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1.发明授权公开(公告)号：US07544230B2
公开(公告)日：2009-06-09
申请号：US10792297
申请日：2004-03-04
IPC分类号： B22F9/24
CPC分类号： B22F9/24 , B22F2998/00 , B22F2999/00 , C22C1/0491 , G11B5/70605 , H01F1/066 , H01F10/123 , B22F1/0003 , B22F1/0018
摘要： The solution I is spouted from a first nozzle into a mixing chamber as a high-pressure jet stream of not less than 1 MPa and as a turbulent flow having a Reynolds number of not less than 10000 during the flow into the mixing chamber, and the solution II having a lower pressure than the solution I is spouted from a second nozzle into the mixing chamber as an orthogonal flow which intersects the solution I almost at right angles. The two solutions are mixed together and caused to react with each other, with the result that a mixed reaction solution Z containing alloy particles Z is formed.
摘要翻译： 将溶液I作为不小于1MPa的高压喷射流从第一喷嘴喷射到混合室中，并且在流入混合室期间以雷诺数不小于10000的湍流喷射， 具有比溶液I低的压力的溶液II从第二喷嘴喷射到混合室中，作为与溶液I几乎成直角相交的正交流。 将两种溶液混合在一起形成反应，结果形成含有合金粒子Z的混合反应溶液Z。
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2.发明授权Method of producing magnetic particles and reaction method using microreactor and microreactor 有权使用微反应器和微反应器制备磁性颗粒的方法和反应方法公开(公告)号：US07470308B2
公开(公告)日：2008-12-30
申请号：US11054344
申请日：2005-02-10
申请人： Fumiko Shiraishi , Seiji Sugiyama , Koukichi Waki , Yasunori Ichikawa , Tomohide Ueyama , Yasushi Hattori
发明人： Fumiko Shiraishi , Seiji Sugiyama , Koukichi Waki , Yasunori Ichikawa , Tomohide Ueyama , Yasushi Hattori
IPC分类号： B22F9/24
CPC分类号： B22F9/24 , B22F2998/00 , B33Y80/00 , G11B5/70605 , H01F1/06 , H01F10/123 , H01F10/147 , B22F1/0085 , B22F1/0018
摘要： In a method of producing magnetic particles which includes the steps of preparing alloy particles capable of forming a CuAu or Cu3Au hard magnetic ordered alloy phase and of forming magnetic particles for forming CuAu or Cu3Au magnetic particles, a plurality of solutions L1 and L2 for preparing the alloy particles are passed in a thin-plate laminar flow and diffused in the direction perpendicular to the flow direction at the contact interface of the solutions L1 and L2 in a mixing channel by using a microreactor, whereby a uniform mixing reaction is conducted in a short time.
摘要翻译： 在制造磁性粒子的方法中，包括制备能够形成CuAu或Cu3Au硬磁性有序合金相的合金粒子和形成用于形成CuAu或Cu3Au磁性粒子的磁性粒子的步骤，制备多个溶液L1和L2 合金颗粒以薄板层流通过，并通过使用微反应器在混合通道中在溶液L1和L2的接触界面处垂直于流动方向的方向上扩散，由此在短时间内进行均匀的混合反应 时间。
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3.发明申请Method of producing magnetic particles and reaction method using microreactor and microreactor 有权使用微反应器和微反应器制备磁性颗粒的方法和反应方法公开(公告)号：US20050223847A1
公开(公告)日：2005-10-13
申请号：US11054344
申请日：2005-02-10
申请人： Fumiko Shiraishi , Seiji Sugiyama , Koukichi Waki , Yasunori Ichikawa , Tomohide Ueyama , Yasushi Hattori
发明人： Fumiko Shiraishi , Seiji Sugiyama , Koukichi Waki , Yasunori Ichikawa , Tomohide Ueyama , Yasushi Hattori
CPC分类号： B22F9/24 , B22F2998/00 , B33Y80/00 , G11B5/70605 , H01F1/06 , H01F10/123 , H01F10/147 , B22F1/0085 , B22F1/0018
摘要： In a method of producing magnetic particles which includes the steps of preparing alloy particles capable of forming a CuAu or Cu3Au hard magnetic ordered alloy phase and of forming magnetic particles for forming CuAu or Cu3Au magnetic particles, a plurality of solutions L1 and L2 for preparing the alloy particles are passed in a thin-plate laminar flow and diffused in the direction perpendicular to the flow direction at the contact interface of the solutions L1 and L2 in a mixing channel by using a microreactor, whereby a uniform mixing reaction is conducted in a short time.
