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1.发明授权Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime 有权在湍流状态下，使用连续的产物萃取法在微反应器和磨粒反应器中形成硝酸酯公开(公告)号：US08536366B2
公开(公告)日：2013-09-17
申请号：US12808829
申请日：2008-12-19
申请人： Sascha Braune , Stefan Steinhofer , Peter Poechlauer , Rafael Wilhelmus E. G. Reintjens , Nicole Theodora W. Linssen , Mehul Thathagar
发明人： Sascha Braune , Stefan Steinhofer , Peter Poechlauer , Rafael Wilhelmus E. G. Reintjens , Nicole Theodora W. Linssen , Mehul Thathagar
IPC分类号： C07C201/02 , C07C201/16 , B01J14/00 , B01D11/04
CPC分类号： B01J19/0093 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00966 , B01J2219/00984 , C07C201/02 , C07C203/04
摘要： A process for the continuous production of a compound of Formula (II), HO—R1—ONO2 (II) wherein R1 is a straight chain alkyl radical having from 3 to 6 carbon atoms, in a two-phase solvent system, comprising contacting a compound of Formula (I), HO—R1—OH (I) wherein R1 is as defined above, with nitric acid in the presence of a first solvent, wherein the compound of Formula (II) is continuously extracted into a second solvent, and the reaction is carried out in a mixing microreactor which provides a power loss of at least 1.3 times the power loss provided under identical conditions by a circular cross-section straight-channel microreactor having an internal diameter equal to the average hydraulic diameter of the mixing microreactor and a length equal to the length of the mixing microreactor.
摘要翻译： 在二相溶剂系统中连续制备其中R 1为具有3至6个碳原子的直链烷基的式（II）化合物HO-R1-ONO2（Ⅱ）的方法，包括使 式（I）化合物，其中R 1如上定义的HO-R 1 -OH（I）与硝酸在第一溶剂存在下反应，其中将式（II）化合物连续萃取到第二溶剂中， 反应在混合微反应器中进行，该混合微反应器通过圆形截面直通微反应器提供至少1.3相同条件下功率损耗的功率损失，该反应器的内径等于混合微反应器的平均水力直径 长度等于混合微反应器的长度。
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2.发明申请公开(公告)号：US20100152479A1
公开(公告)日：2010-06-17
申请号：US12600513
申请日：2008-05-28
IPC分类号： B01J19/00 , C07C41/02 , C07B41/00 , C07C67/00 , C07C17/013
CPC分类号： B01J19/0093
摘要： A tube bundle falling film microreactor for performing gas-liquid reactions, which has: a) at least one vertical tube with b) a device for distributing the liquid on the inside of the tube and c) a liquid collecting system, and d) a device for gas supply and removal, and use thereof.
摘要翻译： 一种用于进行气液反应的管束降膜微反应器，其具有：a）至少一个垂直管，其具有b）用于在所述管内部分配液体的装置，以及c）液体收集系统，以及d） 气体供应和清除装置及其用途。
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3.发明授权公开(公告)号：US08221708B2
公开(公告)日：2012-07-17
申请号：US12600513
申请日：2008-05-29
IPC分类号： B01J10/02
CPC分类号： B01J19/0093
摘要： A tube bundle falling film microreactor for performing gas-liquid reactions, which has: a) at least one vertical tube with b) a device for distributing the liquid on the inside of the tube and c) a liquid collecting system, and d) a device for gas supply and removal, and use thereof.
摘要翻译： 一种用于进行气液反应的管束降膜微反应器，其具有：a）至少一个垂直管，其具有b）用于在所述管内部分配液体的装置，以及c）液体收集系统，以及d） 气体供应和清除装置及其用途。
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4.发明申请FORMATION OF NITRATE ESTERS IN MICROREACTORS AND MILLIREACTORS USING A CONTINUOUS PRODUCT EXTRACTION IN A TURBULENT FLOW REGIME 有权在湍流流程中使用连续产物萃取在微生物和乳清液中形成硝酸酯公开(公告)号：US20110034720A1
公开(公告)日：2011-02-10
申请号：US12808829
申请日：2008-12-19
申请人： Sascha Braune , Stefan Steinhofer , Peter Poechlauer , Rafael Wilhelmus E.G. Reintjens , Nicole Theodora W. Linssen , Mehul Thathagar
发明人： Sascha Braune , Stefan Steinhofer , Peter Poechlauer , Rafael Wilhelmus E.G. Reintjens , Nicole Theodora W. Linssen , Mehul Thathagar
IPC分类号： C07C201/02
CPC分类号： B01J19/0093 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00966 , B01J2219/00984 , C07C201/02 , C07C203/04
摘要： A process for the continuous production of a compound of Formula (II), HO—R1—ONO2 (II) wherein R1 is a straight chain alkyl radical having from 3 to 6 carbon atoms, in a two-phase solvent system, comprising contacting a compound of Formula (I), HO—R1—OH (I) wherein R1 is as defined above, with nitric acid in the presence of a first solvent, wherein the compound of Formula (II) is continuously extracted into a second solvent, and the reaction is carried out in a mixing microreactor which provides a power loss of at least 1.3 times the power loss provided under identical conditions by a circular cross-section straight-channel microreactor having an internal diameter equal to the average hydraulic diameter of the mixing microreactor and a length equal to the length of the mixing microreactor.
摘要翻译： 在二相溶剂系统中连续制备其中R 1为具有3至6个碳原子的直链烷基的式（II）化合物HO-R1-ONO2（Ⅱ）的方法，包括使 式（I）化合物，其中R 1如上定义的HO-R 1 -OH（I）与硝酸在第一溶剂存在下反应，其中将式（II）化合物连续萃取到第二溶剂中， 反应在混合微反应器中进行，该混合微反应器通过圆形截面直通微反应器提供至少1.3相同条件下功率损耗的功率损失，该反应器的内径等于混合微反应器的平均水力直径 长度等于混合微反应器的长度。
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5.发明申请REACTION PLATES WITH ALTERNATIVE, UNORDERED MICROSTRUCTURED SURFACES FOR MICROREACTORS FOR PERFORMING GAS-LIQUID REACTIONS 审中-公开具有替代性，不相关的微结构表面的反应板用于执行气液反应的微粒体公开(公告)号：US20100130787A1
公开(公告)日：2010-05-27
申请号：US12532220
申请日：2008-03-18
申请人： Sascha Braune , Stefan Steinhofer
发明人： Sascha Braune , Stefan Steinhofer
IPC分类号： B01J19/00 , B01J10/02 , B01J7/02 , C07C45/33 , C07C209/00
CPC分类号： B01J19/0093 , B01J2219/00783 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/0086 , B01J2219/00873
摘要： Reaction plates for microreactors for performing gas-liquid reactions, which consist of falling-film plates with a surface which has a randomly distributed, unordered fine structure or microstructure.
摘要翻译： 用于进行气 - 液反应的微反应器的反应板，其由具有随机分布的无序精细结构或微观结构的表面的落膜板组成。
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