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1.发明授权
公开(公告)号：US5204198A
公开(公告)日：1993-04-20
申请号：US783590
申请日：1991-10-28
IPC分类号： G03G5/026
CPC分类号： G03G5/026
摘要： The present invention relates to a photoelectrographic element having a conductive layer in electrical contact with an acid photogenerating layer which is free of photopolymerizable materials and contains an electrically insulating binder and a nonionic sulfonic acid photogenerator. A method of forming images with this element is also disclosed.
摘要翻译： 本发明涉及一种光电元件，其具有与不含可光聚合材料并含有电绝缘粘合剂和非离子磺酸光电发生器的酸性光生电层电接触的导电层。 还公开了用该元件形成图像的方法。
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2.发明授权
公开(公告)号：US5766810A
公开(公告)日：1998-06-16
申请号：US734799
申请日：1996-10-23
CPC分类号： G03G5/0696 , C09B67/0035
摘要： Amorphous and cocrystallized unsubstituted titanyl phthalocyanine-titanyl fluorophthalocyanine compositions, preparation methods, and electrophotographic elements utilizing the compositions. The method has the steps of: admixing crude titanyl phthalocyanine and crude titanyl fluorophthalocyanine to provide a pigment mixture; increasing the amorphousness of the pigment mixture as determined by X-ray crystallography using X-radiation characteristic of Cu K.alpha. at a wavelength of 1.541 .ANG. of the Bragg angle 2.theta. to provide an amorphous pigment mixture; contacting the amorphous pigment mixture with a non-crystallizing solvent.
摘要翻译： 无定形和共结晶的未取代的氧钛酞菁 - 钛氧基酞菁组合物，制备方法和使用该组合物的电子照相元件。 该方法具有以下步骤：将粗钛酞菁和粗钛氧基酞菁混合以提供颜料混合物; 通过X射线晶体学使用在布拉格角2θ的波长为1.541的CuKα的X射线特性来确定颜料混合物的非晶性，以提供无定形颜料混合物; 使非晶颜料混合物与非结晶溶剂接触。
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3.发明授权
公开(公告)号：US5614342A
公开(公告)日：1997-03-25
申请号：US434148
申请日：1995-05-02
CPC分类号： G03G5/0696 , C09B67/0035
摘要： Cocrystallized titanyl phthalocyanine-titanyl fluorophthalocyanine compositions, preparation methods, and electrophotographic elements utilizing the compositions. The method has the steps of: admixing crude titanyl phthalocyanine and crude titanyl fluorophthalocyanine to provide a pigment mixture; increasing the amorphousness of the pigment mixture as determined by X-ray crystallography using X-radiation characteristic of Cu K.alpha. at a wavelength of 1.541 .ANG. of the Bragg angle 2.theta. to provide an amorphous pigment mixture; contacting the amorphous pigment mixture with organic solvent having a gamma.sub.c hydrogen bonding parameter of less than 8.0; and prior to the contacting, substantially excluding the amorphous pigment mixture from contact with organic solvent having a gamma.sub.c hydrogen bonding parameter greater than 9.0.
摘要翻译： 结晶的氧钛酞菁 - 钛氧基酞菁组合物，制备方法和使用该组合物的电子照相元件。 该方法具有以下步骤：将粗钛酞菁和粗钛氧基酞菁混合以提供颜料混合物; 通过X射线晶体学使用在布拉格角2θ的波长为1.541的CuKα的X射线特性来确定颜料混合物的非晶性，以提供无定形颜料混合物; 使无定形颜料混合物与具有小于8.0的gammac氢键参数的有机溶剂接触; 并且在接触之前，基本上排除非晶颜料混合物与具有大于9.0的gammac氢键参数的有机溶剂接触。
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4.发明授权Two-stage milling process for preparing cocrystals of titanyl fluorophthalocyanine and titanyl phthalocyanine, and electrophotographic element containing same 失效用于制备钛氧基酞菁和氧钛酞菁的共晶的两阶段研磨方法和含有它们的电子照相元件公开(公告)号：US07033716B2
公开(公告)日：2006-04-25
申请号：US10655388
申请日：2003-09-04
CPC分类号： C09B67/0035 , G03G5/0696
摘要： An amorphous mixture consisting essentially of TiOFPc and TiOPc and containing more than 75 weight percent of substantially chlorine-free TiOPc is produced by forming a mixture of crude crystalline TiOFPc and crude crystalline, substantially chlorine-free TiOPc that contains less than 80 weight percent TiOPc, treating the mixture under conditions effective to form a substantially amorphous mixture of TiOFPc and TiOPc containing less than 75 weight percent TiOPc, which is then treated with water, and dried. A further amount of crude crystalline, substantially chlorine-free TiOPc sufficient to form a new mixture containing more than 75 weight percent of substantially chlorine-free TiOPc is added, and the new mixture is converted to a substantially amorphous mixture of TiOFPc and TiOPc. A nanoparticulate cocrystalline composition is obtained by forming a slurry in an organic solvent of the dried substantially amorphous mixture, and wet milling the slurry to form the cocrystalline composition.
