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    Treatment of resins to lower levels of CPD-producing species and improve gelation stability
    1.
    发明授权
    Treatment of resins to lower levels of CPD-producing species and improve gelation stability 有权
    树脂处理降低生产CPD的物质水平，提高凝胶稳定性

    公开(公告)号：US07081512B2

    公开(公告)日：2006-07-25

    申请号：US10838636

    申请日：2004-05-04

    申请人： Richard J. Riehle

    发明人： Richard J. Riehle

    IPC分类号： C08F6/00

    CPC分类号： D21H17/55 ,  C08G73/0286 ,  D21H21/20

    摘要： A process for treating a composition containing a polyamine-epihalohydrin resin that has a low level of CPD-producing species and good gelation stability is disclosed. A polyamine-epihalohydrin resin is prepared with a ratio of epihalohydrin:amine of less than about 1.1:1.0; The resin is then subjected to a base treatment followed by an acid treatment resulting in a resin that has good gelation storage stability and produces low levels of CPD.

    摘要翻译： 公开了一种处理含有具有低水平的CPD生产物质和良好凝胶稳定性的多胺 - 表卤醇树脂的组合物的方法。 制备表面卤代醇：胺的比例小于约1.1:1.0的多胺 - 表卤醇树脂; 然后对树脂进行碱处理，然后进行酸处理，得到具有良好凝胶化储存稳定性并产生低水平CPD的树脂。

    Quaternary vinylamine-containing polymers as additives in papermaking
    4.
    发明授权
    Quaternary vinylamine-containing polymers as additives in papermaking 有权
    第四纪含乙烯基胺的聚合物作为造纸中的添加剂

    公开(公告)号：US08518215B2

    公开(公告)日：2013-08-27

    申请号：US12696237

    申请日：2010-01-29

    申请人： Jonathan M. McKay ,  Qu-Ming Gu ,  Richard J. Riehle

    发明人： Jonathan M. McKay ,  Qu-Ming Gu ,  Richard J. Riehle

    IPC分类号： D21H17/33 ,  D21H17/44 ,  D21H21/10 ,  D21H21/18 ,  D21H23/04

    CPC分类号： C08F226/02 ,  C08F8/44 ,  D21H17/46 ,  D21H19/24

    摘要： Vinylamine-containing polymers are disclosed where the amine groups are substituted with cationic functional groups. Processes for preparing such polymers, as well as compositions comprising such polymers are also disclosed. Among other applications, these polymers can be used in papermaking applications as dry strength additives, wet strength additives, retention aids, drainage aids, and pitch and stickies control agents.

    摘要翻译： 公开了含胺基的聚合物，其中胺基被阳离子官能团取代。 还公开了制备这种聚合物的方法，以及包含这种聚合物的组合物。 除了其它应用之外，这些聚合物可用于造纸应用中，作为干强度添加剂，湿强度添加剂，助留剂，引流助剂以及沥青和粘合剂控制剂。

    Quaternary Vinylamine-Containing Polymers as Additives in Papermaking
    5.
    发明申请
    Quaternary Vinylamine-Containing Polymers as Additives in Papermaking 有权
    第四纪含乙烯胺的聚合物作为造纸中的添加剂

    公开(公告)号：US20100193148A1

    公开(公告)日：2010-08-05

    申请号：US12696237

    申请日：2010-01-29

    申请人： Jonathan M. McKay ,  Qu-Ming Gu ,  Richard J. Riehle

    发明人： Jonathan M. McKay ,  Qu-Ming Gu ,  Richard J. Riehle

    IPC分类号： D21H23/04 ,  C08G73/00

    CPC分类号： C08F226/02 ,  C08F8/44 ,  D21H17/46 ,  D21H19/24

    摘要： Vinylamine-containing polymers are disclosed where the amine groups are substituted with cationic functional groups. Processes for preparing such polymers, as well as compositions comprising such polymers are also disclosed. Among other applications, these polymers can be used in papermaking applications as dry strength additives, wet strength additives, retention aids, drainage aids, and pitch and stickies control agents.

