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    Intercalates and exfoliates formed with oligomers and polymers and composite materials containing same
    1.
    发明授权
    Intercalates and exfoliates formed with oligomers and polymers and composite materials containing same 失效
    用低聚物和聚合物形成的插层物和去角质物以及含有它们的复合材料

    公开(公告)号：US5552469A

    公开(公告)日：1996-09-03

    申请号：US488264

    申请日：1995-06-07

    申请人： Gary W. Beall ,  Semeon Tsipsursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipsursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： C01B33/44 ,  C08K3/34 ,  C08K9/04 ,  C11C5/00 ,  C03C10/14

    CPC分类号： C01B33/44 ,  C08K3/34 ,  C08K9/04 ,  C11C5/002

    摘要： Exfoliated layered silicate material derived from intercalates formed by contacting the layer material, e.g., a phyllosilicate, with an intercalant polymer to sorb or intercalate the polymer between adjacent platelets of the layered material. Sufficient intercalant polymer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 10 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-45 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with a thermoplastic or thermosetting matrix polymer melt, to provide a matrix polymer/platelet nanocomposite material--the platelets being exfoliated from the intercalate.

    摘要翻译： 衍生自通过使层状材料例如页硅酸盐与嵌入聚合物接触而形成的嵌层的剥离层状硅酸盐材料在分层材料的相邻片晶之间吸附或嵌入聚合物。 在相邻的血小板之间吸附足够的嵌入聚合物以将相邻的血小板膨胀至至少约10安培（除水后测量）的间隔，高达约100安培，优选在约30-45安培的范围内， 插入物容易被剥离，例如当与热塑性或热固性基质聚合物熔体混合时，提供基质聚合物/血小板纳米复合材料 - 血小板从插层中剥离。

    Intercalates and exfoliates formed with monomeric ethers and esters; composite materials containing same methods of modifying rheology therewith
    4.
    发明授权
    Intercalates and exfoliates formed with monomeric ethers and esters; composite materials containing same methods of modifying rheology therewith 失效
    用单体醚和酯形成的插层和去角质; 含有与其一起改性流变性的相同方法的复合材料

    公开(公告)号：US06287634B1

    公开(公告)日：2001-09-11

    申请号：US08577700

    申请日：1995-12-22

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： B05D700

    CPC分类号： C08K9/04 ,  C01B33/44

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer ether and/or ester to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 Å (as measured after water removal to a maximum of 5% by weight water), up to about 100 Å and preferably in the range of about 10-45 Å, so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to combination with the organic liquid or the matrix polymer.

    摘要翻译： 通过使层状材料（例如页硅酸盐）与嵌入单体醚和/或酯接触而形成的嵌入体，以在层状材料的相邻片晶之间吸附或插入插入剂单体。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5埃的水平（在除水后测量为最多5重量％的水），至多约100埃，优选在 约10-45埃，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。 或者，插入的复合物可以在与有机液体或基质聚合物组合之前被剥离。

    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composites materials containing same and methods of modifying rheology therewith
    6.
    发明授权
    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composites materials containing same and methods of modifying rheology therewith 失效
    插层和去角质形成羟基官能团; 多羟基官能团 和芳香族化合物; 含有相同材料的复合材料以及改性流变性的方法

    公开(公告)号：US5830528A

    公开(公告)日：1998-11-03

    申请号：US654648

    申请日：1996-05-29

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： C01B33/44 ,  C08K9/04 ,  B05D7/00

    CPC分类号： C01B33/44 ,  C08K9/04

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.

    摘要翻译： 通过使分层材料例如页硅酸盐与具有羟基和/或芳环官能团的嵌入剂单体接触形成的嵌入体，以在分层材料的相邻片晶之间吸附或插入插入剂单体。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在 约10-45安士，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。 或者，插入的复合物可以在与有机液体或基质聚合物组合之前或之后剥离。

    Intercalates and exfoliates formed with monomeric carbonyl-functional organic compounds, including carboxylic and polycarboxylic acids; aldehydes; and ketones; composite materials containing same and methods of modifying rheology therewith
    7.
    发明授权
    Intercalates and exfoliates formed with monomeric carbonyl-functional organic compounds, including carboxylic and polycarboxylic acids; aldehydes; and ketones; composite materials containing same and methods of modifying rheology therewith 失效
    由单体羰基官能的有机化合物（包括羧酸和多元羧酸）形成的插层和去角质; 醛 和酮类 含有其的复合材料以及用其改性流变性的方法