摘要翻译： 通过形成粗结晶TiOFPc和含有少于80重量％TiOPc的粗结晶，基本上无氯的TiOPc的混合物，生成基本上由TiOFPc和TiOPc组成并且含有大于75重量％的基本上无氯的TiOPc的无定形混合物， 在有效形成含有小于75重量％TiOPc的TiOFPc和TiOPc的基本无定形混合物的条件下处理混合物，然后用水处理，并干燥。 加入足量形成含有超过75重量％基本上无氯TiOPc的新混合物的粗结晶，基本上无氯的TiOPc，并将新混合物转化为基本上无定形的TiOFPc和TiOPc混合物。 通过在干燥的基本无定形混合物的有机溶剂中形成浆料，并湿法研磨浆料以形成共晶组合物，获得纳米颗粒共晶组合物。
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5.发明授权公开(公告)号：US07026084B2
公开(公告)日：2006-04-11
申请号：US10655113
申请日：2003-09-04
CPC分类号： C09B67/0085 , G03G5/0696
摘要： In a process for forming an amorphous TiOPc/TiOFPc pigment mixture containing a low concentration of TiOFPc, a mixture containing phthalonitrile and titanium tetrachloride is subjected to reaction conditions effective to form lightly chlorine-substituted crude crystalline Cl—TiOPc. The lightly chlorine-substituted crude crystalline Cl—TiOPc is combined with crude crystalline TiOFPc in a weight ratio from about 75:25 Cl—TiOPc:TiOFPc to about 99.5:0.5 Cl—TiOPc:TiOFPC to form a crude crystalline pigment mixture, which is treated under conditions effective to form a substantially amorphous pigment mixture of Cl—TiOPc and TiOFPc. The substantially amorphous mixture can subsequently be converted to a nanocrystalline Cl—TiOPc/TiOFPc pigment composition containing a low concentration of TiOFPc.
摘要翻译： 在形成含有低浓度TiOFPc的无定形TiOPc / TiOFPc颜料混合物的方法中，将含有邻苯二腈和四氯化钛的混合物进行有效形成轻氯取代的粗结晶Cl-TiOPc的反应条件。 将轻氯取代的粗结晶Cl-TiOPc与粗结晶TiOFPc以约75:25 Cl-TiOPc：TiOFPc至约99.5:0.5 Cl-TiOPc：TiOFPC的重量比组合以形成粗结晶颜料混合物，其为 在有效形成Cl-TiOPc和TiOFPc的基本上无定形的颜料混合物的条件下进行处理。 随后将基本上无定形的混合物转化成含有低浓度TiOFPc的纳米晶体Cl-TiOPc / TiOFPC颜料组合物。
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公开(公告)号：US5629418A
公开(公告)日：1997-05-13
申请号：US330396
申请日：1994-10-27
CPC分类号： C09B67/0016 , C09B67/0019 , G03G5/0696
摘要： Titanyl fluorophthalocyanines, and electrophotographic elements, and a method for preparing titanyl fluorophthalocyanine having the steps of: dissolving titanyl fluorophthalocyanine in acid to form a solution; admixing the solution and water to precipitate out amorphous titanyl fluorophthalocyanine; washing the amorphous titanyl fluorophthalocyanine until substantially all of the acid is removed; and retaining the amorphous titanyl fluorophthalocyanine under ambient conditions of wetness/dryness and temperature exclusive of conditions combining both dryness and a temperature of greater than about 50.degree. C.
