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    Methods for producing a dispersion containing silicon dioxide particles and cationization agent
    5.
    发明授权
    Methods for producing a dispersion containing silicon dioxide particles and cationization agent 有权
    生产含有二氧化硅颗粒和阳离子化剂的分散体的方法

    公开(公告)号：US08980960B2

    公开(公告)日：2015-03-17

    申请号：US13642862

    申请日：2011-05-23

    申请人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    发明人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    IPC分类号： C01B33/141 ,  C09C1/28 ,  D21H19/40 ,  B41M5/52 ,  B41M5/42

    CPC分类号： B41M5/5218 ,  B41M5/426 ,  C01B33/141 ,  D21H19/40

    摘要： Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of cationizing agent per square meter of the BET surface area of the silicon dioxide particles, wherein the cationizing agent is obtainable by reacting at least one haloalkyl-functional alkoxysilane, hydrolysis products, condensation products and/or mixtures thereof with at least one aminoalcohol and water; and optionally removing the resulting hydrolysis alcohol from the reaction mixture. Also the process for preparing the dispersion, wherein the cationizing agent comprises one or more quaternary, aminoalcohol-functional, organosilicon compounds of formula III and/or condensation products thereof, wherein Ru and Rv are independently C2-4 alkyl group, m is 2-5 and n is 2-5.

    摘要翻译： 制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂可通过使至少一种卤代烷基官能的烷氧基硅烷，水解产物，缩合产物和/或其与至少一种氨基醇的混合物和 水; 并任选地从反应混合物中除去所得的水解醇。 还有制备分散体的方法，其中阳离子化剂包含一种或多种式III的季氨基醇官能的有机硅化合物和/或其缩合产物，其中Ru和Rv独立地是C 2-4烷基，m是2- 5，n为2-5。

    METHODS FOR PRODUCING A DISPERSION CONTAINING SILICON DIOXIDE PARTICLES AND CATIONIZATION AGENT
    6.
    发明申请
    METHODS FOR PRODUCING A DISPERSION CONTAINING SILICON DIOXIDE PARTICLES AND CATIONIZATION AGENT 有权
    生产含二氧化硅颗粒和起泡剂的分散体的方法

    公开(公告)号：US20130040078A1

    公开(公告)日：2013-02-14

    申请号：US13642862

    申请日：2011-05-23

    申请人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    发明人： Stefan Scharfe ,  Andrea Heuschen ,  Christoph Batz-Sohn ,  Burkhard Standke ,  Christian Wassmer ,  Heinz Lach

    IPC分类号： C09D5/00 ,  B41M5/50 ,  C09D129/04

    CPC分类号： B41M5/5218 ,  B41M5/426 ,  C01B33/141 ,  D21H19/40

    摘要： Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of cationizing agent per square metre of the BET surface area of the silicon dioxide particles, wherein the cationizing agent is obtainable by reacting at least one haloalkyl-functional alkoxysilane, its hydrolysis products or condensation products and/or a mixture thereof with at least one aminoalcohol and a defined amount of water and optionally removing the resulting hydrolysis alcohol at least partly from the reaction mixture.Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of a cationizing agent per square metre of the BET surface area of the silicon dioxide particles, wherein the cationizing agent comprises one or more quaternary, aminoalcohol-functional, organosilicon compounds of the general formula III and/or condensation products thereof, wherein Ru and Rv are each independently of each other an alkyl group having 2 to 4 carbon atoms, m is 2 to 5 and n is 2 to 5.

    摘要翻译： 制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂可通过使至少一种卤代烷基官能的烷氧基硅烷，其水解产物或缩合产物和/或其混合物与至少一种 氨基醇和限定量的水，并任选地从反应混合物中部分地除去所得的水解醇。 制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂包含一种或多种通式III的季铵，氨基醇官能的有机硅化合物和/或其缩合产物，其中Ru和 Rv各自独立地为具有2至4个碳原子的烷基，m为2至5，n为2至5。

    Process for controlled hydrolysis and condensation of epoxy-functional organosilanes and the cocondensation thereof with further organofunctional alkoxysilanes
    9.
    发明授权
    Process for controlled hydrolysis and condensation of epoxy-functional organosilanes and the cocondensation thereof with further organofunctional alkoxysilanes 有权
    控制水解和缩合环氧官能有机硅烷的方法及其与另外的有机官能烷氧基硅烷的共缩聚

    公开(公告)号：US08394972B2

    公开(公告)日：2013-03-12

    申请号：US12673390

    申请日：2008-06-17

    申请人： Christian Wassmer ,  Burkhard Standke ,  Irene Lippert ,  Peter Jenkner

    发明人： Christian Wassmer ,  Burkhard Standke ,  Irene Lippert ,  Peter Jenkner

    IPC分类号： C07F7/02

    CPC分类号： C08G77/08 ,  C08G77/14

    摘要： The present invention relates to a process for performing a controlled hydrolysis and condensation of an epoxy-functional silane of the general formula I R1-SiR′m(OR)3-m (I) in which R1 is a (III) or (IV) group and R, R′ and R″ groups are the same or different and are each hydrogen (H) or a linear, branched or cyclic, optionally substituted alkyl group having from 1 to 6 carbon atoms, A and A′ groups are the same or different and are each a bivalent alkyl group having from 1 to 10 carbon atoms, R2 groups are the same or different and R2 is a linear, branched or cyclic, optionally substituted alkyl group having from 1 to 20 carbon atoms, and m is 0 or 1, and optionally of at least one further organofunctional silane of the general formula II R2-SiR′n(OR)3-n (II) in which R2 is an organofunctional group as already defined above, R′ is methyl, R groups are each independently hydrogen or a linear, branched or cyclic alkyl group having from 1 to 6 carbon atoms and n is 0 or 1, where from 0.001 to ≦5 mol of water is used per mole of alkoxy function of the silanes used, no further hydrolysis or condensation catalyst is used apart from boric acid as the hydrolysis catalyst and condensation component, and the condensates formed in the reaction are based on Si—O—B— and/or Si—O—Si bonds.

