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公开(公告)号：US4294953A
公开(公告)日：1981-10-13
申请号：US044040
申请日：1979-05-31
申请人： Clayton B. Quinn , William Hilakos
发明人： Clayton B. Quinn , William Hilakos
CPC分类号： C08G64/14
摘要： A process for preparing a thermoplastic, randomly branched aromatic polycarbonate is disclosed which comprises reacting a carbonate precursor, a dihydric phenol, and a dianhydride branching agent and maintaining the resultant reaction medium at a pH of from about 9 to about 12 to thereby produce a thermoplastic randomly branched aromatic polycarbonate.
摘要翻译： 公开了一种制备热塑性无规支化芳族聚碳酸酯的方法，其包括使碳酸酯前体，二元酚和二酐支化剂反应，并将所得反应介质保持在约9至约12的pH，从而制备热塑性 无规分支的芳族聚碳酸酯。
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2.发明授权Method for converting cyclic polycarbonate oligomer mixtures to linear polycarbonate, and composition resulting therefrom 失效将环状聚碳酸酯低聚物混合物转化为线性聚碳酸酯的方法，以及由其制得的组合物
公开(公告)号：US4740583A
公开(公告)日：1988-04-26
申请号：US888673
申请日：1986-07-24
申请人： Daniel J. Brunelle , Thomas L. Evans , Michael A. Vallance , Kevin R. Stewart , Thomas G. Shannon , David A. Williams , Dwight J. Patterson , Niles R. Rosenquist , William Hilakos
发明人： Daniel J. Brunelle , Thomas L. Evans , Michael A. Vallance , Kevin R. Stewart , Thomas G. Shannon , David A. Williams , Dwight J. Patterson , Niles R. Rosenquist , William Hilakos
摘要： Cyclic polycarbonate (or thiol analog) oligomer mixtures are prepared by the reaction of bishaloformates or their thio analogs, or mixtures thereof with dihydroxy or dimercapto compounds, with alkali metal hydroxides and various amines. The oligomer mixtures may be converted to polycarbonates or their thiol analogs by a method which is particularly adaptable to integration with polycarbonate processing operations. Polymerization may be conducted simultaneously with molding, extrusion and the like. The oligomer mixtures are adaptable to the preparation of filled prepregs.
摘要翻译： 通过双卤代甲酸酯或其硫代类似物或其与二羟基或二巯基化合物的混合物与碱金属氢氧化物和各种胺的反应制备环状聚碳酸酯（或硫醇类似物）低聚物混合物。 低聚物混合物可以通过特别适用于与聚碳酸酯加工操作整合的方法转化为聚碳酸酯或其硫醇类似物。 聚合可以与成型，挤出等同时进行。 低聚物混合物适用于填充的预浸料的制备。
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公开(公告)号：US4728387A
公开(公告)日：1988-03-01
申请号：US941653
申请日：1986-12-15
申请人： William Hilakos
发明人： William Hilakos
CPC分类号： D07B7/145 , B29B15/122 , B29C70/52 , Y10T156/1727 , Y10T156/1732
摘要： An embodiment assembly for the impregnation of a continuous length of fibers comprises a convex surface and a non-convex surface over which the length of fibers is drawn under tension. The pressure of impingement on the surfaces alternately separates and consolidates the fibers in sequence during their impregnation with the resin, to obtain a complete and homogeneous impregnation.
摘要翻译： 用于浸渍连续长度的纤维的实施方案组件包括凸形表面和非凸形表面，在该表面上纤维的长度在其下拉伸。 表面上的冲击压力在树脂浸渍期间交替分离和固结纤维，以获得完全均匀的浸渍。
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公开(公告)号：US4621132A
公开(公告)日：1986-11-04
申请号：US625260
申请日：1984-06-27
申请人： Clayton B. Quinn , William Hilakos
发明人： Clayton B. Quinn , William Hilakos
IPC分类号： C08G63/64
CPC分类号： C08G63/64
摘要： Thermoplastic randomly branched copolyester-carbonate resin containing from about 40 mole percent to about 90 mole percent ester bonds which is particularly suited for blow molding operations. This branched copolyester-carbonate resin is obtained by reacting a carbonate precursor, at least one dihydric phenol, at least one ester forming reactive derivative of a difunctional carboxylic acid, and a polyfunctional aromatic branching agent.
