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1.发明授权Process for manufacturing sodium carbonate perhydrate particles and coating them with sodium borosilicate 失效制造碳酸钠过水合物颗粒并用硼硅酸钠涂覆它们的方法
公开(公告)号：US5328721A
公开(公告)日：1994-07-12
申请号：US922712
申请日：1992-07-30
IPC分类号： B05D5/00 , B01J2/00 , B01J2/16 , B05D7/02 , B05D7/24 , C01B15/10 , C01D7/00 , C11D3/10 , C11D3/39 , C11D17/00
CPC分类号： C01B15/106 , B01J2/003 , B01J2/16 , C11D17/0039 , C11D3/3942
摘要： A process to manufacture and coat a sodium carbonate perhydrate containing 10.5% to 14% active oxygen which is stable in a non-phosphate detergent composition and which has a bulk density of from 900 to 1,050 kg/m.sup.3. Anhydrous sodium carbonate with a pore volume of at least 0.29 ml/g is contacted with 50% to 75% by weight hydrogen peroxide in the presence of 1-hydroxyethylidene-1,1-diphosphonic acid and water is evaporated at a rate to maintain a dry reaction mixture. The product is coated by sparging sodium borosilicate at a rate to avoid moistening the particles.
摘要翻译： 制造和涂覆含有10.5％至14％活性氧的碳酸钠过水合物的方法，其在非磷酸盐洗涤剂组合物中是稳定的，其堆积密度为900至1050kg / m 3。 在1-羟基亚乙基-1,1-二膦酸的存在下，将孔体积至少为0.29ml / g的无水碳酸钠与50％至75％重量的过氧化氢接触，并以保持水 干燥反应混合物。 通过以硼酸钠硼沸石的速率涂覆产物以避免润湿颗粒。
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公开(公告)号：US4511498A
公开(公告)日：1985-04-16
申请号：US557706
申请日：1983-12-02
摘要： A mixed phenyl/mesityl phosphate ester composition that is useful as a fire retardant additive, having a phosphorus content of from about 8.2% to about 8.4% is prepared by reacting with agitation at about 120.degree. C. to 130.degree. C. distilled still bottom phenols with phosphorus oxychloride in the presence of a Friedel-Crafts catalyst to form a reaction product containing a substantial quantity of monoaryl phosphodichloridate and diaryl phosphochloridate. This reaction product is then further reacted at an elevated temperature with sufficient phenol to form a triaryl phosphate ester mixture. The mixed phenyl/mesityl phosphate ester so obtained remains a liquid at room temperature over a substantial period of time.
摘要翻译： 通过在约120℃至130℃下搅拌反应制备磷含量为约8.2％至约8.4％的可用作阻燃添加剂的混合苯基/均三磷酸酯组合物，蒸馏的底部 苯酚与磷酰氯在Friedel-Crafts催化剂存在下反应形成含有大量单芳基磷酸二氯化物和二芳基磷酸氯化物的反应产物。 然后将该反应产物在升高的温度下与足够的苯酚反应以形成磷酸三芳基酯混合物。 如此获得的混合苯基/均三甲基磷酸酯在相当长的时间内在室温下保持液体。
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公开(公告)号：US4446062A
公开(公告)日：1984-05-01
申请号：US348636
申请日：1982-02-16
摘要： A mixed phenyl/mesityl phosphate ester composition that is useful as a fire retardant additive, having a phosphorus content of from about 8.2% to about 8.4% is prepared by reacting with agitation at about 120.degree. C. to 130.degree. C. distilled still bottom phenols with phosphorus oxychloride in the presence of a Friedel-Crafts catalyst to form a reaction product containing a substantial quantity of monoaryl phosphodichloridate and diaryl phosphochloridate. This reaction product is then further reacted at an elevated temperature with sufficient phenol to form a triaryl phosphate ester mixture. The mixed phenyl/mesityl phosphate ester so obtained remains a liquid at room temperature over a substantial period of time.
