公开(公告)号：US06821616B1

公开(公告)日：2004-11-23

申请号：US09457743

申请日：1999-12-10

申请人： Hideaki Sakurai ,  Yukiya Yamashita ,  Yoshirou Kuromitsu

发明人： Hideaki Sakurai ,  Yukiya Yamashita ,  Yoshirou Kuromitsu

IPC分类号： B32B904

CPC分类号： C03C17/3452 ,  C03C2218/32 ,  C03C2218/355 ,  Y10T428/26 ,  Y10T428/265

摘要： The present invention provides a protecting film capable of preventing deterioration in adhesion and matching to a substrate (dielectric layer), and deterioration in electric insulation. The protecting film includes a film body composed of MgO or the like which is inhibited from reacting with CO2 gas and H2O gas in air to prevent degeneration of MgO or the like into MgCO3 and Mg(OH)2, etc. harmful to FPD. The film body is formed on the surface of the substrate, and the fluoride layer is formed on the surface of the film body. The fluoride layer is represented by MOXFY (M is Mg, Ca, Sr, Ba, an alkali earth complex metal, a rare earth metal, or a complex metal of an alkali earth metal and a rare earth metal, 0≦X

摘要翻译： 本发明提供能够防止粘合性劣化和与基板（电介质层）匹配的保护膜以及电绝缘性的劣化。 保护膜包括由MgO等构成的膜体，其被抑制与空气中的CO 2气体和H 2 O气体反应，以防止MgO等变为对FPD有害的MgCO 3和Mg（OH）2等。 在基材的表面上形成膜体，并且在膜体的表面上形成氟化物层。 氟化物层由MOXFY（M是Mg，Ca，Sr，Ba，碱土金属络合物，稀土金属或碱土金属和稀土金属的复合金属，0 <= X 2 ，0

公开(公告)号：US06329490B1

公开(公告)日：2001-12-11

申请号：US09540285

申请日：2000-03-31

申请人： Yukiya Yamashita ,  Kenji Hayashi ,  Masaoki Ishihara

发明人： Yukiya Yamashita ,  Kenji Hayashi ,  Masaoki Ishihara

IPC分类号： C08G7724

CPC分类号： C08G77/045 ,  C08G77/22 ,  C08G77/24

摘要： Disclosed are polyhedral organosilicon compounds which are possible to be polymerized and can form a film excellent in adhesiveness to a substrate, having a high hardness, a high transparency and having water and oil repellency, and comprise organofluoro groups or both of organofluoro groups and reactive functional groups, the compounds being soluble in an organic solvent and stable. Organosilicon compounds which have perfluoroalkyl groups or both perfluoroalkyl groups and reactive functional groups and which have a polyhedral structure have the following formulas of (I), (II) and (III): [Rf1—X1—(CH2)a—SiO1.5]m  (I) [Rf1—X1—(CH2)a—SiO1.5]m[Rf2—(X2)c—(CH2)b—SiO1.5]n  (II) [Rf1—X1—(CH2)a—SiO1.5]m[R—(X2)c—(CH2)b—SiO1.5]n  (III) wherein each of Rf1 and Rf2 represents a perfluoroalkyl group, R represents a functional group, each of X1 and X2 represents a divalent bonding group, each of a and b represents 0 or an integer of up to 10, c represents 0 or 1, each of m and n represents an integer of 1 to 19 and m+n is an integer of 4 to 20.

摘要翻译： 公开了可能聚合的多面体有机硅化合物，并且可以形成具有高硬度，高透明度和具有拒水拒油性的基材粘附性优异的膜，并且包含有机氟基团或有机氟基团和反应性官能团 所述化合物可溶于有机溶剂并稳定。具有全氟烷基或全氟烷基和反应性官能团两者并具有多面体结构的有机硅化合物具有下式（I），（II）和（III）： 其中，Rf1和Rf2各自表示全氟烷基，R表示官能团，X1和X2各自表示二价键合基​​，a和b各自表示0或10以下的整数，c表示0或1， m表示1〜19的整数，m + n表示4〜20的整数。

公开(公告)号：US06265126B1

公开(公告)日：2001-07-24

申请号：US09447830

申请日：1999-11-23

申请人： Akira Nishihara ,  Yukiya Yamashita ,  Hideaki Sakurai

发明人： Akira Nishihara ,  Yukiya Yamashita ,  Hideaki Sakurai

IPC分类号： G03G9097

CPC分类号： C09C3/006 ,  C01P2004/84 ,  C01P2006/12 ,  C01P2006/80 ,  C01P2006/90 ,  C09C1/3081 ,  C09C1/309 ,  C09C1/3684 ,  C09C1/3692 ,  C09C1/407 ,  C09C3/12 ,  G03G9/09716 ,  Y10T428/2995 ,  Y10T428/2998

摘要： A hydrophobic metal oxide powder obtained by simultaneously surface-treating a powder of a metal oxide (for example, silica, titania, alumina, or the like) with silicone oil having epoxy groups and a non-polymeric amine compound having a lower number of primary and/or secondary amino groups than the number required for reaction with all epoxy groups, or surface-treating the powder with silicon oil having epoxy groups and amino groups and previously obtained by reaction. Straight silicone oil may be further used for surface treatment. Frictional charge which is controlled within a wide range of from negative charge to positive charge, high hydrophobicity and fluidity can be imparted to the powder by using a relatively small amount of coating, and a hydrophobic metal oxide powder useful as an additive for an electrophotographic developer can be obtained.

摘要翻译： 通过用具有环氧基的硅油同时表面处理金属氧化物粉末（例如二氧化硅，二氧化钛，氧化铝等）而获得的疏水性金属氧化物粉末和具有较低数量的主要原料的非聚合胺化合物 和/或仲氨基，而不是与所有环氧基反应所需的数目，或用具有环氧基和氨基的硅油表面处理并预先通过反应获得的仲氨基。 直接硅油可进一步用于表面处理。 通过使用相对少量的涂层，可以将粉末中的从负电荷到正电荷，高疏水性和流动性的宽范围内控制的摩擦电荷和用作电子照相显影剂的添加剂的疏水性金属氧化物粉末 可以获得。