    摘要翻译： 公开了含胺基的聚合物，其中胺基被阳离子官能团取代。 还公开了制备这种聚合物的方法，以及包含这种聚合物的组合物。 除了其它应用之外，这些聚合物可用于造纸应用中，作为干强度添加剂，湿强度添加剂，助留剂，引流助剂以及沥青和粘合剂控制剂。

    MEMBRANE SEPARATION PROCESS FOR REMOVING RESIDUALS FROM POLYAMINE-EPIHALOHYDRIN RESINS
    6.
    发明申请
    MEMBRANE SEPARATION PROCESS FOR REMOVING RESIDUALS FROM POLYAMINE-EPIHALOHYDRIN RESINS 有权
    用于从聚氨基甲酸乙烯酯树脂中除去残留物的膜分离方法

    公开(公告)号：US20080066881A1

    公开(公告)日：2008-03-20

    申请号：US11856224

    申请日：2007-09-17

    申请人： Richard J. Riehle ,  Stephen Vinciguerra

    发明人： Richard J. Riehle ,  Stephen Vinciguerra

    IPC分类号： D21H17/33

    CPC分类号： D21H17/56 ,  C08G73/022 ,  C08G73/0286 ,  C09J179/02 ,  D21H21/146 ,  D21H21/18 ,  D21H21/20

    摘要： This invention relates to a process for preparing polyamine-epihalohydrin resins having reduced levels of residuals. The process comprises (a) charging a membrane separation apparatus with an aqueous composition comprising at least one polyamine-epihalohydrin resin, and (b) separating the aqueous composition into a permeate and a retentate by passing the aqueous composition through the membrane of the membrane separation apparatus. The retentate comprises at least one polyamine-epihalohydrin resin having lower levels of residuals on an equal active component basis than the aqueous composition of (a). The permeate comprises residuals removed from the aqueous composition of (a) and less than 5% by weight of the active component of said at least one polyamine-epihalohydrin resin. The polyamine-epihalohydrin resins having reduced levels of residuals can be used to make wet strength agents, dry strength agents, creping adhesives for paper products, curing agents for wood product adhesives, and other products.

    摘要翻译： 本发明涉及一种制备具有降低残留水平的多胺 - 表卤代醇树脂的方法。 该方法包括：（a）用包含至少一种多胺 - 表卤醇树脂的水性组合物对膜分离装置进行充填，和（b）通过使含水组合物通过膜分离膜将水性组合物分离成渗透物和渗余物 仪器。 所述保留物包含至少一种与（a）的水性组合物相同的活性成分基础上具有较低残留水平的多胺 - 表卤醇树脂。 渗透物包含从（a）的水性组合物中除去的残余物和小于所述至少一种多胺 - 表卤代醇树脂的活性组分的5重量％。 具有降低残留水平的多胺 - 表卤醇树脂可用于制备湿强度剂，干强度剂，纸产品起皱粘合剂，木制品粘合剂用固化剂和其它产品。

    Alkaline paper surface sizing agents, method of use and surface sized paper
    7.
    发明授权
    Alkaline paper surface sizing agents, method of use and surface sized paper 有权
    碱性纸表面施胶剂，使用方法和表面尺寸纸

    公开(公告)号：US06325893B1

    公开(公告)日：2001-12-04

    申请号：US09436342

    申请日：1999-11-08

    申请人： Clement L. Brungardt ,  Richard J. Riehle ,  Jian Jian Zhang

    发明人： Clement L. Brungardt ,  Richard J. Riehle ,  Jian Jian Zhang

    IPC分类号： D21H1717

    摘要： A sizing agent for paper that is a 2-oxetanone ketene multimer which is not solid at 35° C., particularly a multimer mixture in which at least 25 weight percent of the hydrocarbon substituents contain irregularities such as branched alkyl groups or linear or branched alkenyl groups. Paper surface sized with the 2-oxetanone ketene multimer sizing agent and the method of surface sizing paper are also disclosed.

    摘要翻译： 一种作为在35℃下不固体的2-氧杂环丁酮乙烯酮多聚体的纸浆剂，特别是其中至少25重量％的烃取代基含有不规则性的多聚体混合物，例如支链烷基或直链或支链烯基 。 还公开了用2-氧杂环丁酮乙烯酮多聚体施胶剂和表面施胶纸的方法的纸张表面

    Poly(aminoamideureylene) resin, its synthesis, and its use in paper and paperboard manufacture
    9.
    依法登记的发明
    Poly(aminoamideureylene) resin, its synthesis, and its use in paper and paperboard manufacture 失效
    聚（氨基酰亚胺）树脂，其合成及其在纸和纸板制造中的应用

