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    Process for the production of chemical compounds from carbon dioxide
    1.
    发明授权
    Process for the production of chemical compounds from carbon dioxide 有权
    从二氧化碳生产化学化合物的方法

    公开(公告)号：US09273020B2

    公开(公告)日：2016-03-01

    申请号：US14394508

    申请日：2013-04-11

    申请人： Haldor Topsøe A/S

    发明人： Niels Christian Schjødt ,  John Bøgild Hansen ,  Claus Friis Pedersen

    IPC分类号： C07D305/00 ,  C07C69/96 ,  C07C51/14 ,  C07D305/12 ,  C07C67/38 ,  C07C68/00 ,  C07C201/02 ,  C07D301/04 ,  C25B1/02 ,  C25B15/08 ,  C25B1/00 ,  C07C67/035 ,  C07C68/04

    CPC分类号： C07D305/12 ,  C07C51/14 ,  C07C67/035 ,  C07C67/38 ,  C07C68/005 ,  C07C68/04 ,  C07C201/02 ,  C07D301/04 ,  C25B1/00 ,  C25B1/02 ,  C25B15/08 ,  Y02E60/366 ,  Y02P20/133 ,  Y02P20/134 ,  Y02P20/582 ,  C07C203/04 ,  C07C69/96 ,  C07C53/124 ,  C07C69/24

    摘要： Process for the production of a chemical compound from a carbon dioxide starting material, comprising the steps of a) providing a feed stream consisting mainly of carbon dioxide; b) electrolyzing in an electrolysis stage the carbon dioxide in the feed stream to a first gas stream containing carbon monoxide and a second gas stream containing oxygen, wherein the molar ratio between carbon monoxide and oxygen is about 1:0.5 in an electrolysis stage; c) adjusting the composition of the first gas stream or the second gas stream or both gas streams to include carbon dioxide, either by operating at less than full conversion of CO2 or by sweeping one or both gas streams with a gas containing CO2 or by at some stage between the electrolysis cell and the oxidative carbonylation reactor diluting one or both gas streams with a gas containing CO2; all while maintaining an overall molar ratio of carbon monoxide to oxygen of about 1:0.5; and d) introducing the first and second process stream into a reaction stage and reacting the first and second process stream combined or in succession with a substrate to the chemical compound by means of an oxidative carbonylation reaction with the carbon monoxide and oxygen contained in the process feed stream.

    摘要翻译： 用于从二氧化碳原料生产化合物的方法，包括以下步骤：a）提供主要由二氧化碳组成的进料流; b）在电解阶段中将进料流中的二氧化碳电解成含有一氧化碳和含有氧的第二气流的第一气流，其中在电解阶段一氧化碳和氧之间的摩尔比为约1:0.5; c）调节第一气流或第二气流或两种气流的组成以包括二氧化碳，或者通过以少于二氧化碳的全部转化率进行操作，或者通过用含有CO 2的气体或通过在 在电解池和氧化羰基化反应器之间的某个阶段，用含CO 2的气体稀释一种或两种气流; 同时保持一氧化碳与氧的总摩尔比为约1:0.5; 和d）将第一和第二工艺流引入反应阶段，并通过与该方法中所含的一氧化碳和氧气进行氧化羰基化反应，将第一和第二工艺流与底物组合或连续地与化学化合物反应 饲料流。

    PROCESS FOR THE PRODUCTION OF CHEMICAL COMPOUNDS FROM CARBON DIOXIDE
    2.
    发明申请
    PROCESS FOR THE PRODUCTION OF CHEMICAL COMPOUNDS FROM CARBON DIOXIDE 有权
    从二氧化碳生产化学化合物的方法