摘要翻译： 在制备磁性颗粒的方法中，包括以下步骤：制备能够形成CuAu或Cu 3 Au硬磁性有序合金相的合金颗粒，并形成用于形成CuAu或Cu 3的磁性颗粒 Au磁性颗粒，用于制备合金颗粒的多个溶液L 1和L 2在薄板层流中通过，并在与溶液L 1的接触界面处的流动方向垂直的方向上扩散 和L 2在混合通道中使用微反应器，从而在短时间内进行均匀的混合反应。
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公开(公告)号：US07717977B2
公开(公告)日：2010-05-18
申请号：US12330907
申请日：2008-12-09
IPC分类号： B22F9/24
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/24 , C22B3/02 , C22B3/20 , G11B5/70615 , Y02P10/234
摘要： The producing unit for continuously producing metal microparticles formed of a multicomponent alloy accompanied by the generation of a byproduct gas through an early reaction of the formation of the metal particles comprises a first mixing unit for continuously supplying and mixing a plurality of solutions for conducting the early reaction, a second mixing unit for continuously supplying another solution to the reaction liquid containing the metal microparticles formed in the early reaction and for mixing the two solutions, to introduce dissimilar metal atoms into the crystal lattices of the metal microparticles, and a gas-liquid separation unit that is installed in a midway of the pipe which is made so as to have enough length to finish the early reaction, and which continuously passes the reaction liquid to the second mixing unit from the first mixing unit, and that continuously removes the byproduct gas generated with the proceeding of the early reaction.
摘要翻译： 通过金属颗粒的形成的早期反应，连续生产由多组分合金形成的伴随产生副产物气体的金属微粒的制造单元包括：第一混合单元，用于连续地供给和混合用于进行早期的多种溶液 反应，第二混合单元，用于向包含在早期反应中形成的金属微粒的反应液中连续供给另一种溶液并混合两种溶液，以将不同的金属原子引入金属微粒的晶格中，并将气液 分离单元，其安装在管道的中途，其制造成具有足够的长度以完成早期反应，并且将反应液体从第一混合单元连续地通过第二混合单元，并且连续地除去副产物 随着早期反应的进行而产生的气体。
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公开(公告)号：US07470391B2
公开(公告)日：2008-12-30
申请号：US10975377
申请日：2004-10-29
IPC分类号： C22B3/02
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/24 , C22B3/02 , C22B3/20 , G11B5/70615 , Y02P10/234
摘要： The producing unit for continuously producing metal microparticles formed of a multicomponent alloy accompanied by the generation of a byproduct gas through an early reaction of the formation of the metal particles comprises a first mixing unit for continuously supplying and mixing a plurality of solutions for conducting the early reaction, a second mixing unit for continuously supplying another solution to the reaction liquid containing the metal microparticles formed in the early reaction and for mixing the two solutions, to introduce dissimilar metal atoms into the crystal lattices of the metal microparticles, and a gas-liquid separation unit that is installed in a midway of the pipe which is made so as to have enough length to finish the early reaction, and which continuously passes the reaction liquid to the second mixing unit from the first mixing unit, and that continuously removes the byproduct gas generated with the proceeding of the early reaction.