    公开(公告)号：USH1629H

    公开(公告)日：1997-01-07

    申请号：US375063

    申请日：1995-01-19

    申请人： Richard J. Riehle ,  Ronald R. Staib

    发明人： Richard J. Riehle ,  Ronald R. Staib

    IPC分类号： C08G69/48 ,  C08G73/02 ,  D21H17/54 ,  D21H21/20 ,  C08F283/04

    CPC分类号： C08G73/0226 ,  C08G69/48 ,  C08G73/0293 ,  D21H17/54 ,  D21H21/20

    摘要： The invention provides a novel poly(aminoamideureylene) resin and a process for making the resin without epichlorohydrin. The resin useful for improving wet strength of paper and paperboard intermediates. The resin is formed by making a prepolymer by reacting a diaminoamine, a dicarboxylic acid, and urea, allylating the prepolymer, and then reacting with hypohalous acid to produce an allylated quaternized poly(aminoamideureylene) having halohydrin substituents with resort to using epichlorohydrin. The resin can be activated for use in a papermaking process by treatment with a caustic (alkaline) agent. Optionally, the resin can be cross-linked prior to activation by heating in the presence of a caustic agent.The invention also provides an improvement in making polymers having halohydrin substituents formed by reacting an allylated polymer with hypohalous acid wherein the reaction is conducted without control of the pH.This invention also provides a method for producing hypohalous acid by acidifying an aqueous solution of an alkali metal hypohalite.

    摘要翻译： 本发明提供了一种新的聚（氨基酰胺亚乙基）树脂和一种制备没有表氯醇的树脂的方法。 该树脂可用于提高纸张和纸板中间体的湿强度。 树脂通过使二氨基胺，二羧酸和脲反应制备预聚物，使预聚物烯丙化，然后与次卤酸反应，产生具有卤代醇取代基的烯丙基季铵化聚（氨基酰胺），并使用表氯醇。 树脂可以通过用苛性碱（碱）剂处理而被活化用于造纸过程。 任选地，树脂可以在通过在苛性剂的存在下加热而活化之前进行交联。 本发明还提供了制备具有通过使烯丙基化聚合物与次卤酸反应形成的卤代醇取代基的聚合物的改进，其中反应进行而不控制pH。 本发明还提供了通过酸化碱金属次卤酸盐的水溶液来生产次卤酸的方法。

    Membrane separation process for removing residuals from polyamine-epihalohydrin resins
    10.
    发明授权
    Membrane separation process for removing residuals from polyamine-epihalohydrin resins 有权
    用于除去多胺 - 表卤醇树脂残留物的膜分离方法

    公开(公告)号：US08101710B2

    公开(公告)日：2012-01-24

    申请号：US13093527

    申请日：2011-04-25

    申请人： Richard J. Riehle ,  Stephen Vinciguerra

    发明人： Richard J. Riehle ,  Stephen Vinciguerra

    IPC分类号： C08F6/00 ,  C08J3/00

    CPC分类号： D21H17/56 ,  C08G73/022 ,  C08G73/0286 ,  C09J179/02 ,  D21H21/146 ,  D21H21/18 ,  D21H21/20

    摘要： This invention relates to a process for preparing polyamine-epihalohydrin resins having reduced levels of residuals. The process comprises (a) charging a membrane separation apparatus with an aqueous composition comprising at least one polyamine-epihalohydrin resin, and (b) separating the aqueous composition into a permeate and a retentate by passing the aqueous composition through the membrane of the membrane separation apparatus. The retentate comprises at least one polyamine-epihalohydrin resin having lower levels of residuals on an equal active component basis than the aqueous composition of (a). The permeate comprises residuals removed from the aqueous composition of (a) and less than 5% by weight of the active component of said at least one polyamine-epihalohydrin resin. The polyamine-epihalohydrin resins having reduced levels of residuals can be used to make wet strength agents, dry strength agents, creping adhesives for paper products, curing agents for wood product adhesives, and other products.

    摘要翻译： 本发明涉及一种制备具有降低残留水平的多胺 - 表卤代醇树脂的方法。 该方法包括：（a）用包含至少一种多胺 - 表卤醇树脂的水性组合物对膜分离装置进行充填，和（b）通过使含水组合物通过膜分离膜将水性组合物分离成渗透物和渗余物 仪器。 所述保留物包含至少一种与（a）的水性组合物相同的活性成分基础上具有较低残留水平的多胺 - 表卤醇树脂。 渗透物包含从（a）的水性组合物中除去的残余物和小于所述至少一种多胺 - 表卤代醇树脂的活性组分的5重量％。 具有降低残留水平的多胺 - 表卤醇树脂可用于制备湿强度剂，干强度剂，纸产品起皱粘合剂，木制品粘合剂用固化剂和其它产品。