    公开(公告)号：US5804613A

    公开(公告)日：1998-09-08

    申请号：US577557

    申请日：1995-12-22

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： C01B33/44 ,  C08K9/04 ,  C08K9/00 ,  C08J3/20 ,  C08K9/06 ,  C08L33/02

    CPC分类号： C08K9/04 ,  C01B33/44

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer carbonyl-functional compound and/or a carboxylic acid-functional compound to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to combination with the organic liquid or the matrix polymer.

    摘要翻译： 通过使层状材料例如页硅酸盐与嵌入单体羰基官能化合物和/或羧酸官能化合物接触而形成的插层，以在层状材料的相邻片晶之间吸附或插入插入剂单体。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在 约10-45安士，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。 或者，插入的复合物可以在与有机液体或基质聚合物组合之前被剥离。

    Viscous carrier compositions, including gels, formed with an organic liquid carrier and a layered material:polymer complex
    8.
    发明授权
    Viscous carrier compositions, including gels, formed with an organic liquid carrier and a layered material:polymer complex 失效
    粘性载体组合物，包括由有机液体载体形成的凝胶和层状材料：聚合物复合物

    公开(公告)号：US5721306A

    公开(公告)日：1998-02-24

    申请号：US525416

    申请日：1995-09-08

    申请人： Semeon Tsipursky ,  Gary W. Beall ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Semeon Tsipursky ,  Gary W. Beall ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： C01B33/44 ,  C08K3/34 ,  C08K7/00 ,  C08K9/04 ,  C08K9/08 ,  C11C5/00 ,  C08K5/05 ,  C08K5/06 ,  C08K5/10

    CPC分类号： B82Y30/00 ,  A61K8/26 ,  A61Q5/04 ,  C01B33/44 ,  C08K3/34 ,  C08K7/00 ,  C08K9/04 ,  C08K9/08 ,  C11C5/002 ,  A61K2800/56 ,  C01P2002/74 ,  C01P2004/20 ,  C01P2004/54 ,  C01P2004/64

    摘要： Intercalates formed by contacting the layer material, e.g., a phyllosilicate, with an intercalant polymer to sorb or intercalate the polymer between adjacent platelets of the layered material. Sufficient intercalant polymer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 50 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex is combined with an organic liquid into an unexpectedly viscous carrier material, for delivery of the carrier material, or for delivery of an active compound, e.g., a pharmaceutical, or cosmetic, or lubricant, e.g., food guide lubricants dissolved or dispersed in the carrier material. Alternatively, the intercalated complex can be exfoliated prior to combination with the organic liquid.

    摘要翻译： 通过使层状材料例如页硅酸盐与嵌入聚合物接触而形成的插层，以在层状材料的相邻片晶之间吸附或嵌入聚合物。 在相邻的血小板之间吸附足够的嵌入聚合物以使相邻的血小板膨胀至至少约50安培的水平（在除水至最多5重量％水之后测量），高达约100安培，优选在 约10-45安士，使得插入物容易被剥离成单独的血小板。 插入的络合物与有机液体结合成意外粘稠的载体材料，用于递送载体材料，或用于递送活性化合物，例如药物或化妆品或润滑剂，例如溶解或分散的食品导向剂润滑剂 在载体材料中。 或者，插入的复合物可以在与有机液体组合之前被剥离。

    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith
    9.
    发明授权
    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith 有权
    插层和去角质形成羟基官能团; 多羟基官能团 和芳香族化合物; 含有其的复合材料以及用其改性流变性的方法

    公开(公告)号：US6126734A

    公开(公告)日：2000-10-03

    申请号：US158490

    申请日：1998-09-22

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： C01B33/44 ,  C08K9/04 ,  B05D7/00

    CPC分类号： C01B33/44 ,  C08K9/04

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.

    摘要翻译： 通过使分层材料例如页硅酸盐与具有羟基和/或芳环官能团的嵌入剂单体接触形成的嵌入体，以在分层材料的相邻片晶之间吸附或插入插入剂单体。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在 约10-45安士，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。 或者，插入的复合物可以在与有机液体或基质聚合物组合之前或之后剥离。