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公开(公告)号：US07985821B2
公开(公告)日：2011-07-26
申请号：US12761719
申请日：2010-04-16
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
CPC分类号： C09D183/06 , C08G77/045 , C08G77/14
摘要： A process for producing a low VOC epoxy silane oligomer which includes hydrolyzing an epoxy silane, the epoxy silane upon hydrolysis of its hydrolyzable sites producing a reduced amount of volatile organic compound compared to that produced by the hydrolysis of a silane possessing an equivalent number of hydrolyzable sites all of which are hydrolyzable alkoxy groups, the hydrolyzing of the epoxy silane being carried out with less than 1.5 equivalents of water, said water being continuously fed during the hydrolysis reaction.
摘要翻译： 一种生产低VOC环氧硅烷低聚物的方法，其包括水解环氧硅烷，环氧硅烷在其水解可水解位点水解时产生的挥发性有机化合物的量相比，通过水解具有相当数量的可水解的硅烷 所有这些都是可水解的烷氧基，所述环氧硅烷的水解用小于1.5当量的水进行，所述水在水解反应期间连续进料。
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公开(公告)号：US20110112221A1
公开(公告)日：2011-05-12
申请号：US13006917
申请日：2011-01-14
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
CPC分类号： C08G77/14 , C08K3/08 , C09D183/06
摘要： A process for producing an epoxy silane oligomer including a reaction glycidoxy silane and/or cycloaliphatic epoxy silane having 2 or 3 allcoxy groups and, optionally, a copolymerizable silane other than glycidoxy and cycloaliphatic epoxy silane, with less than 1.5 equivalents of water in the presence of a catalyst, wherein said water is continuously fed during the reaction.
摘要翻译： 包括具有2或3个全氧基的反应缩水甘油氧基硅烷和/或环脂族环氧硅烷的环氧硅烷低聚物的方法，以及任选的除缩水甘油氧基和环脂族环氧硅烷以外的可共聚的硅烷，在存在下具有小于1.5当量的水 的催化剂，其中所述水在反应期间连续进料。
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公开(公告)号：US07906604B2
公开(公告)日：2011-03-15
申请号：US12761719
申请日：2010-04-16
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
摘要： A process for producing a low VOC epoxy silane oligomer which includes hydrolyzing an epoxy silane, the epoxy silane upon hydrolysis of its hydrolyzable sites producing a reduced amount of volatile organic compound compared to that produced by the hydrolysis of a silane possessing an equivalent number of hydrolyzable sites all of which are hydrolyzable alkoxy groups, the hydrolyzing of the epoxy silane being carried out with less than 1.5 equivalents of water, said water being continuously fed during the hydrolysis reaction.
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公开(公告)号：US07732552B2
公开(公告)日：2010-06-08
申请号：US11341800
申请日：2006-01-27
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
CPC分类号： C09D183/06 , C08G77/045 , C08G77/14
摘要： A process for producing a low VOC epoxy silane oligomer which includes the reaction of an epoxy silane with water in a water to silane molar ratio of from 0.1 to 1.5, in which the epoxy silane is the reaction product of an epoxy alkoxy-substituted silane and a diol or a dicarboxylic acid.
摘要翻译： 一种生产低VOC环氧硅烷低聚物的方法，其包括环氧硅烷与水的反应，水与硅烷的摩尔比为0.1至1.5，其中环氧硅烷是环氧烷氧基取代的硅烷和 二醇或二羧酸。
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公开(公告)号：US07595372B2
公开(公告)日：2009-09-29
申请号：US11297714
申请日：2005-12-08
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
IPC分类号： C08G77/18
CPC分类号： C09D5/028 , C08K3/08 , C09D5/10 , C09D7/70 , C09D183/06 , C08L2666/54
摘要： A process for producing an epoxy silane oligomer including a reaction glycidoxy silane and/or cycloaliphatic epoxy silane having 2 or 3 alkoxy groups and, optionally, a copolymerizable silane other than glycidoxy and cycloaliphatic epoxy silane, with less than 1.5 equivalents of water in the presence of a catalyst, wherein said water is continuously fed during the reaction.