    摘要翻译： 本发明涉及一种通式I R 1 -Si R'm（OR）3-m（I）的环氧官能硅烷进行受控水解和缩合的方法，其中R 1是（III）或（IV ）基团，R，R'和R“基团相同或不同，各自为氢（H）或具有1至6个碳原子的直链，支链或环状，任选取代的烷基，A和A'基团为 相同或不同，各自为具有1至10个碳原子的二价烷基，R 2基团相同或不同，并且R 2为具有1至20个碳原子的直链，支链或环状的任选取代的烷基，m为 0或1，以及任选地至少一种另外的通式为R 2 -SiR'n（OR）3-n（II）的有机官能硅烷，其中R 2是如上定义的有机官能团，R'是甲基，R 基团各自独立地为氢或具有1至6个碳原子且n为0或1，w的直链，支链或环状烷基 这里为0.001至＆lt; nlE;每摩尔使用的硅烷的烷氧基官能度使用5摩尔的水，除了作为水解催化剂和缩合组分的硼酸之外不再使用进一步的水解或缩合催化剂，反应中形成的缩合物 基于Si-O-B和/或Si-O-Si键。

    PROCESS FOR CONTROLLED HYDROLYSIS AND CONDENSATION OF EPOXY-FUNCTIONAL ORGANOSILANES AND THE COCONDENSATION THEREOF WITH FURTHER ORGANOFUNCTIONAL ALKOXYSILANES
    10.
    发明申请
    PROCESS FOR CONTROLLED HYDROLYSIS AND CONDENSATION OF EPOXY-FUNCTIONAL ORGANOSILANES AND THE COCONDENSATION THEREOF WITH FURTHER ORGANOFUNCTIONAL ALKOXYSILANES 有权
    环氧官能有机物的控制水解和缩合方法及其与有机官能烷氧基化合物的共聚

    公开(公告)号：US20100191001A1

    公开(公告)日：2010-07-29

    申请号：US12673390

    申请日：2008-06-17

    申请人： Christian Wassmer ,  Burkhard Standke ,  Irene Lippert ,  Peter Jenkner

    发明人： Christian Wassmer ,  Burkhard Standke ,  Irene Lippert ,  Peter Jenkner

    IPC分类号： C07D303/02 ,  C07F7/02

    CPC分类号： C08G77/08 ,  C08G77/14

    摘要： The present invention relates to a process for performing a controlled hydrolysis and condensation of an epoxy-functional silane of the general formula I R1-SiR′m(OR)3-m (I) in which R1 is a (III) or (IV) group and R, R′ and R″ groups are the same or different and are each hydrogen (H) or a linear, branched or cyclic, optionally substituted alkyl group having from 1 to 6 carbon atoms, A and A′ groups are the same or different and are each a bivalent alkyl group having from 1 to 10 carbon atoms, R2 groups are the same or different and R2 is a linear, branched or cyclic, optionally substituted alkyl group having from 1 to 20 carbon atoms, and m is 0 or 1, and optionally of at least one further organofunctional silane of the general formula II R2-SiR′n(OR)3-n (II) in which R2 is an organofunctional group as already defined above, R′ is methyl, R groups are each independently hydrogen or a linear, branched or cyclic alkyl group having from 1 to 6 carbon atoms and n is 0 or 1, where from 0.001 to ≦5 mol of water is used per mole of alkoxy function of the silanes used, no further hydrolysis or condensation catalyst is used apart from boric acid as the hydrolysis catalyst and condensation component, and the condensates formed in the reaction are based on Si—O—B— and/or Si—O—Si bonds.

    摘要翻译： 本发明涉及一种通式I R 1 -Si R'm（OR）3-m（I）的环氧官能硅烷进行受控水解和缩合的方法，其中R 1是（III）或（IV ）基团，R，R'和R“基团相同或不同，各自为氢（H）或具有1至6个碳原子的直链，支链或环状，任选取代的烷基，A和A'基团为 相同或不同，各自为具有1至10个碳原子的二价烷基，R 2基团相同或不同，并且R 2为具有1至20个碳原子的直链，支链或环状的任选取代的烷基，m为 0或1，以及任选地至少一种另外的通式II的有机官能硅烷R2-SiR'n（OR）3-n（II），其中R2是如上定义的有机官能团，R'是甲基，R 基团各自独立地为氢或具有1至6个碳原子且n为0或1，w的直链，支链或环状烷基 这里为0.001至＆lt; nlE;每摩尔使用的硅烷的烷氧基官能度使用5摩尔的水，除了作为水解催化剂和缩合组分的硼酸之外不再使用进一步的水解或缩合催化剂，反应中形成的缩合物 基于Si-O-B和/或Si-O-Si键。