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    Poly-[(dialkyl and hydroxy-dialkyl-imino)ethylene halides] and process
    1.
    发明授权
    Poly-[(dialkyl and hydroxy-dialkyl-imino)ethylene halides] and process 失效
    聚{8（二烷基和羟基 - 二烷基 - 亚氨基）乙烯卤化物{9}和方法

    公开(公告)号：US4161581A

    公开(公告)日：1979-07-17

    申请号：US837980

    申请日：1977-09-29

    申请人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    发明人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    IPC分类号： C07D265/08 ,  C08G73/02

    CPC分类号： C08G73/0233 ,  C07D265/08 ,  C08G73/0226

    摘要： Novel polymers having a linear backbone which is free from both branching and cross-linking, comprising either tertiary or quaternized nitrogen atoms linked to each other through ethylene groups. These polymers are useful as antimicrobials, flocculating agents, antistatic agents, electroconductive agents for coating paper, chelating agents and bile acid binding agents, as well as in similar applications where their high charge to weight ratio and fully accessible nitrogen atoms can be employed. The polymers are obtained by the polymerization of an oxazoline, hydrolysis or direct reduction, nitrogen substitution, and optional quaternization of the resulting polymer.

    摘要翻译： 具有不含支链和交联的直链骨架的新型聚合物包括通过乙烯基彼此连接的叔或季铵化的氮原子。 这些聚合物可用作抗微生物剂，絮凝剂，抗静电剂，用于涂布纸的导电剂，螯合剂和胆汁酸结合剂，以及可以使用其高电荷重量比和完全可及的氮原子的类似应用。 通过恶唑啉的聚合，所得聚合物的水解或直接还原，氮取代和任选的季铵化获得聚合物。

    Poly[{alkyl-(3-ammoniopropyl)iminio}trimethylene dihalides] and process
    2.
    发明授权
    Poly[{alkyl-(3-ammoniopropyl)iminio}trimethylene dihalides] and process 失效
    聚{8 {55烷基 - （3-氨基丙基）亚氨基{56三亚甲基二卤化物{9 {0和方法

    公开(公告)号：US4098726A

    公开(公告)日：1978-07-04

    申请号：US783886

    申请日：1977-04-01

    申请人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    发明人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    IPC分类号： C08G73/00 ,  A61K31/14 ,  C07C67/00 ,  C07C209/00 ,  C07C209/12 ,  C07C211/63 ,  C08G73/02

    CPC分类号： C08G73/0226 ,  C07C209/68 ,  C07C209/74

    摘要： Novel polymers having a linear backbone which is free from both branching and cross-linking, comprising quaternized nitrogen atoms linked to each other through trimethylene groups. By the term "linear backbone" is meant that the polymer has only acyclic groups, i. e. trimethylene, linking the nitrogen atoms in a single continuous chain; the polymer is free from "branching" when it has no repeating monomer units extending from the polymer backbone; and it is free from "cross-linking" when there is no joining of two linear backbones. These polymers are useful as antimicrobials, flocculating agents, antistatic agents, electroconductive agents for coating paper, chelating agents and bile acid binding agents, as well as in similar applications where their high charge to weight ratio and fully accessible nitrogen atoms can be employed. The polymers are obtained by the polymerization of dihydro-oxazine, reductive alkylation of the resulting polymer, followed by quaternization.

    摘要翻译： 具有不含支链和交联的线性骨架的新型聚合物，其包含通过三亚甲基彼此连接的季铵化氮原子。 术语“直链骨架”是指聚合物仅具有非循环基团， e。 三亚甲基，连接单个连续链中的氮原子; 当聚合物没有从聚合物骨架延伸的重复单体单元时，没有“支化”; 当没有连接两个线性骨架时，它没有“交联”。 这些聚合物可用作抗微生物剂，絮凝剂，抗静电剂，用于涂布纸的导电剂，螯合剂和胆汁酸结合剂，以及可以使用其高电荷重量比和完全可及的氮原子的类似应用。 聚合物通过二氢恶嗪的聚合，所得聚合物的还原烷基化，然后季铵化得到。

    Poly-[(methylimino)trimethylene]
    3.
    发明授权
    Poly-[(methylimino)trimethylene] 失效
    聚 - [（甲基亚氨基）三亚甲基]

    公开(公告)号：US4217429A

    公开(公告)日：1980-08-12

    申请号：US028954

    申请日：1979-04-11

    申请人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    发明人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    IPC分类号： C07D265/08 ,  C08G73/02