摘要翻译： 通过金属颗粒的形成的早期反应，连续生产由多组分合金形成的伴随产生副产物气体的金属微粒的制造单元包括：第一混合单元，用于连续地供给和混合用于进行早期的多种溶液 反应，第二混合单元，用于向包含在早期反应中形成的金属微粒的反应液中连续供给另一种溶液并混合两种溶液，以将不同的金属原子引入金属微粒的晶格中，并将气液 分离单元，其安装在管道的中途，其制造成具有足够的长度以完成早期反应，并且将反应液体从第一混合单元连续地通过第二混合单元，并且连续地除去副产物 随着早期反应的进行而产生的气体。
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公开(公告)号：US07384451B2
公开(公告)日：2008-06-10
申请号：US10975371
申请日：2004-10-29
IPC分类号： B01D19/00
CPC分类号： B01D19/0036 , B01D19/0042
摘要： When a reaction liquid is passed through a gas-liquid separation pipe having a larger volume per unit length than the volume per unit length of a pipe, a headspace part into which gas can be released is formed above the gas-liquid separation pipe, and the byproduct gas generated by the reaction changes into bubbles, moves upward in the reaction liquid, and is continuously released from a gas-liquid interface into the headspace part. While the gas is removed in the gas-liquid separation pipe, the pressure of the headspace part is controlled so as to be constant by a pressure adjustment device.
摘要翻译： 当反应液通过具有比单位长度的每单位长度的体积更大的气液分离管时，可以在气液分离管的上方形成能够释放气体的顶部空间部分， 由反应产生的副产物气体变成气泡，在反应液中向上移动，并从气 - 液界面连续释放到顶空部分。 当在气液分离管中除去气体时，顶空部分的压力通过压力调节装置被控制为恒定。
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公开(公告)号：US20050093211A1
公开(公告)日：2005-05-05
申请号：US10975377
申请日：2004-10-29
IPC分类号： B01D19/00 , B01F5/02 , B01F5/06 , B01F7/16 , B01F7/28 , B01J19/00 , B22F1/00 , B22F9/24 , C22B3/02 , C22B3/20 , G11B5/706
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/24 , C22B3/02 , C22B3/20 , G11B5/70615 , Y02P10/234
摘要： The producing unit for continuously producing metal microparticles formed of a multicomponent alloy accompanied by the generation of a byproduct gas through an early reaction of the formation of the metal particles comprises a first mixing unit for continuously supplying and mixing a plurality of solutions for conducting the early reaction, a second mixing unit for continuously supplying another solution to the reaction liquid containing the metal microparticles formed in the early reaction and for mixing the two solutions, to introduce dissimilar metal atoms into the crystal lattices of the metal microparticles, and a gas-liquid separation unit that is installed in a midway of the pipe which is made so as to have enough length to finish the early reaction, and which continuously passes the reaction liquid to the second mixing unit from the first mixing unit, and that continuously removes the byproduct gas generated with the proceeding of the early reaction.
摘要翻译： 通过金属颗粒的形成的早期反应，连续生产由多组分合金形成的伴随产生副产物气体的金属微粒的制造单元包括：第一混合单元，用于连续地供给和混合用于进行早期的多种溶液 反应，第二混合单元，用于向包含在早期反应中形成的金属微粒的反应液中连续供给另一种溶液并混合两种溶液，以将不同的金属原子引入金属微粒的晶格中，并将气液 分离单元，其安装在管道的中途，其制造成具有足够的长度以完成早期反应，并且将反应液体从第一混合单元连续地通过第二混合单元，并且连续地除去副产物 随着早期反应的进行而产生的气体。
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公开(公告)号：US20090090215A1
公开(公告)日：2009-04-09
申请号：US12330907
申请日：2008-12-09
IPC分类号： B22F9/00
CPC分类号： B82Y30/00 , B22F1/0018 , B22F9/24 , C22B3/02 , C22B3/20 , G11B5/70615 , Y02P10/234
摘要： The producing unit for continuously producing metal microparticles formed of a multicomponent alloy accompanied by the generation of a byproduct gas through an early reaction of the formation of the metal particles comprises a first mixing unit for continuously supplying and mixing a plurality of solutions for conducting the early reaction, a second mixing unit for continuously supplying another solution to the reaction liquid containing the metal microparticles formed in the early reaction and for mixing the two solutions, to introduce dissimilar metal atoms into the crystal lattices of the metal microparticles, and a gas-liquid separation unit that is installed in a midway of the pipe which is made so as to have enough length to finish the early reaction, and which continuously passes the reaction liquid to the second mixing unit from the first mixing unit, and that continuously removes the byproduct gas generated with the proceeding of the early reaction.