摘要翻译： 钛氧基酞菁和电子照相元件，以及制备钛氧基酞菁的方法，其具有以下步骤：将钛氧基酞菁溶于酸中以形成溶液; 混合溶液和水以沉淀出无定形氧钛酞菁; 洗涤无定形氧钛酞菁直到基本上除去所有的酸; 并且在环境湿润/干燥和温度条件下保留无定形氧钛酞菁，不包括结合干燥和温度大于约50℃的条件。
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公开(公告)号：US5334477A
公开(公告)日：1994-08-02
申请号：US976099
申请日：1992-11-13
CPC分类号： G03G5/0596 , G03G13/16 , G03G5/0592 , G03G5/14791 , G03G5/14795 , G03G7/0006 , G03G7/004
摘要： A method is provided for non-electrostatically transferring dry toner particles which comprise a toner binder and have a particle size of less than 8 micrometers from the surface of an element to a receiver. The element comprises a conductive substrate and a surface layer which contains an electrically insulating polymeric binder resin matrix which comprises a block copolyester or copolycarbonate having a fluorinated polyether block and the receiver comprises a substrate having a coating of a thermoplastic addition polymer on a surface of the substrate in which the Tg of the polymer is less than approximately 10.degree. C. above the Tg of the toner binder. The method involves contacting the toner particles with the receiver which is heated to a temperature such that the temperature of the thermoplastic polymer coating on the receiver substrate during transfer is at least approximately 15.degree. C. above the Tg of the thermoplastic polymer whereby virtually all of the toner particles are transferred from the surface of the element to the thermoplastic polymer coating on the receiver substrate and the thermoplastic polymer coating is prevented from adhering to the element surface during transfer in the absence of a layer of a release agent on the thermoplastic polymer coating or the element. After transfer, the receiver is separated from the element while the temperature of the thermoplastic polymer coating is maintained above the Tg of the thermoplastic polymer.The method is particularly well suited for providing images having high resolution and low granularity from very small size toner particles.
摘要翻译： 提供了一种用于非静电转印干调色剂颗粒的方法，所述干调色剂颗粒包含调色剂粘合剂并且具有从元件表面到接收体的小于8微米的粒度。 元件包括导电基底和表面层，其包含电绝缘聚合物粘合剂树脂基质，其包含具有氟化聚醚嵌段的嵌段共聚酯或共聚碳酸酯，并且所述接收剂包括在基材表面上具有热塑性加聚物涂层的基材 基质，其中聚合物的Tg低于调色剂粘合剂的Tg以上约10℃。 该方法包括将调色剂颗粒与接收器接触，该接收器被加热到使得转移期间接收器基底上的热塑性聚合物涂层的温度比热塑性聚合物的Tg高至少约15℃， 调色剂颗粒从元件的表面转移到接收器基底上的热塑性聚合物涂层上，并且在热塑性聚合物涂层不存在剥离剂层的情况下，在转移过程中防止热塑性聚合物涂层粘附到元件表面 或元素。 转移后，将接收器与元件分离，同时热塑性聚合物涂层的温度保持在热塑性聚合物的Tg以上。 该方法特别适用于从非常小尺寸的调色剂颗粒提供具有高分辨率和低粒度的图像。
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8.发明授权Thermally assisted transfer process for transferring electrostatographic toner particles to a thermoplastic bearing receiver 失效用于将静电色调剂颗粒转移到热塑性轴承接收器的热辅助转印方法
公开(公告)号：US5358820A
公开(公告)日：1994-10-25
申请号：US976071
申请日：1992-11-13
CPC分类号： G03G7/004 , G03G13/16 , G03G5/056 , G03G9/0819
摘要： A method is provided for non-electrostatically transferring dry toner particles which comprise a toner binder and have a particle size of less than 8 micrometers from the surface of an element to a receiver. The element comprises a conductive substrate and a surface layer which contains an electrically insulating polymeric binder resin matrix which comprises a crystalline side chain polyester or a block copolyester or copolycarbonate having a crystalline side chain polyester block and the receiver comprises a substrate having a coating of a thermoplastic addition polymer on a surface of the substrate in which the Tg of the polymer is less than approximately 10.degree. C. above the Tg of the toner binder. The method involves contacting the toner particles with the receiver which is heated to a temperature such that the temperature of the thermoplastic polymer coating on the receiver substrate during transfer is at least approximately 15.degree. C. above the Tg of the thermoplastic polymer whereby virtually all of the toner particles are transferred from the surface of the element to the thermoplastic polymer coating on the receiver substrate and the thermoplastic polymer coating is prevented from adhering to the element surface during transfer in the absence of a layer of a release agent on the thermoplastic polymer coating or the element. After transfer, the receiver is separated from the element while the temperature of the thermoplastic polymer coating is maintained above the Tg of the thermoplastic polymer.
