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公开(公告)号：US07279077B2
公开(公告)日：2007-10-09
申请号：US10685370
申请日：2003-10-13
申请人： Dennis N. Bingham , Bruce M. Wilding , Kerry M. Klingler , William T. Zollinger , Kraig M. Wendt
发明人： Dennis N. Bingham , Bruce M. Wilding , Kerry M. Klingler , William T. Zollinger , Kraig M. Wendt
摘要： A method of forming a chemical composition such as a chemical hydride is described and which includes the steps of selecting a composition having chemical bonds and which is capable of forming a chemical hydride; providing a source of hydrogen; and exposing the selected composition to an amount of ionizing radiation to encourage the changing of the chemical bonds of the selected composition, and chemically reacting the selected composition with the source of hydrogen to facilitate the formation of a chemical hydride.
摘要翻译： 描述了形成诸如化学氢化物的化学组成的方法，其包括选择具有化学键并能够形成化学氢化物的组合物的步骤; 提供氢源; 并将所选择的组合物暴露于一定量的电离辐射，以促进所选择的组合物的化学键的改变，以及使所选择的组合物与氢源化学反应以促进形成化学氢化物。
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公开(公告)号：US4935100A
公开(公告)日：1990-06-19
申请号：US357892
申请日：1989-05-30
申请人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
发明人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
IPC分类号： C07C51/44
CPC分类号： C07C51/44
摘要： Formic acid cannot be completely removed from formic acid and water mixtures by distillation because of the presence of the maximum azeotrope. Formic acid can be readily removed from formic acid - water mixtures by extractive distillation in which the extractive agent is a benzoic acid derivative mixed with certain higher boiling organic compounds. Examples of effective agents are: o-toluic acid and heptanoic acid; 2-benzoylbenzoic acid and methyl salicylate; p-hydroxybenzoic acid, pelargonic acid and 2-hydroxyacetophenone.
摘要翻译： 由于存在最大共沸物，甲酸不能通过蒸馏从甲酸和水混合物中完全除去。 通过萃取蒸馏可以从甲酸 - 水混合物中容易地除去甲酸，其中萃取剂是与某些较高沸点有机化合物混合的苯甲酸衍生物。 有效试剂的实例是：邻甲苯甲酸和庚酸; 2-苯甲酰基苯甲酸和水杨酸甲酯; 对羟基苯甲酸，壬酸和2-羟基苯乙酮。
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公开(公告)号：US07294323B2
公开(公告)日：2007-11-13
申请号：US10778789
申请日：2004-02-13
申请人： Kerry M. Klingler , William T. Zollinger , Bruce M. Wilding , Dennis N. Bingham , Kraig M. Wendt
发明人： Kerry M. Klingler , William T. Zollinger , Bruce M. Wilding , Dennis N. Bingham , Kraig M. Wendt
摘要： A method of producing a chemical hydride is described and which includes selecting a composition having chemical bonds and which is capable of forming a chemical hydride; providing a source of a hydrocarbon; and reacting the composition with the source of the hydrocarbon to generate a chemical hydride.
摘要翻译： 描述了一种生产化学氢化物的方法，其包括选择具有化学键并能够形成化学氢化物的组合物; 提供烃的来源; 并使组合物与烃源产生化学氢化物反应。
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公开(公告)号：US5173156A
公开(公告)日：1992-12-22
申请号：US803509
申请日：1991-12-09
申请人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
发明人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
摘要： Formic acid cannot be completely removed from formic acid--water mixtures by distillation because of the presence of the maximum azeotrope. Formic acid can be readily removed from mixtures containing it and water by using extractive distillation in which the extractive distillation agent is cyclohexanone, isophorone or a mixture of these with certain organic compounds. Typical examples of effective agents are cyclohexanone; isophorone; cyclohexanone and neodecanoic acid; isophorone and diisobutyl ketone.
摘要翻译： 由于存在最大共沸物，甲酸不能通过蒸馏从甲酸 - 水混合物中完全除去。 采用萃取蒸馏法萃取蒸馏剂是环己酮，异佛尔酮或它们与某些有机化合物的混合物，可以容易地从含有它和水的混合物中除去甲酸。 有效试剂的典型例子是环己酮; 异佛尔酮 环己酮和新癸酸; 异佛尔酮和二异丁基酮。
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公开(公告)号：US5006205A
公开(公告)日：1991-04-09
申请号：US297181
申请日：1989-01-17
申请人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
发明人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
摘要： Formic acid cannot be completely removed from formic acid and water mixtures by distillation because of the presence of the maximum azeotrope. Formic acid can be readily removed from formic acid - water mixtures by extractive distillation in which the extractive agent is a mono carboxylic acid mixed with certain high boiling organic compounds. Examples of effective agents are: hexanoic acid and butyl benzoate; octanoic acid and nitrobenzene; heptanoic acid, benzyl benzoate and pelargonic acid.
摘要翻译： 由于存在最大共沸物，甲酸不能通过蒸馏从甲酸和水混合物中完全除去。 通过萃取蒸馏可以从甲酸 - 水混合物中容易地除去甲酸，其中萃取剂是与某些高沸点有机化合物混合的单羧酸。 有效试剂的实例是：己酸和苯甲酸丁酯; 辛酸和硝基苯; 庚酸，苯甲酸苄酯和壬酸。
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6.发明授权
公开(公告)号：US4877490A
公开(公告)日：1989-10-31
申请号：US299977
申请日：1989-01-23
申请人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
发明人： Lloyd Berg , Kraig M. Wendt , Rudolph J. Szabados
摘要： Formic acid cannot be completely removed from formic acid and water mixtures by distillation because of the presence of the maximum azeotrope. Formic acid can be readily removed from formic acid--water mixtures by extractive distillation in which extractive agent is a dicarboxylic acid mixed with certain high boiling organic compounds. Examples of effective agents are: itaconic acid and diethylene glycol diethyl ether; azelaic acid, heptanoic acid and 2-hydroxyacetophenone.
摘要翻译： 由于存在最大共沸物，甲酸不能通过蒸馏从甲酸和水混合物中完全除去。 通过萃取蒸馏可以从甲酸 - 水混合物中容易地除去甲酸，其中萃取剂是与某些高沸点有机化合物混合的二羧酸。 有效试剂的实例是：衣康酸和二甘醇二乙醚; 壬二酸，庚酸和2-羟基苯乙酮。
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