    CPC分类号： C07D265/08 ,  C08G73/0226 ,  C08G73/0233

    摘要： Novel polymers having a linear backbone which is free from both branching and cross-linking, comprising quaternized nitrogen atoms linked to each other through trimethylene groups. By the term "linear backbone" is meant that the polymer has only acyclic groups, i.e. trimethylene, linking the nitrogen atoms in a single continuous chain; the polymer is free from "branching" when it has no repeating monomer units extending from the polymer backbone; and it is free from "cross-linking" when there is no joining of two linear backbones. These polymers are useful as antimicrobials, flocculating agents, antistatic agents, electroconductive agents for coating paper, chelating agents and bile acid binding agents, as well as in similar applications where their high charge to weight ratio and fully accessible nitrogen atoms can be employed. The polymers are obtained by the polymerization of dihydro-oxazine, reductive alkylation of the resulting polymer, followed by quaternization.

    摘要翻译： 具有不含支链和交联的线性骨架的新型聚合物，其包含通过三亚甲基彼此连接的季铵化氮原子。 术语“直链骨架”是指聚合物只有非循环基团，即三亚甲基，连接单个连续链中的氮原子; 当聚合物没有从聚合物骨架延伸的重复单体单元时，没有“支化”; 当没有连接两个线性骨架时，它没有“交联”。 这些聚合物可用作抗微生物剂，絮凝剂，抗静电剂，用于涂布纸的导电剂，螯合剂和胆汁酸结合剂，以及可以使用其高电荷重量比和完全可及的氮原子的类似应用。 聚合物通过二氢恶嗪的聚合，所得聚合物的还原烷基化，然后季铵化得到。

    Process of preparing poly[{alkyl-(3-ammoniopropyl)iminio}trimethylene dihalides]
    4.
    发明授权
    Process of preparing poly[{alkyl-(3-ammoniopropyl)iminio}trimethylene dihalides] 失效
    制备聚[{烷基 - （3-氨基丙基）亚氨基]三亚甲基二卤化物的方法]

    公开(公告)号：US4206295A

    公开(公告)日：1980-06-03

    申请号：US28933

    申请日：1979-04-11

    申请人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    发明人： Arthur F. Wagner ,  Nathaniel Grier ,  Tsung-Ying Shen

    IPC分类号： C07D265/08 ,  C08G73/02 ,  C08L79/00

    CPC分类号： C08G73/0226 ,  C07D265/08 ,  C08G73/0233

    摘要： Novel polymers having a linear backbone which is free from both branching and cross-linking, comprising quaternized nitrogen atoms linked to each other through trimethylene groups. By the term "linear backbone" is meant that the polymer has only acyclic groups, i.e. trimethylene, linking the nitrogen atoms in a single continuous chain; the polymer is free from "branching" when it has no repeating monomer units extending from the polymer backbone; and it is free from "cross-linking" when there is no joining of two linear backbones. These polymers are useful as antimicrobials, flocculating agents, antistatic agents, electroconductive agents for coating paper, chelating agents and bile acid binding agents, as well as in similar applications where their high charge to weight ratio and fully accessible nitrogen atoms can be employed. The polymers are obtained by the polymerization of dihydro-oxazine, reductive alkylation of the resulting polymer, followed by quaternization.

    摘要翻译： 具有不含支链和交联的线性骨架的新型聚合物，其包含通过三亚甲基彼此连接的季铵化氮原子。 术语“直链骨架”是指聚合物只有非循环基团，即三亚甲基，连接单个连续链中的氮原子; 当聚合物没有从聚合物骨架延伸的重复单体单元时，没有“支化”; 当没有连接两个线性骨架时，它没有“交联”。 这些聚合物可用作抗微生物剂，絮凝剂，抗静电剂，用于涂布纸的导电剂，螯合剂和胆汁酸结合剂，以及可以使用其高电荷重量比和完全可及的氮原子的类似应用。 聚合物通过二氢恶嗪的聚合，所得聚合物的还原烷基化，然后季铵化得到。

    Controlled partially cross-linked 3,3-ionenes
    6.
    发明授权
    Controlled partially cross-linked 3,3-ionenes 失效
    受控的部分交联的3,3-紫罗烯

