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公开(公告)号：US12116311B2
公开(公告)日：2024-10-15
申请号：US18212661
申请日：2023-06-21
申请人： CORNING INCORPORATED
发明人： Matthew John Dejneka , Sinue Gomez , Guangli Hu , Charlene Marie Smith , Zhongzhi Tang , Steven Alvin Tietje
CPC分类号： C03C21/002 , C03C3/091 , C03C3/093 , C03C3/097 , C03C10/0027 , H05K5/0017 , H05K5/03
摘要： Embodiments of a glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t up to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer, are disclosed. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension in the range from about 80 MPa to about 100 MPa. In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a value at a point between the first surface and the second surface and increases from the value to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US20240166558A1
公开(公告)日：2024-05-23
申请号：US18411468
申请日：2024-01-12
申请人： Corning Incorporated
发明人： Timothy Michael Gross , Guangli Hu , Rostislav Vatchev Roussev , Charlene Marie Smith , Zhongzhi Tang , Steven Alvin Tietje
CPC分类号： C03C21/002 , C03C3/093 , C03C3/097 , C03C4/18 , C03C23/007 , C03C2204/00
摘要： A glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension of less than about 71.5/√(t) (MPa). In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a point between the first surface and the second surface and increases from the point to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US20230348322A1
公开(公告)日：2023-11-02
申请号：US18212661
申请日：2023-06-21
申请人： CORNING INCORPORATED
发明人： Matthew John Dejneka , Sinue Gomez , Guangli Hu , Charlene Marie Smith , Zhongzhi Tang , Steven Alvin Tietje
CPC分类号： C03C21/002 , C03C3/091 , C03C3/093 , C03C3/097 , C03C10/0027 , H05K5/0017 , H05K5/03
摘要： Embodiments of a glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t up to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer, are disclosed. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension in the range from about 80 MPa to about 100 MPa. In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a value at a point between the first surface and the second surface and increases from the value to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US20230097645A1
公开(公告)日：2023-03-30
申请号：US17953668
申请日：2022-09-27
申请人： Corning Incorporated
发明人： Timothy Michael Gross , Guangli Hu , Rostislav Vatchev Roussev , Charlene Marie Smith , Zhongzhi Tang , Steven Alvin Tietje
摘要： A glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension of less than about 71.5/√(t) (MPa). In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a point between the first surface and the second surface and increases from the point to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US20220212985A1
公开(公告)日：2022-07-07
申请号：US17695948
申请日：2022-03-16
申请人： CORNING INCORPORATED
发明人： Matthew John Dejneka , Sinue Gomez-Mower , Guangli Hu , Charlene Marie Smith , Zhongzhi Tang , Steven Alvin Tietje
摘要： Embodiments of a glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t up to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer, are disclosed. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension in the range from about 80 MPa to about 100 MPa. In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a value at a point between the first surface and the second surface and increases from the value to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US10710920B2
公开(公告)日：2020-07-14
申请号：US15541240
申请日：2015-12-30
申请人： CORNING INCORPORATED
发明人： Adam James Ellison , Timothy James Kiczenski , Stephanie Lynn Morris , Robert Anthony Schaut , Steven Alvin Tietje
IPC分类号： C03B32/00 , C03C21/00 , C03B25/00 , C03C3/087 , C03C23/00 , C03B25/08 , C03B25/093 , C03B27/03
摘要： According to one embodiment, a method for thermally treating glass articles may include holding a glass article at a treatment temperature equal to an annealing temperature of the glass article ±15° C. for a holding time greater than or equal to 5 minutes. Thereafter, the glass article may be cooled from the treatment temperature through a strain point of the glass article at a first cooling rate CR1 less than 0° C./min and greater than −20° C./min such that a density of the glass article is greater than or equal to 0.003 g/cc after cooling. The glass article is subsequently cooled from below the strain point at a second cooling rate CR2, wherein |CR2|>|CR1|.
