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    Separation of ionic liquids in coalescing devices
    1.
    发明授权
    Separation of ionic liquids in coalescing devices 有权

    公开(公告)号：US10137386B2

    公开(公告)日：2018-11-27

    申请号：US15039084

    申请日：2014-12-01

    Applicant: BASF SE

    Inventor： Daniel Pfeiffer ,  Stefan Bitterlich ,  Michael Hübner

    IPC: C07C7/144 ,  B01D17/04 ,  B01D17/00 ,  C07C7/00

    Abstract: A process for separating a phase (A) comprising at least one ionic liquid from a phase (B), where phase (A) has a higher viscosity than phase (B), comprising: a) providing a stream (S1) comprising a dispersion (D1) in which phase (A) is dispersed in phase (B), b) introducing stream (S1) into a coalescing device (KV), where the inflow rate of stream (S1) is from 0.05 to 150 kg/(cm2*h) based on the average cross-sectional area of coalescing device (KV), wherein the packing density of coalescing device (KV) is from 50 to 500 kg/m3, separating phase (A) from phase (B) in coalescing device (KV), discharging a stream (S2) comprising at least 70% by weight of phase (A) from coalescing device (KV) and discharging a stream (S3) comprising at least 70% by weight of phase (B) from coalescing device (KV).

    CHEMICAL CONVERSION PROCESS IN A DISPERSION
    2.
    发明申请
    CHEMICAL CONVERSION PROCESS IN A DISPERSION 审中-公开
    化学转化过程

    公开(公告)号：US20140018591A1

    公开(公告)日：2014-01-16

    申请号：US13937351

    申请日：2013-07-09

    Applicant: BASF SE

    Inventor： Steffen Tschirschwitz ,  Joni Joni ,  Jochen Bürkle ,  Stefan Bitterlich ,  Daniel Pfeiffer ,  Michael Hübner ,  Nicole Holub

    IPC: C07C5/29

    CPC classification number: C07C5/29 ,  C07C2601/14 ,  C07C13/18

    Abstract: The present invention relates to a chemical conversion process, preferably an isomerization process, for at least one hydrocarbon in the presence of an ionic liquid. The chemical conversion is performed in a dispersion, with dispersion of the hydrocarbon (phase (B)) in the ionic liquid (phase (A)) in the dispersion, the volume ratio of phase (A) to phase (B) being in the range from 2.5 to 4:1 [vol/vol].

    Abstract translation: 本发明涉及在离子液体存在下至少一种烃的化学转化方法，优选异构化方法。 在分散体中进行化学转化，其中烃（相（B））在分散体中的离子液体（相（A））中分散，相（A）与相（B）的体积比在 范围为2.5至4：1 [vol / vol]。

    Extraction column and process for extracting a constituent from a fluid
    4.
    发明授权
    Extraction column and process for extracting a constituent from a fluid 有权

    公开(公告)号：US09643910B2

    公开(公告)日：2017-05-09

    申请号：US14573313

    申请日：2014-12-17

    Applicant: BASF SE

    Inventor： Ulrich Hammon ,  Daniel Pfeiffer ,  Jonathan Walter

    IPC: B01D3/40 ,  C07C51/48 ,  B01D11/04 ,  B01D3/14 ,  B01D11/00

    CPC classification number: C07C51/48 ,  B01D3/141 ,  B01D3/40 ,  B01D11/0426 ,  B01D11/043 ,  B01D2011/002

    Abstract: The present invention relates to an extraction column 1 having a vertically aligned column body 2 which is cylindrical at least in sections and forms a column cavity 3 having a horizontal maximum extent, with provision in the column body 2 of at least one first feed 4 for an extractant, at least one second feed 5 for the fluid to be extracted and at least one outlet 6 for the extract mixture and at least one outlet for the raffinate. In the inventive extraction column 1, a vertically aligned divider 7 arranged within the column cavity 3 subdivides the column cavity 3 into a plurality of vertically aligned and horizontally divided regions, the horizontal maximum extent of each region being less than the horizontal maximum extent of the column cavity 3. The invention further relates to a process for extracting a constituent from a fluid by means of such an extraction column 1.

