Process for 3,4-disubstituted dinitroanilines
    10.
    发明授权
    Process for 3,4-disubstituted dinitroanilines 失效
    3,4-二取代二硝基苯胺的方法

    公开(公告)号:US6028226A

    公开(公告)日:2000-02-22

    申请号:US056415

    申请日:1998-04-07

    IPC分类号: C07C209/18 C07C213/00

    CPC分类号: C07C209/18

    摘要: Preparation process for 3,4-disubstituted dinitroanilines of formula ##STR1## in which, R.sub.1 and R.sub.2, which are identical to or different from one another, represent a hydrogen atom, a C.sub.1 to C.sub.6 saturated, linear or branched alkyl radical, a C.sub.2 to C.sub.6 linear or branched alkylene radical, a cyclopropyl radical or a chloroethyl radical,R.sub.3 and R.sub.4, which are identical to or different from one another are chosen from the group containing the chlorine atom, the amino group, the C.sub.1 to C.sub.3 lower alkyl radicals and the trifluoromethyl radical,comprising successively a dinitration stage of a 3,4-disubstituted phenol, an alkylation stage of the dinitrated derivative thus obtained and an amination stage of the 3,4-disubstituted 2,6-dinitro-alkoxybenzene thus obtained.

    摘要翻译: 其中R1和R2彼此相同或不同的3,4-二取代二硝基苯胺的制备方法代表氢原子,C1-C6饱和,直链或支链烷基,C2至C6直链 或支链亚烷基,环丙基或氯乙基,R3和R4彼此相同或不同,选自含有氯原子,氨基,C1至C3低级烷基和三氟甲基的基团 自由基,连续地包括3,4-二取代苯酚的二硝化阶段,如此获得的二硝基衍生物的烷基化阶段和由此获得的3,4-二取代2,6-二硝基 - 烷氧基苯胺的胺化阶段。