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公开(公告)号：US10532947B2
公开(公告)日：2020-01-14
申请号：US16299646
申请日：2019-03-12
申请人： CORNING INCORPORATED
摘要： Embodiments of a glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than 0.7·t, comprise a tangent that is less than about −0.1 MPa/micrometers or greater than about 0.1 MPa/micrometers, are disclosed. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t). In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a point between the first surface and the second surface and increases from the point to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US20180002223A1
公开(公告)日：2018-01-04
申请号：US15708783
申请日：2017-09-19
申请人： CORNING INCORPORATED
CPC分类号： C03C21/002 , C03C3/091 , C03C3/093 , C03C3/097 , C03C10/00 , C03C10/0027 , C03C23/007
摘要： Embodiments of a glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than 0.7·t, comprise a tangent that is less than about −0.1 MPa/micrometers or greater than about 0.1 MPa/micrometers, are disclosed. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t). In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a point between the first surface and the second surface and increases from the point to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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公开(公告)号：US20170291849A1
公开(公告)日：2017-10-12
申请号：US15482213
申请日：2017-04-07
申请人： CORNING INCORPORATED
发明人： Matthew John Dejneka , Sinue Gomez , Guangli Hu , Charlene Marie Smith , Zhongzhi Tang , Steven Alvin Tietje
CPC分类号： C03C21/002 , C03C3/091 , C03C3/093 , C03C3/097 , C03C10/0027 , H05K5/0017 , H05K5/03
摘要： Embodiments of a glass-based article including a first surface and a second surface opposing the first surface defining a thickness (t) of about 3 millimeters or less (e.g., about 1 millimeter or less), and a stress profile, wherein all points of the stress profile between a thickness range from about 0·t up to 0.3·t and from greater than about 0.7·t up to t, comprise a tangent with a slope having an absolute value greater than about 0.1 MPa/micrometer, are disclosed. In some embodiments, the glass-based article includes a non-zero metal oxide concentration that varies along at least a portion of the thickness (e.g., 0·t to about 0.3·t) and a maximum central tension in the range from about 80 MPa to about 100 MPa. In some embodiments, the concentration of metal oxide or alkali metal oxide decreases from the first surface to a value at a point between the first surface and the second surface and increases from the value to the second surface. The concentration of the metal oxide may be about 0.05 mol % or greater or about 0.5 mol % or greater throughout the thickness. Methods for forming such glass-based articles are also disclosed.
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10.发明申请WHITE, OPAQUE, ß-SPODUMENE/RUTILE GLASS-CERAMIC ARTICLES AND METHODS FOR MAKING THE SAME 审中-公开白色，OPAQUE，ß-SPODUMENE / RUTILE GLASS-CERAMIC ARTICLES AND METHODS FOR MAKING THE SAME公开(公告)号：US20140057092A1
公开(公告)日：2014-02-27
申请号：US14068558
申请日：2013-10-31
申请人： CORNING INCORPORATED
发明人： George Halsey Beall , Marie Jacqueline Monique Comte , George Owen Dale , Linda Ruth Pinckney , Charlene Marie Smith , Ronald Leroy Stewart , Steven Alvin Tietje
CPC分类号： C03C14/006 , C03B20/00 , C03B32/02 , C03C3/085 , C03C3/093 , C03C10/0009 , C03C10/0027 , C03C14/00 , C03C21/002 , Y10T428/315
摘要： Crystallizable glasses, glass-ceramics, IXable glass-ceramics, and IX glass-ceramics are disclosed. The glass-ceramics exhibit β-spodumene ss as the predominant crystalline phase. These glasses and glass-ceramics, in mole %, include: 62-75 SiO2; 10.5-17 Al2O3; 5-13 Li2O; 0-4 ZnO; 0-8 MgO; 2-5 TiO2; 0-4 B2O3; 0-5 Na2O; 0-4 K2O; 0-2 ZrO2; 0-7 P2O5; 0-0.3 Fe2O3; 0-2 MnOx; and 0.05-0.2 SnO2. Additionally, these glasses and glass-ceramics exhibit the following criteria: a. a ratio: [ Li 2 O + Na 2 O + K 2 O + MgO + ZnO ] [ Al 2 O 3 + B 2 O 3 ] between 0.7 to 1.5; b. a ratio : [ TiO 2 + SnO 2 ] [ SiO 2 + B 2 O 3 ] greater than 0.04. Furthermore, the glass-ceramics exhibit an opacity ≧about 85% over the wavelength range of 400-700 nm for an about 0.8 mm thickness and colors an observer angle of 10° and a CIE illuminant F02 determined with specular reflectance included of a* between −3 and +3, b* between −6 and +6, and L* between 88 and 97.
摘要翻译： 公开了可结晶玻璃，玻璃陶瓷，IXable玻璃陶瓷和IX玻璃陶瓷。 玻璃陶瓷显示出β-锂辉石为主要结晶相。 这些玻璃和玻璃陶瓷（摩尔％）包括：62-75SiO 2; 10.5-17 Al2O3; 5-13 Li2O; 0-4 ZnO; 0-8 MgO; 2-5 TiO2; 0-4 B2O3; 0-5 Na2O; 0-4 K2O 0-2 ZrO2; 0-7 P2O5; 0-0.3 Fe2O3; 0-2 MnOx; 和0.05-0.2 SnO2。 另外，这些玻璃和玻璃陶瓷具有以下标准：a。 比例：0.7〜1.5的[Li 2 O + Na 2 O + K 2 O + MgO + ZnO] [Al 2 O 3 + B 2 O 3] b。 比例：[TiO 2 + SnO 2] [SiO 2 + B 2 O 3]大于0.04。 此外，玻璃陶瓷在400-700nm的波长范围内表现出大约85％的不透明度，约0.8mm厚度，并且观察角度为10°，CIE光源F02由包含a * 在-3和+3之间，b *在-6和+6之间，L *在88和97之间。
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