    NOVEL PROCESS FOR PREPARING CYCLOHEXANE FROM METHYLCYCLOPENTANE AND BENZENE
    5.
    发明申请
    NOVEL PROCESS FOR PREPARING CYCLOHEXANE FROM METHYLCYCLOPENTANE AND BENZENE 审中-公开
    从甲基环戊烷和苯甲腈制备环己烷的新工艺

    公开(公告)号：US20140114100A1

    公开(公告)日：2014-04-24

    申请号：US14053647

    申请日：2013-10-15

    Applicant: BASF SE

    Inventor： Steffen Tschirschwitz ,  Nicole Holub ,  Jochen Burkle ,  Oliver Christian Gobin ,  Markus Schmitt ,  Martin Bock ,  Aisha Ahmad Naddaf ,  Katharina SpuhI ,  Stefan Bitterlich ,  Daniel Pfeiffer

    IPC: C07C5/29

    CPC classification number: C07C5/29 ,  C07C5/10 ,  C07C7/163 ,  C07C2521/04 ,  C07C2521/06 ,  C07C2521/08 ,  C07C2523/46 ,  C07C2523/745 ,  C07C2523/75 ,  C07C2523/755 ,  C07C2527/06 ,  C07C2527/11 ,  C07C2527/1206 ,  C07C2527/1213 ,  C07C2527/126 ,  C07C2527/135 ,  C07C2601/14 ,  C07C13/18 ,  C07C13/10

    Abstract: The present invention relates to a process for preparing cyclohexane from methylcyclopentane (MCP) and benzene. In the context of the present invention, MCP and benzene are constituents of a hydrocarbon mixture (HM1) additionally comprising dimethylpentanes (DMP), possibly cyclohexane and at least one compound (low boiler) selected from acyclic C5-C6-alkanes and cyclopentane. First of all, benzene is converted in a hydrogenation step to cyclohexane, while MCP is isomerized in the presence of a catalyst, preferably of an acidic ionic liquid, to cyclohexane. The hydrogenation is preceded by a prior removal of the dimethylpentanes (DMP), with initial removal of any cyclohexane present in the hydrocarbon mixture (HM1) together with DMP. This cyclohexane already present can be separated again from DMP in a downstream rectification step and recycled into the process for cyclohexane preparation. Between hydrogenation and isomerization, low boilers are removed and, after the isomerization, the cyclohexane is isolated with return of unisomerized MCP and optionally of low boilers.

    Abstract translation: 本发明涉及从甲基环戊烷（MCP）和苯制备环己烷的方法。 在本发明的上下文中，MCP和苯是另外包含二甲基戊烷（DMP），可能的环己烷和至少一种选自无环C5-C6烷烃和环戊烷的化合物（低沸点）的烃混合物（HM1）的组分。 首先，将苯在氢化步骤中转化为环己烷，而MCP在催化剂，优选酸性离子液体存在下异构化为环己烷。 之前先氢化二甲基戊烷（DMP），然后与DMP一起初始除去烃混合物（HM1）中存在的任何环己烷。 已经存在的环己烷可以在下游精馏步骤中再次从DMP分离并再循环到环己烷制备方法中。 在氢化和异构化之间，除去低锅炉，在异构化之后，环己烷被分离出来，分离出未异构化的MCP和任选的低锅炉。

    REMOVAL OF IONIC LIQUIDS BY MEANS OF A KNITTED FABRIC
    6.
    发明申请
    REMOVAL OF IONIC LIQUIDS BY MEANS OF A KNITTED FABRIC 有权
    通过针织织物去除离子液体

    公开(公告)号：US20140018596A1

    公开(公告)日：2014-01-16

    申请号：US13937395

    申请日：2013-07-09

    Applicant: BASF SE

    Inventor： Daniel Pfeiffer ,  Stefan Bitterlich

    IPC: C07C7/144

    CPC classification number: C07C7/144 ,  C07C2601/14 ,  C07C13/18

    Abstract: The present invention relates to a process for separating a phase (A) comprising at least one ionic liquid from a phase (B), phase (A) having a higher viscosity than phase (B), comprising the following steps: a) providing a stream (S1) comprising a dispersion (D1) in which phase (A) is dispersed in phase (B), b) introducing stream (S1) into a phase separation unit (PT1) comprising a knitted fabric, preferably a knitted glass fiber fabric, c) separating the dispersed phase (A) from phase (B) in the phase separation unit (PT1), d) discharging a stream (S2) comprising at least 70% by weight, preferably at least 90% by weight, of phase (A) from the phase separation unit (PT1), and e) discharging a stream (S3) comprising at least 70% by weight, preferably at least 90% by weight, of phase (B) from the phase separation unit (PT1).

