Closed heat-decomposing appliance, pretreatment method of sample using it, analytical method and device therefor
    1.
    发明授权
    Closed heat-decomposing appliance, pretreatment method of sample using it, analytical method and device therefor 失效
    封闭式热分解设备,样品预处理方法,分析方法及装置

    公开(公告)号:US06960477B2

    公开(公告)日:2005-11-01

    申请号:US09774641

    申请日:2001-02-01

    IPC分类号: G01N1/44 G01N1/10 B01L3/00

    摘要: Disclosed are a closed heat-decomposing appliance comprising a heating section with one side closed and other side having common ground portion, screw portion or O-ring-mounted portion and a closed introducing section that allows to connect to this heating section and common ground portion, screw portion or O-ring via O-ring-mounted portion and has cock or valve as a mechanism for closing and introducing the absorbing liquid to absorb the testing components from outside after heat-decomposition, or has packing or septum to introduce the absorbing liquid with needle pipe as well, and a pretreatment method of sample using this appliance. The purpose is to provide a closed heat-decomposing appliance for the pretreatment on accurate quantitative determination or detection of the testing components in sample, which requires no combustion assistant, which is not obstructed by ash present in sample absorbing the testing components, which requires no complicated and dangerous procedures, which can be used repeatedly, and which allows to inject the absorbing liquid after heat-decomposition, and a pretreatment method using it.

    摘要翻译: 本发明公开了一种封闭的热分解装置,其特征在于,包括:一侧封闭的加热部,另一侧具有公共接地部,螺纹部或O形环安装部,以及封闭导入部,其与上述加热部和公共接地部 螺纹部分或O形环,并且具有旋塞或阀作为关闭和引入吸收液体的机构,以在热分解后从外部吸收测试部件,或者具有包装或隔膜以引入吸收 液体用针管,以及使用该器具的样品的预处理方法。 目的是提供一种用于预处理的封闭式热分解设备,用于准确定量或检测样品中的测试组件,其不需要燃烧助剂,其不吸收样品中吸收测试组分的灰分,这不需要 复杂而危险的程序,可以重复使用,并且允许在热分解后注入吸收液体,以及使用它的预处理方法。