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公开(公告)号：US07615662B2
公开(公告)日：2009-11-10
申请号：US12001270
申请日：2007-12-11
申请人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
发明人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
IPC分类号： C07C263/00
CPC分类号： C07C263/10 , C07C265/14
摘要： Isocyanates are produced by reaction of primary amines with phosgene in the gas phase. In this process, the reaction is terminated by guiding the reaction mixture from the reaction chamber through a cooling stretch into which liquids are injected. Direct cooling takes place in the cooling stretch in one stage in two or more cooling zones connected in series.
摘要翻译： 异氰酸酯是通过伯胺与光气在气相中的反应产生的。 在该过程中，通过将反应混合物从反应室引导通过其中注入液体的冷却延伸来终止反应。 在连续串联的两个或更多个冷却区域中的一个阶段中的冷却拉伸中直接冷却。
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公开(公告)号：US07541487B2
公开(公告)日：2009-06-02
申请号：US12001235
申请日：2007-12-11
申请人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
发明人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C2601/14 , C07C265/14
摘要： An isocyanate is produced by reacting a primary amine with phosgene in the gas phase above the boiling point of the amine over an average contact time of 0.05 to 15 seconds under adiabatic conditions.
摘要翻译： 在绝热条件下，平均接触时间为0.05〜15秒，通过使伯胺与光气在高于胺沸点的气相中反应来制备异氰酸酯。
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公开(公告)号：US20080146834A1
公开(公告)日：2008-06-19
申请号：US12001235
申请日：2007-12-11
申请人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
发明人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C2601/14 , C07C265/14
摘要： An isocyanate is produced by reacting a primary amine with phosgene in the gas phase above the boiling point of the amine over an average contact time of 0.05 to 15 seconds under adiabatic conditions.
摘要翻译： 在绝热条件下，平均接触时间为0.05〜15秒，通过使伯胺与光气在高于胺沸点的气相中反应来制备异氰酸酯。
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公开(公告)号：US20080167490A1
公开(公告)日：2008-07-10
申请号：US12001270
申请日：2007-12-11
申请人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
发明人： Fritz Pohl , Klaus Biskup , Rainer Bruns , Friedhelm Steffens , Herbert Stutz
IPC分类号： C07C263/00
CPC分类号： C07C263/10 , C07C265/14
摘要： Isocyanates are produced by reaction of primary amines with phosgene in the gas phase. In this process, the reaction is terminated by guiding the reaction mixture from the reaction chamber through a cooling stretch into which liquids are injected. Direct cooling takes place in the cooling stretch in one stage in two or more cooling zones connected in series.
摘要翻译： 异氰酸酯是通过伯胺与光气在气相中的反应产生的。 在该过程中，通过将反应混合物从反应室引导通过其中注入液体的冷却延伸来终止反应。 在连续串联的两个或更多个冷却区域中的一个阶段中的冷却拉伸中直接冷却。
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公开(公告)号：US08563768B2
公开(公告)日：2013-10-22
申请号：US13382615
申请日：2010-06-26
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C01B32/80 , C07C265/14
摘要： An isocyanate is produced by reacting an amine with a stoichiometric excess of phosgene in the gas phase. This reaction is carried out at a temperature above the amine's boiling point to obtain a liquid stream containing the isocyanate and a gas stream containing hydrogen chloride and phosgene. The gas stream containing hydrogen chloride and phosgene thus produced is separated into a gas stream containing hydrogen chloride and a liquid stream containing phosgene. At least part of the liquid stream containing phosgene is then converted to a gas stream containing phosgene which gas stream is then recycled. The gaseous phosgene stream is maintained at a higher pressure than the liquid phosgene stream.
摘要翻译： 通过在气相中使胺与化学计量过量的光气反应来制备异氰酸酯。 该反应在高于胺沸点的温度下进行，得到含有异氰酸酯和含有氯化氢和光气的气流的液体流。 将由此产生的含有氯化氢和光气的气流分离成含有氯化氢的气流和含有光气的液体流。 然后将含有光气的液体物流的至少一部分转化成含有光气的气流，然后将气流再循环。 气态光气流保持在比液体光气流更高的压力下。
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公开(公告)号：US20120123152A1
公开(公告)日：2012-05-17
申请号：US13382615
申请日：2010-06-26
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C01B32/80 , C07C265/14
摘要： An isocyanate is produced by reacting an amine with a stoichiometric excess of phosgene in the gas phase. This reaction is carried out at a temperature above the amine's boiling point to obtain a liquid stream containing the isocyanate and a gas stream containing hydrogen chloride and phosgene. The gas stream containing hydrogen chloride and phosgene thus produced is separated into a gas stream containing hydrogen chloride and a liquid stream containing phosgene. At least part of the liquid stream containing phosgene is then converted to a gas stream containing phosgene which gas stream is then recycled. The gaseous phosgene stream is maintained at a higher pressure than the liquid phosgene stream.