    公开(公告)号：US4071478A

    公开(公告)日：1978-01-31

    申请号：US693589

    申请日：1976-06-07

    申请人： Tsung-Ying Shen ,  Arthur F. Wagner

    发明人： Tsung-Ying Shen ,  Arthur F. Wagner

    IPC分类号： C08G73/02

    CPC分类号： C08G73/0226

    摘要： The invention disclosed herein relates to novel partially cross-linked, fully quaternized poly-[(methylimino)trimethylene] polymers wherein a minor proportion (1% to 20%) of the nitrogen atoms in adjacent poly-[(methylimino)trimethylene] linear chains are, by quaternization, joined through trimethylene or 2-hydroxy-trimethylene bridges, the non-cross-linked nitrogens in the said linear chains being fully quaternized with lower alkyl or trialkylammoniopropyl groupings; and to the novel process for preparing these partially cross-linked, fully quaternized polymers which comprises reacting poly-[(methylimino)trimethylene] with 0.01 to 0.2 equivalents of 1,3-dihalo-propane or 1,3-dihalo-2-hydroxypropane per equivalent of tertiary amine in said poly-[(methylimino)trimethylene], and subsequently reacting the resulting product with excess alkyl halide or 3-halopropyltrialkylammonium halide. These partially cross-linked fully quaternized poly-[(methylimino) trimethylene] polymers are useful as highly-efficient bile acid sequestrants.

    摘要翻译： 本文公开的本发明涉及新的部分交联的完全季铵化的聚[（甲基亚氨基）三亚甲基]聚合物，其中相邻的聚 - [（甲基亚氨基）三亚甲基]线性链中的少量（1％至20％）的氮原子 通过季铵化通过三亚甲基或2-羟基 - 三亚甲基桥连接，所述直链中的非交联氮被低级烷基或三烷基铵丙基团全部季铵化; 以及制备这些部分交联的完全季铵化聚合物的新方法，其包括使聚[（甲基亚氨基）三亚甲基]与0.01至0.2当量的1,3-二卤代丙烷或1,3-二卤代-2-羟基丙烷 在所述聚 - [（甲基亚氨基）三亚甲基]中每当量的叔胺，然后使所得产物与过量的烷基卤化物或3-卤代丙基三烷基卤化铵反应。 这些部分交联的完全季铵化的聚[（甲基亚氨基）三亚甲基]聚合物可用作高效胆汁酸螯合剂。

    3-[N'-(3-Halopropyl)-N-'-methylamino]-N,N,N-trimethyl-1-propanaminium halide and acid addition salts thereof
    7.
    发明授权
    3-[N'-(3-Halopropyl)-N-'-methylamino]-N,N,N-trimethyl-1-propanaminium halide and acid addition salts thereof 失效
    3- {8 N {40-（3-氯丙基）-N- {40-甲基氨基{9-N，N，N-三甲基-1-丙酰胺及其酸加成盐

    公开(公告)号：US4016209A

    公开(公告)日：1977-04-05

    申请号：US570910

    申请日：1975-04-23

    申请人： Arthur F. Wagner ,  Tsung-Ying Shen

    发明人： Arthur F. Wagner ,  Tsung-Ying Shen

    IPC分类号： C08G73/00 ,  A61K31/14 ,  C07C67/00 ,  C07C209/00 ,  C07C209/12 ,  C07C211/63 ,  C08G73/02 ,  C07C87/30

    CPC分类号： C08G73/0226 ,  C07C209/68 ,  C07C209/74

    摘要： Novel linear, unbranched, non-cross-linked polymers particularly poly-[{methyl-(3-trimethylammoniopropyl)imino} trimethylene dihalide] are prepared by the polymerization of the novel monomer, 3-[N'-(3-halopropyl)-N'-methylamino]-N,N,N-trimethyl-l-propanaminium halide, or an acid addition salt thereof preferably in an oxygen excluded environment, e.g., under nitrogen or argon. The polymer, especially after modification of terminal groups, is an excellent oral anticholesterolemic.

    摘要翻译： 通过新型单体3- [N' - （3-卤代丙基） - 苯基）亚胺的聚合制备了新的直链，非支链，非交联的聚合物，特别是聚 - [{甲基 - （3-三甲基铵丙基）亚氨基} N'-甲基氨基] -N，N，N-三甲基-1-丙酰胺或其酸加成盐，优选在排除氧的环境中，例如在氮气或氩气下。 聚合物，特别是端基修饰后，是优异的口服抗胆固醇血症。