摘要翻译： 通过金属颗粒的形成的早期反应，连续生产由多组分合金形成的伴随产生副产物气体的金属微粒的制造单元包括：第一混合单元，用于连续地供给和混合用于进行早期的多种溶液 反应，第二混合单元，用于向包含在早期反应中形成的金属微粒的反应液中连续供给另一种溶液并混合两种溶液，以将不同的金属原子引入金属微粒的晶格中，并将气液 分离单元，其安装在管道的中途，其制造成具有足够的长度以完成早期反应，并且将反应液体从第一混合单元连续地通过第二混合单元，并且连续地除去副产物 随着早期反应的进行而产生的气体。
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公开(公告)号：US20050109211A1
公开(公告)日：2005-05-26
申请号：US10975371
申请日：2004-10-29
CPC分类号： B01D19/0036 , B01D19/0042
摘要： When a reaction liquid is passed through a gas-liquid separation pipe having a larger volume per unit length than the volume per unit length of a pipe, a headspace part into which gas can be released is formed above the gas-liquid separation pipe, and the byproduct gas generated by the reaction changes into bubbles, moves upward in the reaction liquid, and is continuously released from a gas-liquid interface into the headspace part. While the gas is removed in the gas-liquid separation pipe, the pressure of the headspace part is controlled so as to be constant by a pressure adjustment device.
摘要翻译： 当反应液通过具有比单位长度的每单位长度的体积更大的气液分离管时，可以在气液分离管的上方形成能够释放气体的顶部空间部分， 由反应产生的副产物气体变成气泡，在反应液中向上移动，并从气 - 液界面连续释放到顶空部分。 当在气液分离管中除去气体时，顶空部分的压力通过压力调节装置被控制为恒定。
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10.发明申请Reaction Method and Apparatus and Method and Apparatus for Manufacturing Chemical Substance Using the Same 审中-公开用于制造化学物质的反应方法和装置及其方法和装置公开(公告)号：US20090087683A1
公开(公告)日：2009-04-02
申请号：US11910263
申请日：2006-03-28
CPC分类号： B01J19/1856 , B01D19/0042 , B01F5/0256 , B01F15/065 , B01F2015/062 , B01J4/002 , B01J10/00 , B01J14/00 , B01J19/0066 , B01J19/008 , B01J19/10 , B01J19/1806 , B01J19/1862 , B01J19/2405 , B01J19/26 , B01J2219/00094 , B82Y25/00 , G11B5/706 , G11B5/714 , H01F1/0054 , H01F1/065 , H01F10/007
摘要： The present invention provides a reaction method for a reaction system generating gas by a reaction, comprising the steps of: providing a sealed mixing section for mixing a plurality of liquids to start a reaction and a degassing section having a gas-liquid interface for removing, from a reaction liquid, gas bubbles generated from a mixed reaction liquid, separately; and feeding the reaction liquid mixed in the mixing section to the degassing section, without being interfered by gas bubbles even in a reaction system where gas is generated by a reaction, so that it is possible to stabilize a reaction at the start of the reaction and in the progress of the reaction and stably feed liquid to a subsequent process.
摘要翻译： 本发明提供了通过反应产生气体的反应体系的反应方法，包括以下步骤：提供用于混合多种液体以开始反应的密封混合部分和具有气液界面的脱气部分， 从反应液中分离出由混合反应液产生的气泡; 以及即使在通过反应产生气体的反应系统中也将混合部分中混合的反应液体进料到脱气部分，而不会被气泡干扰，从而可以稳定反应开始时的反应， 在反应进程中并稳定地将液体进料到随后的过程中。
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