摘要翻译： 包括具有2或3个烷氧基的反应缩水甘油氧基硅烷和/或环脂族环氧硅烷的环氧硅烷低聚物的方法，以及任选的除缩水甘油氧基和环脂族环氧硅烷以外的可共聚硅烷，在存在下具有小于1.5当量的水 的催化剂，其中所述水在反应期间连续进料。
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公开(公告)号：US07893183B2
公开(公告)日：2011-02-22
申请号：US11100840
申请日：2005-04-07
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
IPC分类号： C08G77/14
CPC分类号： C08G77/14 , C08K3/08 , C09D183/06
摘要： A process for producing an epoxy silane oligomer including a reaction glycidoxy silane and/or cycloaliphatic epoxy silane having 2 or 3 alkoxy groups and, optionally, a copolymerizable silane other than glycidoxy and cycloaliphatic epoxy silane, with less than 1.5 equivalents of water in the presence of a catalyst, wherein said water is continuously fed during the reaction.
摘要翻译： 包括具有2或3个烷氧基的反应缩水甘油氧基硅烷和/或环脂族环氧硅烷的环氧硅烷低聚物的方法，以及任选的除缩水甘油氧基和环脂族环氧硅烷以外的可共聚硅烷，在存在下具有小于1.5当量的水 的催化剂，其中所述水在反应期间连续进料。
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公开(公告)号：US20100217016A1
公开(公告)日：2010-08-26
申请号：US12761719
申请日：2010-04-16
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
IPC分类号： C07F7/02
CPC分类号： C09D183/06 , C08G77/045 , C08G77/14
摘要： A process for producing a low VOC epoxy silane oligomer which includes hydrolyzing an epoxy silane, the epoxy silane upon hydrolysis of its hydrolyzable sites producing a reduced amount of volatile organic compound compared to that produced by the hydrolysis of a silane possessing an equivalent number of hydrolyzable sites all of which are hydrolyzable alkoxy groups, the hydrolyzing of the epoxy silane being carried out with less than 1.5 equivalents of water, said water being continuously fed during the hydrolysis reaction.
摘要翻译： 一种生产低VOC环氧硅烷低聚物的方法，其包括水解环氧硅烷，环氧硅烷在其水解可水解位点水解时产生的挥发性有机化合物的量相比，通过水解具有相当数量的可水解的硅烷 所有这些都是可水解的烷氧基，所述环氧硅烷的水解用小于1.5当量的水进行，所述水在水解反应期间连续进料。
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公开(公告)号：US20060225613A1
公开(公告)日：2006-10-12
申请号：US11100840
申请日：2005-04-07
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
CPC分类号： C08G77/14 , C08K3/08 , C09D183/06
摘要： A process for producing an epoxy silane oligomer including a reaction glycidoxy silane and/or cycloaliphatic epoxy silane having 2 or 3 alkoxy groups and, optionally, a copolymerizable silane other than glycidoxy and cycloaliphatic epoxy silane, with less than 1.5 equivalents of water in the presence of a catalyst, wherein said water is continuously fed during the reaction.
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公开(公告)号：US20060225612A1
公开(公告)日：2006-10-12
申请号：US11297714
申请日：2005-12-08
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
CPC分类号： C09D5/028 , C08K3/08 , C09D5/10 , C09D7/70 , C09D183/06 , C08L2666/54
摘要： A process for producing an epoxy silane oligomer including a reaction glycidoxy silane and/or cycloaliphatic epoxy silane having 2 or 3 alkoxy groups and, optionally, a copolymerizable silane other than glycidoxy and cycloaliphatic epoxy silane, with less than 1.5 equivalents of water in the presence of a catalyst, wherein said water is continuously fed during the reaction.
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公开(公告)号：US08338531B2
公开(公告)日：2012-12-25
申请号：US13006917
申请日：2011-01-14
申请人： Alain Lejeune , Yves Gentil
发明人： Alain Lejeune , Yves Gentil
IPC分类号： C08L83/06
CPC分类号： C08G77/14 , C08K3/08 , C09D183/06
摘要： A process for producing an epoxy silane oligomer including a reaction glycidoxy silane and/or cycloaliphatic epoxy silane having 2 or 3 alkoxy groups and, optionally, a copolymerizable silane other than glycidoxy and cycloaliphatic epoxy silane, with less than 1.5 equivalents of water in the presence of a catalyst, wherein said water is continuously fed during the reaction.
摘要翻译： 包括具有2或3个烷氧基的反应缩水甘油氧基硅烷和/或环脂族环氧硅烷的环氧硅烷低聚物的方法，以及任选的除缩水甘油氧基和环脂族环氧硅烷以外的可共聚硅烷，在存在下具有小于1.5当量的水 的催化剂，其中所述水在反应期间连续进料。
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