    公开(公告)号：US20150057458A1

    公开(公告)日：2015-02-26

    申请号：US14394508

    申请日：2013-04-11

    申请人： Haldor Topsøe A/S

    发明人： Niels Christian Schjødt ,  John Bøgild Hansen ,  Claus Friis Pedersen

    IPC分类号： C07D305/12 ,  C25B1/02 ,  C25B1/00 ,  C07C68/04 ,  C07C67/035

    CPC分类号： C07D305/12 ,  C07C51/14 ,  C07C67/035 ,  C07C67/38 ,  C07C68/005 ,  C07C68/04 ,  C07C201/02 ,  C07D301/04 ,  C25B1/00 ,  C25B1/02 ,  C25B15/08 ,  Y02E60/366 ,  Y02P20/133 ,  Y02P20/134 ,  Y02P20/582 ,  C07C203/04 ,  C07C69/96 ,  C07C53/124 ,  C07C69/24

    摘要： Process for the production of a chemical compound from a carbon dioxide starting material, comprising the steps of a) providing a feed stream consisting mainly of carbon dioxide; b) electrolysing in an electrolysis stage the carbon dioxide in the feed stream to a first gas stream containing carbon monoxide and a second gas stream containing oxygen, wherein the molar ratio between carbon monoxide and oxygen is about 1:0.5 in an electrolysis stage; c) adjusting the composition of the first gas stream or the second gas stream or both gas streams to include carbon dioxide, either by operating at less than full conversion of CO2 or by sweeping one or both gas streams with a gas containing CO2 or by at some stage between the electrolysis cell and the oxidative carbonylation reactor diluting one or both gas streams with a gas containing CO2; all while maintaining an overall molar ratio of carbon monoxide to oxygen of about 1:0.5; and d) introducing the first and second process stream into a reaction stage and reacting the first and second process stream combined or in succession with a substrate to the chemical compound by means of an oxidative carbonylation reaction with the carbon monoxide and oxygen contained in the process feed stream.

    摘要翻译： 用于从二氧化碳原料生产化合物的方法，包括以下步骤：a）提供主要由二氧化碳组成的进料流; b）在电解阶段将电解中的二氧化碳电解成含有一氧化碳和含有氧的第二气流的第一气流，其中一氧化碳与氧之间的摩尔比在电解阶段为约1:0.5; c）调节第一气流或第二气流或两种气流的组成以包括二氧化碳，或者通过以少于二氧化碳的全部转化率进行操作，或者通过用含有CO 2的气体或通过在 在电解池和氧化羰基化反应器之间的某个阶段，用含CO 2的气体稀释一种或两种气流; 同时保持一氧化碳与氧的总摩尔比为约1:0.5; 和d）将第一和第二工艺流引入反应阶段，并通过与该方法中所含的一氧化碳和氧气进行氧化羰基化反应，将第一和第二工艺流与底物组合或连续地与化学化合物反应 饲料流。

    PROCESS FOR PREPARING 4-NITRO-OXY-METHYL-BENZOIC ACID
    4.
    发明申请
    PROCESS FOR PREPARING 4-NITRO-OXY-METHYL-BENZOIC ACID 审中-公开
    制备4-硝基 - 甲基苯甲酸的方法

    公开(公告)号：US20130131378A1

    公开(公告)日：2013-05-23

    申请号：US13509906

    申请日：2010-11-15

    申请人： Luis Anglada ,  Albert Palomer ,  Luis Sobral

    发明人： Luis Anglada ,  Albert Palomer ,  Luis Sobral

    IPC分类号： C07C51/347

    CPC分类号： C07C51/347 ,  C07C201/02 ,  C07C203/04

    摘要： This invention relates to a new process for preparing 4-nitro-oxy-methyl-benzoic acid, comprising the following steps: a) reaction of 4-chloromethyl-benzoic acid with silver nitrate and in the presence of an acid as a catalyst in acetonitrile at reflux temperature, followed by cooling and adding of a polar aprotic solvent; b) separation of the silver salts by filtration, followed by washout with a polar aprotic solvent; c) precipitation of the 4-nitro-oxy-methyl-benzoic acid with water from the filtrate obtained in step b); and d) drying of the 4-nitro-oxy-methyl-benzoic acid.

