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    Use of cyclic carbonates in epoxy resin compositions
    2.
    发明授权
    Use of cyclic carbonates in epoxy resin compositions 有权
    在环氧树脂组合物中使用环状碳酸酯

    公开(公告)号：US08741988B2

    公开(公告)日：2014-06-03

    申请号：US13158841

    申请日：2011-06-13

    申请人： Rainer Klopsch ,  Andreas Lanver ,  Achim Kaffee ,  Klaus Ebel ,  Miran Yu

    发明人： Rainer Klopsch ,  Andreas Lanver ,  Achim Kaffee ,  Klaus Ebel ,  Miran Yu

    IPC分类号： C08L63/00 ,  C08G59/00

    CPC分类号： C08L63/00 ,  C08G59/00 ,  C08K5/04

    摘要： The present invention relates to the use of cyclic carbonates of the formula I or a mixture thereof in epoxy resin compositions and also to epoxy resin compositions which comprise such cyclic carbonates. in which R1 and R2 independently of each other are hydrogen, C1-C6-alkyl, C1-C4-alkoxy-C1-C4-alkyl, C5-C6-cycloalkyl, phenyl, phenyl-C1-C4-alkyl, C2-C6-alkenyl or C2-C6-alkynyl, or R1 and R2 together are a C3-C11-alkylene group; R3 and R4 independently of each other are hydrogen, C1-C6-alkyl, C1-C4-alkoxy-C1-C4-alkyl, C5-C6-cycloalkyl, phenyl, phenyl-C1-C4-alkyl, C2-C6-alkenyl or C2-C6-alkynyl, or R3 and R4 together are a C4-C6-alkylene group; or mixtures thereof, as additives in epoxy resin compositions.

    摘要翻译： 本发明涉及式I的环状碳酸酯或其混合物在环氧树脂组合物中的用途，还涉及包含这种环状碳酸酯的环氧树脂组合物。 其中R1和R2彼此独立地是氢，C1-C6-烷基，C1-C4-烷氧基-C1-C4-烷基，C5-C6-环烷基，苯基，苯基-C1-C4-烷基，C2-C6- 烯基或C 2 -C 6炔基，或者R 1和R 2一起是C 3 -C 11 - 亚烷基; R 3和R 4彼此独立地是氢，C 1 -C 6 - 烷基，C 1 -C 4 - 烷氧基-C 1 -C 4 - 烷基，C 5 -C 6 - 环烷基，苯基，苯基-C 1 -C 4 - 烷基，C 2 -C 6 - 烯基或 C2-C6-炔基或R3和R4一起是C4-C6-亚烷基; 或其混合物，作为环氧树脂组合物中的添加剂。

    Method for the production of 4,4′-[1-trifluoromethyl)alkylidene]-bis-(2,6-diphenylphenols)
    6.
    发明授权
    Method for the production of 4,4′-[1-trifluoromethyl)alkylidene]-bis-(2,6-diphenylphenols) 有权
    制备4,4' - [1-三氟甲基）亚烷基] - 双（2,6-二苯基苯酚）

    公开(公告)号：US08212084B2

    公开(公告)日：2012-07-03

    申请号：US12808865

    申请日：2008-12-17

    申请人： Gabriele Gralla ,  Gunnar Heydrich ,  Klaus Ebel ,  Wolfgang Krause

    发明人： Gabriele Gralla ,  Gunnar Heydrich ,  Klaus Ebel ,  Wolfgang Krause

    IPC分类号： C07C39/16 ,  C07C39/12

    CPC分类号： C07C45/74 ,  C07C37/07 ,  C07C37/20 ,  C07C37/62 ,  C07C49/613 ,  C07C49/653 ,  C07C39/15 ,  C07C39/367

    摘要： The present invention relates to a process for preparing 4,4′-[1-(trifluoromethyl)alkylidene]bis(2,6-diphenylphenols), in particular for preparing 4,4′-[1-(trifluoromethyl)ethylidene]bis(2,6-diphenylphenol), which comprises the self-condensation of cyclohexanone in the presence of a basic catalyst to form tricyclic condensation products, dehydrogenation of the resulting tricyclic condensation products in the presence of a supported transition metal catalyst in the condensed phase to form 2,6-diphenylphenol and reaction of the 2,6-diphenylphenol with a trifluoromethyl ketone. The invention further provides an improved process for preparing 2,6-diphenylphenol by aldol self-condensation of cyclohexanone.

    摘要翻译： 本发明涉及一种制备4,4' - [1-（三氟甲基）亚烷基]双（2,6-二苯基苯酚）的方法，特别是制备4,4' - [1-（三氟甲基）亚乙基]双（ 2,6-二苯基苯酚），其包括环己酮在碱性催化剂存在下的自缩合以形成三环缩合产物，所得三环缩合产物在冷凝相中负载的过渡金属催化剂存在下脱氢形成 2,6-二苯基苯酚和2,6-二苯基苯酚与三氟甲基酮的反应。 本发明还提供了通过环己酮的醛醇自缩合制备2,6-二苯基苯酚的改进方法。

    PROCESS FOR PREPARING HYDROXY-SUBSTITUTED AROMATIC ALDEHYDES
    8.
    发明申请
    PROCESS FOR PREPARING HYDROXY-SUBSTITUTED AROMATIC ALDEHYDES 有权
    制备羟基取代的芳族醛的方法

    公开(公告)号：US20110245544A1

    公开(公告)日：2011-10-06

    申请号：US13078195

    申请日：2011-04-01

    申请人： Klaus Ebel ,  Stefan Rüdenauer

    发明人： Klaus Ebel ,  Stefan Rüdenauer

    IPC分类号： C07C45/61

    CPC分类号： C07C45/65 ,  C07C47/575

    摘要： The present invention therefore relates to a process for preparing an aldehyde of the formula (I) where one, two or all three radicals from the group of R1, R3 and R5 are hydroxyl, and that radical or those radicals from the group of R1, R3 and R5 which are not hydroxyl are each independently hydrogen, C1-C8-alkyl or C6-C14-aryl, and R2 and R4 are each independently hydrogen, C1-C8-alkyl, C1-C8-alkoxy or C6-C14-aryl, which comprises converting an aldehyde of the formula (II) in which one, two or all three radicals from the group of R′1, R′3 and R′5 are C1-C8-alkoxy, and that radical or those radicals from the group of R′1, R′3 and R′5 which are not C1-C8-alkoxy are each independently hydrogen, C1-C8-alkyl or C6-C14-aryl, and R2 and R4 are each as defined for formula (I), at elevated temperature and elevated pressure in the presence of (C1-C4-alkyl)2-amine, and then isolating the reaction product of the formula (I).

    摘要翻译： 因此，本发明涉及一种制备式（I）的醛的方法，其中R 1，R 3和R 5基团中的一个，两个或全部三个基团是羟基，并且该基团或那些来自R1， 不是羟基的R 3和R 5各自独立地为氢，C 1 -C 8 - 烷基或C 6 -C 14 - 芳基，R 2和R 4各自独立地为氢，C 1 -C 8 - 烷基，C 1 -C 8 - 烷氧基或C 6 -C 14 - 芳基 其包括将式（II）的醛转化为其中R 1，R'3和R'5基团中的一个，两个或全部三个基团是C 1 -C 8 - 烷氧基，并且该基团或那些基团 不是C1-C8-烷氧基的R'1，R'3和R'5各自独立地为氢，C1-C8-烷基或C6-C14 - 芳基，R2和R4各自如式 I）在升高的温度和升高的压力下，在（C 1 -C 4 - 烷基）-2-胺的存在下，然后分离式（I）的反应产物。