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公开(公告)号：US20230047367A1
公开(公告)日：2023-02-16
申请号：US17883600
申请日：2022-08-09
Applicant: Battelle Memorial Institute
Inventor： Stephen H. Rosansky , Michael Miller , Patrick Norris , Darwin Argumedo , Douglas Hendry , Ian Haggerty , Keith Brown , Joshua James , Joseph Casciano , Slawomir Winecki , Vivek Lal , Tom McGuinness
IPC: C02F9/00 , B01D61/02 , B01D61/08 , B01D61/10 , B04C5/04 , B04C5/081 , B04C5/085 , B04C5/20 , C04B35/12 , C04B35/622
Abstract: Per- and polyfluoroalkyl substances (PFAS) are destroyed by oxidation in supercritical conditions. PFAS in water is concentrated in a reverse osmosis step and salt from the resulting solution is removed in supercritical conditions prior to destruction of PFAS in supercritical conditions.
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2.发明公开公开(公告)号：US20230227335A1
公开(公告)日：2023-07-20
申请号：US17990765
申请日：2022-11-21
Applicant: Battelle Memorial Institute
Inventor： Lindy E. Dejarme , Kavitha Dasu , Russell R. Sirabian , Jeffrey Ellis , Dan Garbark , Nathan Bryant , John Tallarico , Joseph Casciano , Slawomir Winecki , David Holley , Joshua James , Keith Brown , Doug Hendry , Darwin Argumedo , Aaron Frank , Christopher Gordon Scheitlin , Michael M. Miller
CPC classification number: C02F1/441 , C02F1/04 , C02F1/722 , C02F2101/36
Abstract: Per- and polyfluoroalkyl substances (PFAS) are destroyed by oxidation in supercritical conditions. PFAS in water can be concentrated and prepared for destruction in a pretreatment phase. Following annihilation of the PFAS in supercritical conditions to levels below 5 parts per trillion (ppt), the water effluent can be used to recover heat, returned to sub-critical conditions, and then released back into the environment.
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公开(公告)号：US20200002784A1
公开(公告)日：2020-01-02
申请号：US16541355
申请日：2019-08-15
Applicant: Battelle Memorial Institute
Inventor： Rick Peterson , Michael Heinrichs , Vinay V. Gadkari , Rachid Taha , Slawomir Winecki , Darwin Argumedo
Abstract: A system for recovering rare earth elements from coal ash includes a leaching reactor, an ash dryer downstream of the leaching reactor, and a roaster downstream of the ash dryer that is cooperatively connected to both the leaching reactor and the ash dryer. Coal ash is mixed with an acid stream such that rare earth elements present in the coal ash are dissolved in the acid stream, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. Mixing of the coal ash with the acid stream can occur in a leaching reactor and heating of the leachate can occur in a roaster. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.
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公开(公告)号：US12065370B2
公开(公告)日：2024-08-20
申请号：US17839863
申请日：2022-06-14
Applicant: Battelle Memorial Institute
Inventor： Kurt Blohm , Richard Peterson , Ann E. Lane , Slawomir Winecki , Darwin Argumedo
IPC: C02F9/00 , B01D61/00 , B01D61/02 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , C02F1/36 , C02F1/44 , C02F1/469 , C02F103/08 , F03G7/00
CPC classification number: C02F9/00 , B01D61/002 , B01D61/025 , B01D61/026 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , B01D2311/04 , B01D2311/06 , B01D2311/08 , B01D2311/2523 , B01D2311/2684 , B01D2313/243 , B01D2313/246 , B01D2315/10 , B01D2317/02 , B01D2317/025 , B01D2319/04 , C02F1/36 , C02F1/441 , C02F1/445 , C02F1/4691 , C02F2103/08 , C02F2301/046 , C02F2301/08 , C02F2303/10 , F03G7/005 , B01D2311/06 , B01D2311/04 , B01D2311/08 , B01D2311/25
Abstract: Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.
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公开(公告)号：US10214437B2
公开(公告)日：2019-02-26
申请号：US15612570
申请日：2017-06-02
Applicant: Battelle Memorial Institute
Inventor： Kurt Blohm , Richard Peterson , Ann E. Lane , Slawomir Winecki , Darwin Argumedo
IPC: C02F9/00 , B01D61/00 , B01D61/02 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , C02F1/36 , C02F1/44 , C02F1/469 , C02F103/08 , F03G7/00
Abstract: Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.