    摘要翻译： 本发明涉及一种制备4-硝基 - 氧 - 甲基 - 苯甲酸的新方法，包括以下步骤：a）4-氯甲基 - 苯甲酸与硝酸银的反应，并在乙酸存在下作为催化剂在乙腈 在回流温度下，然后冷却并加入极性非质子溶剂; b）通过过滤分离银盐，然后用极性非质子溶剂洗涤; c）从步骤b）中获得的滤液中用水沉淀4-硝基 - 氧 - 甲基 - 苯甲酸; 和d）4-硝基 - 氧 - 甲基 - 苯甲酸的干燥。

    Process for the preparation of naproxene nitroxyalkylesters
    8.
    发明申请
    Process for the preparation of naproxene nitroxyalkylesters 有权
    制备萘普生硝基烷基酯的方法

    公开(公告)号：US20050119339A1

    公开(公告)日：2005-06-02

    申请号：US10625558

    申请日：2003-07-24

    申请人： Francesca Benedini ,  Erminio Oldani ,  Graziano Castaldi ,  Antonio Tarquini

    发明人： Francesca Benedini ,  Erminio Oldani ,  Graziano Castaldi ,  Antonio Tarquini

    IPC分类号： C07C201/02 ,  C07B53/00 ,  C07B61/00 ,  C07C203/04 ,  A61K31/21

    CPC分类号： C07C201/02 ,  C07C203/04

    摘要： A process for obtaining nitroxyalklesters of the 2(S)(6-methoxy-2-naphthyl)-propanoic acid having an enantiomeric excess higher than or equal to 95%, preferably higher than or equal to 98%, characterized in that an halide of the 2-(S)-(6 methoxy-2-naphthyl)propanoic acid of formula A-Hal, wherein A is the acid acyl residue, is reacted in an inert orgariic solvent with an aliphatic nitroxyalkanol HO—Y—ONO2, wherein Y is a C2-C20 alkylene or a cycloalkylene from 3 to 8 carbon atoms, or an alkylene as defined containing a cycloalkylene as defined, in the presence of an inorganic base.

    摘要翻译： 一种获得具有高于或等于95％，优选高于或等于98％的对映异构体过量的2（S）（6-甲氧基-2-萘基） - 丙酸的硝基螺旋体的方法，其特征在于， 其中A是酸酰基残基的式A-Hal的2-（S） - （6-甲氧基-2-萘基）丙酸在惰性溶剂中与脂族硝基链烷醇HO-Y-ONO 2，其中Y是C 2 -C 20亚烷基或3至8个碳原子的亚环烷基，或如所定义的含有如所定义的亚环烷基的亚烷基 在无机碱存在下进行。

    Co-nitration of trimethylolethane and triethylene glycol
    10.
    发明授权
    Co-nitration of trimethylolethane and triethylene glycol 失效
    三羟甲基乙烷和三甘醇的共同硝化

    公开(公告)号：US5454891A

    公开(公告)日：1995-10-03

    申请号：US275411

    申请日：1994-07-15

    申请人： Scott B. Preston

    发明人： Scott B. Preston

    IPC分类号： C06B25/10 ,  C07C203/04 ,  D03D23/00

    CPC分类号： C06B25/10 ,  C07C201/02

    摘要： Disclosed is a process for preparing an energetic mixture of trimethylolethane trinitrate and triethylene glycol dinitrate by forming a polyol mixture of trimethylolethane, triethylene glycol and water and then nitrating the polyol mixture with a mixture of nitric and sulfuric acids.

    摘要翻译： 公开了通过形成三羟甲基乙烷，三甘醇和水的多元醇混合物，然后用硝酸和硫酸的混合物硝化多元醇混合物来制备三羟甲基乙烷三硝酸三羟甲基乙烷和三乙二醇二硝酸酯的高能混合物的方法。