摘要翻译： 通过在气相中使胺与化学计量过量的光气反应来制备异氰酸酯。 该反应在高于胺沸点的温度下进行，得到含有异氰酸酯和含有氯化氢和光气的气流的液体流。 将由此产生的含有氯化氢和光气的气流分离成含有氯化氢的气流和含有光气的液体流。 然后将含有光气的液体物流的至少一部分转化成含有光气的气流，然后将气流再循环。 气态光气流保持在比液体光气流更高的压力下。
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公开(公告)号：US08378140B2
公开(公告)日：2013-02-19
申请号：US12195495
申请日：2008-08-21
申请人： Herbert Stutz , Frank Diehl , Alexander Schwarz , Rainer Bruns
发明人： Herbert Stutz , Frank Diehl , Alexander Schwarz , Rainer Bruns
IPC分类号： C07C263/00
CPC分类号： C07C263/10 , C07C2601/14 , C07C265/14
摘要： Processes comprising providing an amine reactant, and reacting the amine reactant with a stream of phosgene in a reaction zone to form a product comprising a corresponding isocyanate, wherein the phosgene stream has a CO content of 0.5% by weight or more.
摘要翻译： 方法包括提供胺反应物，并使胺反应物与光气流反应在反应区中以形成包含相应的异氰酸酯的产物，其中光气流的CO含量为0.5重量％以上。
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公开(公告)号：US20090054684A1
公开(公告)日：2009-02-26
申请号：US12195495
申请日：2008-08-21
申请人： Herbert Stutz , Frank Diehl , Alexander Schwarz , Rainer Bruns
发明人： Herbert Stutz , Frank Diehl , Alexander Schwarz , Rainer Bruns
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C2601/14 , C07C265/14
摘要： Processes comprising providing an amine reactant, and reacting the amine reactant with a stream of phosgene in a reaction zone to form a product comprising a corresponding isocyanate, wherein the phosgene stream has a CO content of 0.5% by weight or more.
摘要翻译： 方法包括提供胺反应物，并使胺反应物与光气流反应在反应区中以形成包含相应的异氰酸酯的产物，其中光气流的CO含量为0.5重量％以上。
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9.发明授权
公开(公告)号：US5026789A
公开(公告)日：1991-06-25
申请号：US451387
申请日：1989-12-15
申请人： Thomas Weber , Walter Heckmann , Jurgen Mertes , Helmut Tesch , Volker Altstaedt , Wolfgang Eberle , Thomas Folda , Herbert Stutz , Hans-Gert Recker
发明人： Thomas Weber , Walter Heckmann , Jurgen Mertes , Helmut Tesch , Volker Altstaedt , Wolfgang Eberle , Thomas Folda , Herbert Stutz , Hans-Gert Recker
CPC分类号： C08L63/00 , Y10T428/31511
摘要： A curable impact modified epoxy resin mixture suitable for producing high performance composites is composed ofA. an aromatic epoxy compound,B. an amine type curing agent,C. from 10 to 40% by weight of an aromatic thermoplastic oligomer which contains reactive groups, preferably a polyether sulfone, andD. from 0.1 to 10% by weight of a high molecular weight emulsifier, preferably a phenoxy resin, an epoxy resin or a thermoplastic copolymer, which is compatible not only with the epoxy compound A but also with oligomer C.
摘要翻译： 适用于生产高性能复合材料的可固化冲击改性环氧树脂混合物由A.芳族环氧化合物，B.胺型固化剂，C组成，10至40重量％的含有反应性基团的芳族热塑性低聚物， 优选为聚醚砜，D为0.1〜10重量％的高分子量乳化剂，优选苯氧基树脂，环氧树脂或热塑性共聚物，其不仅与环氧化合物A相容，而且与低聚物C 。
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10.发明授权
公开(公告)号：US4786751A
公开(公告)日：1988-11-22
申请号：US797072
申请日：1985-11-12
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C265/04 , C07C265/10 , C07C265/12 , C07C265/14 , C08G18/10 , C08G18/72 , C08G18/74 , C08G18/76 , C09D175/00 , C07C71/00
CPC分类号： C07C265/12 , C08G18/74
摘要： Diisocyanates and isomeric mixtures of diisocyanates corresponding to the formula ##STR1## in which R.sub.1, R.sub.2, R.sub.3, m and n are as defined herein are made by phosgenating diamines corresponding to the formula ##STR2## in which R.sub.1, R.sub.2, R.sub.3, m and n are as defined herein at a temperature of from -20.degree. to 250.degree. C. These diisocyanates are particularly useful as starting materials for the production of polyurethanes by the isocyanate polyaddition process.
摘要翻译： R 1，R 2，R 3，m和n如本文所定义的对应于式“IMAGE”的二异氰酸酯的二异氰酸酯和异构体混合物通过对应于式“IMAGE”的二胺光气化制备，其中R 1，R 2，R 3，m和 n在-20℃至250℃的温度下定义。这些二异氰酸酯特别可用作通过异氰酸酯加聚方法生产聚氨酯的原料。
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