Analytical method of hydrocarbon compounds
    1.
    发明授权
    Analytical method of hydrocarbon compounds 失效
    烃类化合物的分析方法

    公开(公告)号:US4341634A

    公开(公告)日:1982-07-27

    申请号:US212613

    申请日:1980-12-03

    摘要: A high speed liquid chromatography to separate hydrocarbon compounds contained in a solution into three components, namely, saturates, unsaturates and aromatics, an analytical method of hydrocarbons which comprises(a) using an organic chlorine-containing type solvent or a mixed solvent of an organic chlorine-containing type solvent and a hydrocarbon type solvent as an eluent;(b) connecting the first column into which a silica type packing material is packed and the second column into which a silver-containing silica type packing material is packed in series; and(c) introducing the eluate from the second column to a detector to detect it quantitatively.

    摘要翻译: 将溶液中所含的烃化合物分离成三种组分即饱和物,不饱和化合物和芳族化合物的高速液相色谱法,烃的分析方法,其包括(a)使用有机含氯型溶剂或有机氯混合溶剂 含氯型溶剂和烃类溶剂作为洗脱剂; (b)连接填充有二氧化硅类填料的第一塔和串联包含含银二氧化硅型填料的第二塔; 和(c)将洗脱液从第二塔引入检测器以定量检测。

    Closed heat-decomposing appliance, pretreatment method of sample using it, analytical method and device therefor
    2.
    发明授权
    Closed heat-decomposing appliance, pretreatment method of sample using it, analytical method and device therefor 失效
    封闭式热分解设备,样品预处理方法,分析方法及装置

    公开(公告)号:US06960477B2

    公开(公告)日:2005-11-01

    申请号:US09774641

    申请日:2001-02-01

    IPC分类号: G01N1/44 G01N1/10 B01L3/00

    摘要: Disclosed are a closed heat-decomposing appliance comprising a heating section with one side closed and other side having common ground portion, screw portion or O-ring-mounted portion and a closed introducing section that allows to connect to this heating section and common ground portion, screw portion or O-ring via O-ring-mounted portion and has cock or valve as a mechanism for closing and introducing the absorbing liquid to absorb the testing components from outside after heat-decomposition, or has packing or septum to introduce the absorbing liquid with needle pipe as well, and a pretreatment method of sample using this appliance. The purpose is to provide a closed heat-decomposing appliance for the pretreatment on accurate quantitative determination or detection of the testing components in sample, which requires no combustion assistant, which is not obstructed by ash present in sample absorbing the testing components, which requires no complicated and dangerous procedures, which can be used repeatedly, and which allows to inject the absorbing liquid after heat-decomposition, and a pretreatment method using it.

    摘要翻译: 本发明公开了一种封闭的热分解装置,其特征在于,包括:一侧封闭的加热部,另一侧具有公共接地部,螺纹部或O形环安装部,以及封闭导入部,其与上述加热部和公共接地部 螺纹部分或O形环,并且具有旋塞或阀作为关闭和引入吸收液体的机构,以在热分解后从外部吸收测试部件,或者具有包装或隔膜以引入吸收 液体用针管,以及使用该器具的样品的预处理方法。 目的是提供一种用于预处理的封闭式热分解设备,用于准确定量或检测样品中的测试组件,其不需要燃烧助剂,其不吸收样品中吸收测试组分的灰分,这不需要 复杂而危险的程序,可以重复使用,并且允许在热分解后注入吸收液体,以及使用它的预处理方法。

    Chromatographic apparatus
    3.
    发明授权
    Chromatographic apparatus 失效
    色谱仪

    公开(公告)号:US4556538A

    公开(公告)日:1985-12-03

    申请号:US361423

    申请日:1982-03-24

    CPC分类号: G01N30/88

    摘要: The present invention relates to a chromatographic apparatus for analyzing a sample of an aqueous solution containing a plurality of micro-concentration components. In the apparatus an aqueous solution sample and an eluting solution are introduced into a separating column having a length of 20 to 90 mm, which is filled with a predetermined separating carrier and placed in a thermostatic oven which also contains a detecting cell connected to the separating column, by means of a constant flow, pulse free feeding pump.

    摘要翻译: 本发明涉及一种用于分析含有多个微量浓度组分的水溶液样品的色谱装置。 在设备中,将水溶液样品和洗脱溶液引入到长度为20至90mm的分离柱中,该分离柱填充有预定的分离载体并置于恒温箱中,该恒温炉还含有连接到分离器 柱,通过恒定流量,无脉冲进料泵。