摘要翻译： 提供了一种用于非静电转印干调色剂颗粒的方法，所述干调色剂颗粒包含调色剂粘合剂并且具有从元件表面到接收体的小于8微米的粒度。 该元件包括导电基底和表面层，其包含电绝缘聚合物粘合剂树脂基质，其包含结晶侧链聚酯或具有结晶侧链聚酯嵌段的嵌段共聚酯或共聚碳酸酯，并且所述接收剂包含具有 聚合物的Tg在调色剂粘合剂的Tg以上低于约10℃的基材表面上的热塑性加成聚合物。 该方法包括将调色剂颗粒与接收器接触，该接收器被加热到使得转移期间接收器基底上的热塑性聚合物涂层的温度比热塑性聚合物的Tg高至少约15℃， 调色剂颗粒从元件的表面转移到接收器基底上的热塑性聚合物涂层上，并且在热塑性聚合物涂层不存在剥离剂层的情况下，在转移过程中防止热塑性聚合物涂层粘附到元件表面 或元素。 转移后，将接收器与元件分离，同时热塑性聚合物涂层的温度保持在热塑性聚合物的Tg以上。
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公开(公告)号：US06866902B2
公开(公告)日：2005-03-15
申请号：US10118723
申请日：2002-04-09
申请人： Jeanne E. Kaeding , Jeffrey W. Leon , Christine J. Landry-Coltrain , Alan R. Pitt , Trevor J. Wear , Gregory E. Missell , Dennis E. Smth
发明人： Jeanne E. Kaeding , Jeffrey W. Leon , Christine J. Landry-Coltrain , Alan R. Pitt , Trevor J. Wear , Gregory E. Missell , Dennis E. Smth
CPC分类号： B41M5/52 , B41M5/506 , B41M5/5218 , B41M5/5227 , B41M5/5254 , Y10T428/24802
摘要： An ink recording element is described comprising a support having thereon at least one image-receiving layer comprising polymeric particles in a polymeric binder, wherein the polymeric particle is stabilized by a hydrophobically-capped oligomeric acrylamide dispersant.
摘要翻译： 描述了一种墨水记录元件，其包括其上具有至少一个包含聚合物粘合剂中的聚合物颗粒的图像接收层的载体，其中聚合物颗粒通过疏水封端的低聚丙烯酰胺分散剂来稳定。
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公开(公告)号：US06528147B1
公开(公告)日：2003-03-04
申请号：US09608842
申请日：2000-06-30
IPC分类号： B32B300
CPC分类号： B41M5/52 , B41M5/508 , B41M5/5236 , B41M5/5254 , Y10T428/24802
摘要： An ink jet printing method, comprising the steps of: A) providing an ink jet printer that is responsive to digital data signals; B) loading the printer with an ink jet recording element comprising an opaque support having thereon an image-receiving layer comprising porous polymeric particles in a polymeric binder, the porous polymeric particles having a median diameter of less than about 1 &mgr;m and having a degree of crosslinking of about 27 mole % or greater; C) loading the printer with an ink jet ink composition; and D) printing on the ink jet recording element using the ink jet ink in response to the digital data signals.
摘要翻译： 一种喷墨打印方法，包括以下步骤：A）提供响应于数字数据信号的喷墨打印机; B）用喷墨记录元件装载打印机，所述喷墨记录元件包括其上具有不透明支架的图像接收层，所述图像接收层包括多孔 聚合物粘合剂中的聚合物颗粒，多孔聚合物颗粒的中值直径小于约1μm，交联度为约27摩尔％或更大; C）用喷墨油墨组合物装载打印机; 和D）响应于数字数据信号，使用喷墨油墨在喷墨记录元件上进行打印。
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