摘要翻译： 含有约40摩尔％至约90摩尔％酯键的热塑性无规分支共聚酯 - 碳酸酯树脂，其特别适用于吹塑操作。 该支化的共聚酯 - 碳酸酯树脂通过使碳酸酯前体，至少一种二元酚，至少一种双官能羧酸的酯形成反应性衍生物和多官能芳族支化剂反应而得到。
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5.发明授权Poltrusion apparatus and method for impregnating continuous lengths of multi-filament and multi-fiber structures 失效用于浸渍连续长度的多丝和多纤维结构的聚合装置和方法
公开(公告)号：US4939002A
公开(公告)日：1990-07-03
申请号：US133417
申请日：1987-12-15
申请人： William Hilakos
发明人： William Hilakos
CPC分类号： B29B15/122 , B29C70/521 , Y10S118/18
摘要： Apparatus and method for the impregnation of a continuous length of multifilament or multifiber yarns with a molten thermoplastic polymeric resin includes a member for spreading the multifilaments or multifibers apart during their immersion in a bath of the molten resin. The shape, configuration and location of the member facilitates the homogeneous impregnation, particularly with highly viscous melts, to produce a uniform and thorough encapsulation of the filaments or fibers.
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6.发明授权Apparatus and method for impregnating continuous lengths of multifilament and multi-fiber structures 失效用于浸渍连续长度的复丝和多纤维结构的装置和方法
公开(公告)号：US4864964A
公开(公告)日：1989-09-12
申请号：US133418
申请日：1987-12-15
申请人： William Hilakos
发明人： William Hilakos
CPC分类号： B29C70/521 , B29B15/122
摘要： Apparatus for the impregnation of a continuous length of multifilament or multifiber yarns with a molten thermoplastic polymeric resin includes a pair of convex/concave (mating) surfaces for spreading the multifilaments or multifibers apart during their immersion in a bath of the molten resin. The shape, configuration and location of the surfaces facilitates homogeneous impregnation, particularly with highly viscous metls, to produce a uniform and thorough encapsulation of the filaments or fibers.
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7.发明授权Pultrusion apparatus and method for impregnating continuous lengths of multi-filament and multi-fiber structures 失效用于浸渍连续长度的多丝和多纤维结构的拉挤成型设备和方法
公开(公告)号：US4907527A
公开(公告)日：1990-03-13
申请号：US133419
申请日：1987-12-15
CPC分类号： C08G64/30 , B29C70/521
摘要： Apparatus and method for the pultrusion of polymeric resins reinforced with continuous lengths of multifilaments and/or fibers comprises wetting the lengths of multifilaments and/or fibers with a polymerization initiator, passing the wet length through an impregnating bath of a resin prepolymer and activating the polymerization in-situ.
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公开(公告)号：US4240968A
公开(公告)日：1980-12-23
申请号：US33392
申请日：1979-04-26
IPC分类号： C07D311/58 , C08G64/06 , C07D311/04
CPC分类号： C08G64/06 , C07D311/58
摘要： A process is disclosed for isolating and purifying diphenol by-products to obtain an enriched chroman-I concentrate. The process includes slurrying a mixture of diphenol by-products in a suitable solvent system to form a solid, and then recovering, washing and drying the collected solid.
摘要翻译： 公开了用于分离和纯化二酚副产物以获得富集的色满-1浓缩物的方法。 该方法包括将二酚副产物的混合物在合适的溶剂体系中制浆以形成固体，然后回收，洗涤和干燥所收集的固体。
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公开(公告)号：US4778367A
公开(公告)日：1988-10-18
申请号：US133404
申请日：1987-12-15
申请人： William Hilakos
发明人： William Hilakos
CPC分类号： B29C70/526
摘要： A sizing and/or forming die is employed in the pultrusion of filament or fiber reinforced thermoplastic resins such as polycarbonates. The die is adjustable on-line to change the ratio of resin to reinforcement at will and without interrupting the production process.
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公开(公告)号：US4465820A
公开(公告)日：1984-08-14
申请号：US500846
申请日：1983-06-03
申请人： Kenneth F. Miller , William Hilakos
发明人： Kenneth F. Miller , William Hilakos
CPC分类号： C08G63/64
摘要： A new aromatic copolyestercarbonate is achieved with 70 to 95 weight percent ester content and having consistently high 3.2 mm impact strength while maintaining a high level of stress cracking resistance.
摘要翻译： 实现了新的芳族共聚酯碳酸酯，其具有70至95重量％的酯含量并且具有始终高的3.2mm冲击强度，同时保持高水平的抗应力开裂性。
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