    Abstract translation: 本发明涉及一种分离包含至少一种离子液体的相（A）的方法，所述相（A）相具有比相（B）更高的粘度的相（B）相（A）相，包括以下步骤：a） 流（S1），其中相（A）相分散在相（B）中的分散体（D1），b）将流（S1）引入到包括针织物的相分离单元（PT1）中，优选为针织玻璃纤维织物 ，c）在相分离单元（PT1）中分离相（B）的分散相（A）; d）排出包含至少70重量％，优选至少90重量％的相 （A）的相分离单元（PT1），以及e）从相分离单元（PT1）排出包含至少70重量％，优选至少90重量％的相（B）的物流（S3） 。

    Removal of ionic liquids by means of coalescing filters made from acrylic/phenolic resin
    8.
    发明授权
    Removal of ionic liquids by means of coalescing filters made from acrylic/phenolic resin 有权
    通过由丙烯酸/酚醛树脂制成的聚结过滤器去除离子液体

    公开(公告)号：US09095789B2

    公开(公告)日：2015-08-04

    申请号：US13937386

    申请日：2013-07-09

    Applicant: BASF SE

    Inventor： Daniel Pfeiffer ,  Stefan Bitterlich

    IPC: B01D17/04

    CPC classification number: B01D17/045

    Abstract: The present invention relates to a process for separating a phase (A) comprising at least one ionic liquid from a phase (B), phase (A) having a higher viscosity than phase (B), comprising the following steps: a) providing a stream (S1) comprising a dispersion (D1) in which phase (A) is dispersed in phase (B), b) introducing stream (S1) into a coalescing filter (K) manufactured from acrylic/phenolic resin, c) separating the dispersed phase (A) from phase (B) in the coalescing filter (K), d) discharging a stream (S2) comprising at least 70% by weight, preferably at least 90% by weight, of phase (A) from the coalescing filter (K), and e) discharging a stream (S3) comprising at least 70% by weight, preferably at least 90% by weight, of phase (B) from the coalescing filter (K).

    Abstract translation: 本发明涉及一种分离包含至少一种离子液体的相（A）的方法，所述相（A）相具有比相（B）更高的粘度的相（B）相（A）相，包括以下步骤：a） 流（S1），其中相（A）相分散在相（B）中的分散体（D1），b）将流（S1）引入由丙烯酸/酚醛树脂制成的聚结过滤器（K）中，c） （K）中的相（B）的相（A）相，d）从聚结过滤器（K）中排出包含至少70重量％，优选至少90重量％的相（A）的物流 （K），和e）从聚结过滤器（K）排出包含至少70重量％，优选至少90重量％的相（B）的物流（S3）。

    REMOVAL OF IONIC LIQUIDS BY MEANS OF COALESCING FILTERS MADE FROM ACRYLIC/PHENOLIC RESIN
    10.
    发明申请
    REMOVAL OF IONIC LIQUIDS BY MEANS OF COALESCING FILTERS MADE FROM ACRYLIC/PHENOLIC RESIN 有权
    通过丙烯/酚醛树脂制备过滤器去除离子液体

    公开(公告)号：US20140018598A1

    公开(公告)日：2014-01-16

    申请号：US13937386

    申请日：2013-07-09

    Applicant: BASF SE

    Inventor： Daniel Pfeiffer ,  Stefan Bitterlich

    IPC: B01D17/04

    CPC classification number: B01D17/045

    Abstract: The present invention relates to a process for separating a phase (A) comprising at least one ionic liquid from a phase (B), phase (A) having a higher viscosity than phase (B), comprising the following steps: a) providing a stream (S1) comprising a dispersion (D1) in which phase (A) is dispersed in phase (B), b) introducing stream (S1) into a coalescing filter (K) manufactured from acrylic/phenolic resin, c) separating the dispersed phase (A) from phase (B) in the coalescing filter (K), d) discharging a stream (S2) comprising at least 70% by weight, preferably at least 90% by weight, of phase (A) from the coalescing filter (K), and e) discharging a stream (S3) comprising at least 70% by weight, preferably at least 90% by weight, of phase (B) from the coalescing filter (K).

    Abstract translation: 本发明涉及一种分离包含至少一种离子液体的相（A）的方法，所述相（A）相具有比相（B）更高的粘度的相（B）相（A）相，包括以下步骤：a） 流（S1），其中相（A）相分散在相（B）中的分散体（D1），b）将流（S1）引入由丙烯酸/酚醛树脂制成的聚结过滤器（K）中，c） （K）中的相（B）的相（A）相，d）从聚结过滤器（K）中排出包含至少70重量％，优选至少90重量％的相（A）的物流 （K），和e）从聚结过滤器（K）排出包含至少70重量％，优选至少90重量％的相（B）的物流（S3）。

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