摘要翻译： 通过在约120℃至130℃下搅拌反应制备磷含量为约8.2％至约8.4％的可用作阻燃添加剂的混合苯基/均三磷酸酯组合物，蒸馏的底部 苯酚与磷酰氯在Friedel-Crafts催化剂存在下反应形成含有大量单芳基磷酸二氯化物和二芳基磷酸氯化物的反应产物。 然后将该反应产物在升高的温度下与足够的苯酚反应以形成磷酸三芳基酯混合物。 如此获得的混合苯基/均三甲基磷酸酯在相当长的时间内在室温下保持液体。
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4.发明授权High pressure thermal hydrolysis process to decompose triazines in acid waste streams 失效高压热水解方法在酸性废水中分解三倍体
公开(公告)号：US4013757A
公开(公告)日：1977-03-22
申请号：US569019
申请日：1975-04-17
CPC分类号： C02F1/025
摘要： A high pressure thermal hydrolysis process is described which comprises heating acid waste streams resulting from the manufacture of cyanuric acid and chlorinated derivatives of cyanuric acid, containing cyanuric acid and amino-substituted cyanurates, in a pressure vessel, at a temperature of from about 225.degree. to about 275.degree. C, to effect decomposition of these materials into ammonia and carbon dioxide. This process provides an effective pollution control means, compatible with existing commercial facilities.
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公开(公告)号：US4247988A
公开(公告)日：1981-02-03
申请号：US80882
申请日：1979-10-01
CPC分类号： F26B3/347
摘要： Excess water, both crystalline and non-crystalline, is removed safely and rapidly from active chlorine compounds by applying electromagnetic energy with frequencies lower than infrared to vaporize the excess water.
摘要翻译： 通过施加频率低于红外线的电磁能量蒸发多余的水，从活性氯化合物中安全和快速地除去过量的水，非晶态和非结晶水。
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公开(公告)号：US4556684A
公开(公告)日：1985-12-03
申请号：US644409
申请日：1984-08-27
申请人： Louis T. Gunkel , Charles V. Juelke
发明人： Louis T. Gunkel , Charles V. Juelke
摘要： Flame retardant polyphenylene ether resin compositions are described in which the flame retardant agent is a mixture (by weight) of the following:(a) about 1.5% to about 3.0% of: ##STR1## (b) about 15.0% to about 20.0% of: ##STR2## (c) about 23.0% to about 28.0% of: ##STR3## (d) about 47.0% to about 56.0% of: ##STR4## wherein R.sub.1 and R.sub.2 are each selected from the class consisting of hydrogen, methyl and ethyl, it being understood that when one of R.sub.1 and R.sub.2 is hydrogen the other is ethyl and when one of R.sub.1 and R.sub.2 is methyl the other is methyl, the resulting two methyl groups being in the 2,4-, 2,5-, 2,3-, 3,4- and 3,5-positions, it being further understood that the ethyl groups are almost entirely in the meta (m) and para (p) positions.
摘要翻译： 描述了阻燃聚苯醚树脂组合物，其中阻燃剂是以下的混合物（重量）：（a）约1.5％至约3.0％：（b）约15.0％至约20.0％ （c）约23.0％至约28.0％：（d）约47.0％至约56.0％的：其中R 1和R 2各自选自氢，甲基 和乙基，当R1和R2中的一个是氢时，另一个是乙基，当R 1和R 2之一是甲基时，另一个是甲基，得到的两个甲基在2,4-二 ，2,3,4a和3,5位，还可以理解的是，乙基几乎全部在间位（m）和对位（p）位。
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7.发明授权Refluxing water-in-oil emulsion process for preparing water-soluble polyelectrolyte particles 失效用于制备水溶性聚电解质颗粒的油包水乳液法
公开(公告)号：US4037040A
公开(公告)日：1977-07-19
申请号：US664852
申请日：1976-03-08
IPC分类号： C08F2/32 , C08F236/00
CPC分类号： C08F2/32 , Y10S526/909
摘要： There is provided a process for preparing water-soluble polyelectrolytes by a water-in-oil emulsion process. A mixture of a surfactant, free radical initiator, at least one water-soluble, oil-insoluble, ethylenically unsaturated monomer adapted to polymerize under refluxing conditions, oil and water (the oil and water being adapted to form an azeotropic boiling mixture) is heated with vigorous agitation. The monomer polymerizes at the reflux temperature under the vigorous agitation with a concomitant simultaneous loss of water. Finely divided, water-soluble particles result.
摘要翻译： 提供了一种通过油包水乳液法制备水溶性聚电解质的方法。 将表面活性剂，自由基引发剂，适于在回流条件下聚合的至少一种水溶性，不溶于油的烯属不饱和单体，油和水（油和水适于形成共沸混合物）的混合物被加热 激烈的激动 单体在剧烈搅拌下在回流温度下聚合，伴随同时损失水分。 精细分散，产生水溶性颗粒。
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