Method for producing beta type titanium alloy materials having excellent
strength and elongation
    1.
    发明授权
    Method for producing beta type titanium alloy materials having excellent strength and elongation 失效
    生产具有优异强度和伸长率的β型钛合金材料的方法

    公开(公告)号:US4799975A

    公开(公告)日:1989-01-24

    申请号:US99537

    申请日:1987-09-22

    IPC分类号: C22F1/18 C22C14/00

    CPC分类号: C22F1/183

    摘要: A .beta. type titanium alloy material is passed through processes and heating treatments of cold working--intermediate solution treatment--final cold working--final solution treatment--aging. In this process, a structure, which has been provided with strains by the cold working performed prior to the final cold working, will be changed into a recrystallized structure by carrying out the intermediate solution treatment, where uniform and fine micro substructure of dislocations, remain with grains. If such an intermediate solution-treated material is processed with a slight cold working by the final cold working and further with the solution treatment, only a recovery phenomenon progresses, and it is possible to provide such a micro substructure containing more uniform and finer dislocation network not only in grains but also in grain boundaries. Therefore, in the aging, expedition of precipitation and uniform distribution of .alpha. crystals will be realized in the grains and grain boundary regions, and intergranular cracking is difficult to take place, and alloy materials having high strength and high ductility may be produced.

    Alpha + beta or beta TITANIUM ALLOY AND METHOD FOR PRODUCTION THEREOF
    3.
    发明申请
    Alpha + beta or beta TITANIUM ALLOY AND METHOD FOR PRODUCTION THEREOF 审中-公开
    α+β或β钛合金及其生产方法

    公开(公告)号:US20140044584A1

    公开(公告)日:2014-02-13

    申请号:US14113823

    申请日:2012-04-27

    IPC分类号: C22C1/04 C22C14/00

    摘要: A titanium alloy containing copper, which cannot be realized by a conventional method, is provided, having a composition in which copper is contained in titanium with no segregation, and having improved strength and hardness. In addition a method is also provided, in which the titanium alloy is produced at lower cost than in a conventional method. The α+β or β titanium alloy contains copper at 1 to 10 mass %, has a crystal phase of β and α phase or of β phase, is formed of crystal particles not more than 100 μm, and has a copper concentration per an arbitrary specified 1 mm3 portion of the crystal phase at within ±40% compared to another arbitrary specified portion. The α+β or β titanium alloy is produced by mixing 1 to 10 mass % of copper powder and the remainder of titanium alloy powder and then pressing and forming while being heated. The method for production of the α+β or β titanium alloy has a step of mixing 1 to 10 mass % of copper powder and the remainder of titanium alloy powder and a step of pressing and forming the mixture while being heated.

    摘要翻译: 提供了含有铜的钛合金,其通过常规方法不能实现,其具有在钛中含有铜而没有偏析并且具有改善的强度和硬度的组成。 此外,还提供了一种方法,其中以比常规方法更低的成本生产钛合金。 α+β或β钛合金含有1〜10质量%的铜,具有β相和α相或β相的结晶相,由不超过100μm的晶体粒子形成,并且具有任意的铜浓度 相对于另一个任意的指定部分,指定晶体相的1mm 3部分在±40%以内。 通过混合1〜10质量%的铜粉末和剩余的钛合金粉末,然后在加热的状态下进行加压成型,生成α+β或β钛合金。 制造α+β或β钛合金的方法具有将1〜10质量%的铜粉和剩余的钛合金粉末混合的步骤,以及在加热时压制和形成混合物的步骤。

    Method for production of metal powder
    4.
    发明授权
    Method for production of metal powder 失效
    金属粉末生产工艺

    公开(公告)号:US06372015B1

    公开(公告)日:2002-04-16

    申请号:US09463563

    申请日:2000-01-27

    IPC分类号: B22F912

    CPC分类号: B22F9/28

    摘要: A process for production of metallic powder comprising contacting a metallic chloride gas with a reductive gas in a temperature range for a reducing reaction to form a metallic powder and subsequently contacting the metallic powder with an inert gas such as nitrogen gas to cool the powder, wherein the rate of cooling is 30° C. or more for temperatures from the temperature range for the reducing reaction to a temperature of 800°C. or less. The metallic powder is rapidly cooled, which results in suppression of agglomeration of particles in the metallic powder and the growth of secondary particles. Growth of particles of a metallic powder formed in a reduction process into secondary particles through agglomeration after the reduction process is suppressed, and a ultrafine metallic powder having a particle diameter of, for example, 1&mgr;m or less, can be reliably produced.

