wherein R is hydrogen, alkyl or the like, R.sub.1 and R.sub.2 are each hydrogen, halogen or sulfo, l is 1 or 2, X is sulfo or the like or --V--A--(W).sub.m --Z, and Y is --V.sub.1 --A.sub.1 --U, wherein V and V.sub.1 are each --O-- or --S--, A and A.sub.1 are each a divalent group such as ##STR2## W is --NH-- or the like, Z is hydrogen or a fiber reactive group, and U is hydrogen, a fiber reactive group or a fiber reactive group-containing group, provided that at least one of Z and U is or has a fiber reactive group, which is useful for dyeing or printing fiber materials such as cotton to give a dyed or printed product having excellent fastness properties, particularly those such as light fastness and perspiration-light fastness.

    摘要翻译： 下式的蒽醌化合物，其中R是氢，烷基等，R 1和R 2各自为氢，卤素或磺基，l为1或2，X为磺基等或-VA-（W）mZ ，Y为-V1-A1-U，其中V和V1各自为-O-或-S-，A和A1各自为二价基团，例如W为-NH-等，Z为氢 或纤维反应性基团，U为氢，纤维反应性基团或含纤维反应性基团，条件是Z和U中的至少一个为或具有纤维反应性基团，其可用于染色或印刷纤维材料 例如棉，以得到具有优异坚牢性的染色或印刷产品，特别是耐光牢度和耐汗牢度等。

    Monoazo compounds and method for dyeing or printing fiber materials using the same
    10.
    发明授权
    Monoazo compounds and method for dyeing or printing fiber materials using the same 失效
    单偶氮化合物和使用其的纤维材料的染色或印花方法

    公开(公告)号：US5606092A

    公开(公告)日：1997-02-25

    申请号：US546321

    申请日：1995-10-20

    申请人： Masayuki Miki ,  Kingo Akahori ,  Yutaka Kayane ,  Takeshi Washimi

    发明人： Masayuki Miki ,  Kingo Akahori ,  Yutaka Kayane ,  Takeshi Washimi

    IPC分类号： C09B62/085 ,  C09B62/44 ,  C09B62/51 ,  D06P1/384 ,  C07C317/28 ,  C07C317/34

    CPC分类号： C09B62/4413 ,  C09B62/51

    摘要： A monoazo compound of the following formula, ##STR1## wherein D is phenylene or naphthylene; X is halogeno, pyridinio or ##STR2## B is --OR.sub.3, --SR.sub.4, ##STR3## in which R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, r is 0 or 1, and E is O, SO, SO.sub.2, CH.sub.2 or NR.sub.8, in which R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl; R, R.sub.1, R.sub.2 and R.sub.7 are each hydrogen or alkyl; A.sub.1, A.sub.2 and A.sub.3 are each phenylene, naphthylene or alkylene; Z.sub.1, Z.sub.2 and Z.sub.3 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a splittable group; and p is 0 or 1; which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.

    摘要翻译： 下式的单偶氮化合物，其中D是亚苯基或亚萘基; X是卤素，吡啶鎓或B是-OR 3，-SR 4，其中R 3，R 4，R 5和R 6各自是氢，烷基，苯基，萘基或苄基，r是0或1，E是 O，SO，SO 2，CH 2或NR 8，其中R 8是氢或C 1 -C 4烷基; R，R 1，R 2和R 7各自为氢或烷基; A1，A2和A3各自为亚苯基，亚萘基或亚烷基; Z 1，Z 2和Z 3各自为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可裂解基团; p为0或1; 该化合物可用于染色或印刷纤维材料以获得染色或印刷成具有优异的各种牢度性能的颜色的产品，具有优异的聚集性能。