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Patent Agency Ranking
公开(公告)号：US20170349467A1
公开(公告)日：2017-12-07
申请号：US15613793
申请日：2017-06-05
Applicant: Battelle Memorial Institute
Inventor： Kurt Blohm , Richard Peterson , Ann E. Lane , Slawomir Winecki , Darwin Argumedo
IPC: C02F9/00 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/00 , B01D61/02 , B01D61/58 , C02F103/08 , C02F1/36 , C02F1/44 , C02F1/469
CPC classification number: C02F9/00 , B01D61/002 , B01D61/022 , B01D61/025 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , B01D2311/04 , B01D2311/06 , B01D2311/08 , B01D2311/25 , B01D2311/2684 , B01D2313/243 , B01D2313/246 , B01D2315/10 , B01D2317/02 , B01D2317/025 , B01D2319/04 , C02F1/36 , C02F1/441 , C02F1/445 , C02F1/4691 , C02F2103/08 , C02F2301/046 , C02F2301/08 , C02F2303/10 , F03G7/005
Abstract: Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.
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公开(公告)号：US20170349465A1
公开(公告)日：2017-12-07
申请号：US15612570
申请日：2017-06-02
Applicant: Battelle Memorial Institute
Inventor： Kurt Blohm , Richard Peterson , Ann E. Lane , Slawomir Winecki , Darwin Argumedo
IPC: C02F9/00 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/00 , B01D61/02 , B01D61/58 , C02F103/08 , C02F1/36 , C02F1/44 , C02F1/469
CPC classification number: C02F9/00 , B01D61/002 , B01D61/022 , B01D61/025 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , B01D2311/04 , B01D2311/06 , B01D2311/08 , B01D2311/25 , B01D2311/2684 , B01D2313/243 , B01D2313/246 , B01D2315/10 , B01D2317/02 , B01D2317/025 , B01D2319/04 , C02F1/36 , C02F1/441 , C02F1/445 , C02F1/4691 , C02F2103/08 , C02F2301/046 , C02F2301/08 , C02F2303/10 , F03G7/005
Abstract: Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.
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公开(公告)号：US11999643B2
公开(公告)日：2024-06-04
申请号：US15613793
申请日：2017-06-05
Applicant: Battelle Memorial Institute
Inventor： Kurt Blohm , Richard Peterson , Ann E. Lane , Slawomir Winecki , Darwin Argumedo
IPC: C02F9/00 , B01D61/00 , B01D61/02 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , C02F1/44 , C02F103/08 , C02F1/36 , C02F1/469 , F03G7/00
CPC classification number: C02F9/00 , B01D61/002 , B01D61/025 , B01D61/026 , B01D61/04 , B01D61/06 , B01D61/08 , B01D61/58 , B01D2311/04 , B01D2311/06 , B01D2311/08 , B01D2311/25 , B01D2311/2684 , B01D2313/243 , B01D2313/246 , B01D2315/10 , B01D2317/02 , B01D2317/025 , B01D2319/04 , C02F1/36 , C02F1/441 , C02F1/445 , C02F1/4691 , C02F2103/08 , C02F2301/046 , C02F2301/08 , C02F2303/10 , F03G7/005 , B01D2311/06 , B01D2311/04 , B01D2311/08 , B01D2311/25
Abstract: Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.
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公开(公告)号：US20220315469A1
公开(公告)日：2022-10-06
申请号：US17839863
申请日：2022-06-14
Applicant: Battelle Memorial Institute
Inventor： Kurt Blohm , Richard Peterson , Ann E. Lane , Slawomir Winecki , Darwin Argumedo
Abstract: Systems and processes for purifying and concentrating a liquid feed stream are disclosed. In the systems, the concentrated liquid output from the high pressure side of a reverse osmosis stage is used as the draw solution in the low pressure side of the reverse osmosis stage in a configuration called osmotically assisted reverse osmosis. This reduces the osmotic pressure differential across the membrane, permitting high solute concentrations to be obtained, hastening the purification of the liquid. Reduced system pressures are also obtained by arranging multiple osmotically assisted reverse osmosis stages in a cross-current arrangement. Overall system energy consumption is reduced compared to conventional thermal processes for high concentration streams.
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10.发明申请公开(公告)号：US20170356067A1
公开(公告)日：2017-12-14
申请号：US15617589
申请日：2017-06-08
Applicant: Battelle Memorial Institute
Inventor： Rick Peterson , Michael Heinrichs , Vinay V. Gadkari , Rachid Taha , Slawomir Winecki , Darwin Argumedo
CPC classification number: C22B59/00 , C01B39/02 , C22B1/005 , C22B3/02 , C22B3/065 , C22B7/007 , C22B7/02 , Y02P10/234
Abstract: A system for recovering rare earth elements from coal ash includes a leaching reactor, an ash dryer downstream of the leaching reactor, and a roaster downstream of the ash dryer that is cooperatively connected to both the leaching reactor and the ash dryer. Coal ash is mixed with an acid stream such that rare earth elements present in the coal ash are dissolved in the acid stream, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. Mixing of the coal ash with the acid stream can occur in a leaching reactor and heating of the leachate can occur in a roaster. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.
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