    摘要翻译: 一种金属粉末的制造方法,其特征在于,在还原反应的温度范围内使金属氯化物气体与还原性气体接触,形成金属粉末,随后使金属粉末与氮气等惰性气体接触,使粉末冷却, 对于从还原反应的温度范围到800℃的温度的温度,冷却速率为30℃以上。 或更少。 金属粉末被快速冷却,这导致抑制金属粉末中的颗粒附聚和二次颗粒的生长。 在还原处理后,通过还原过程中的附聚将在还原过程中形成的金属粉末的颗粒生长成二次颗粒,并且可以可靠地制造具有例如1μm或更小的粒径的超细金属粉末。

    Metal powder
    5.
    发明授权
    Metal powder 失效
    金属粉末

    公开(公告)号:US06447571B1

    公开(公告)日:2002-09-10

    申请号:US09508616

    申请日:2000-03-24

    IPC分类号: B22F100

    摘要: The present invention provides a metallic powder which exhibits superior sintering properties in a production of multilayer ceramic capacitors, and exhibits superior dispersion characteristics in forming of conductive pastes, thereby preventing delamination. Metallic powder produced by bringing a metallic chloride gas into contact with a reducing gas in a reducing temperature range is subjected to a surface treatment by a nonionic surfactant in a wet or dry process to obtain final metallic powder.

    摘要翻译: 本发明提供一种金属粉末,其在多层陶瓷电容器的制造中表现出优异的烧结性,并且在形成导电性糊剂时表现出优异的分散特性,从而防止分层。 通过使金属氯化物气体在还原温度范围内与还原气体接触而制造的金属粉末,通过非水性表面活性剂进行湿法或干法的表面处理,得到最终的金属粉末。

    Metal nickel powder
    6.
    发明授权
    Metal nickel powder 有权
    金属镍粉

    公开(公告)号:US06391084B1

    公开(公告)日:2002-05-21

    申请号:US09508820

    申请日:2000-03-29

    IPC分类号: B22F102

    摘要: The present invention provide metallic nickel powder in which the occurrence of delaminatoin can be prevented by providing superior sintering propreties in production processes for multilayer ceramic capacitors and by providind superior dispersion characteristics in the forming of conductive pastes. By being brought into contact with nickel chloride gas and a reducing gas at a temperature in the range of the reduction reaction, metallic nickel power is node gas and a reducing gas at a produced in which the oxigen content is 0.1 to 2.0% by weight and there is not absortion peak at wavelengths ranging from 3600 to 3700 cm−1 in infrared spectroscopy.

    摘要翻译: 本发明提供金属镍粉末,其中通过在多层陶瓷电容器的制造方法中提供优异的烧结性能并且在形成导电浆料中提供优异的分散特性,可以防止脱层的发生。 通过在还原反应范围内的温度下与氯化镍气体和还原气体接触,金属镍电力是生成的氧化物含量为0.1〜2.0重量%的节点气体和还原气体, 红外光谱中波长3600〜3700cm-1处不存在绝缘峰。

    Process for production of ultrafine nickel powder
    8.
    发明授权
    Process for production of ultrafine nickel powder 失效
    超细镍粉生产工艺

    公开(公告)号:US06500227B1

    公开(公告)日:2002-12-31

    申请号:US09720486

    申请日:2001-01-23

    IPC分类号: B22F100

    摘要: In a process for production of ultrafine nickel powder, raw material gas having a partial pressure of nickel chloride vapor within a range from 0.2 to 0.7 is fed into a reducing furnace and the nickel chloride vapor is reduced with hydrogen while flowing the raw material gas in this reducing furnace at a space velocity (SV) within a range from 0.02 to 0.07 sec−1.

    摘要翻译: 在超细镍粉的制造方法中,将氯化镍蒸汽的分压为0.2〜0.7的原料气体供给到还原炉中,在将原料气体流入的同时,将氯化镍蒸气还原, 该还原炉的空速(SV)在0.02〜0.07秒-1的范围内。

    Process for producing metal powders and apparatus for producing the same
    9.
    发明授权
    Process for producing metal powders and apparatus for producing the same 失效
    金属粉末的制造方法及其制造方法

    公开(公告)号:US06168752A

    公开(公告)日:2001-01-02

    申请号:US09117509

    申请日:1998-07-31

    IPC分类号: B22F922

    摘要: A process for producing metallic powders a chlorination step for continuously producing chloride gas of metal by reacting metal with chlorine gas, and a reduction step for continuously reducing the metallic chloride gas by reacting the metallic chloride gas produced in the chlorination step with reducing gas. Regulating the feed rate of the chlorine gas can control the feed rate of the metallic chloride gas, whereby the particle diameters of produced metal powders can be stably controlled. Thus, the invention can make the particle diameters stable and arbitrarily control the diameters in the range of 0.1 to 1.0 &mgr;m.

    摘要翻译: 一种金属粉末的制造方法,其特征在于,使金属与氯气反应生成氯化物气体的氯化气体的氯化工序,以及通过使氯化工序生成的氯化金属气体与还原气体反应而连续还原金属氯化物气体的还原工序。 调节氯气的进料速率可以控制金属氯化物气体的进料速率,从而可以稳定地控制所生产的金属粉末的粒径。 因此,本发明可使粒径稳定且任意地控制直径在0.1〜1.0μm的范围内。