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公开(公告)号:US07368512B2
公开(公告)日:2008-05-06
申请号:US10752290
申请日:2004-09-14
IPC分类号: C08F283/04
CPC分类号: G01N33/582 , Y10T436/17 , Y10T436/201666
摘要: A method of detecting unreacted termini within a dendritic structure is achieved by exposing a dendrimer to a single generating compound capable of bonding to and tagging a deprotected but uncoupled termini. A signal generated by the signal generating compound to an otherwise uncoupled termini provides detection of the unreacted termini.
摘要翻译: 通过将树状聚合物暴露于能够结合去标记但未偶联的末端的单一生成化合物,可以检测树突状结构内未反应的末端的方法。 由信号产生化合物产生的信号到另一个非耦合终端的信号提供对未反应末端的检测。
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公开(公告)号:US20050008571A1
公开(公告)日:2005-01-13
申请号:US10752290
申请日:2004-09-14
申请人: George Newkome , Charles Moorefield , Claus Weis
发明人: George Newkome , Charles Moorefield , Claus Weis
CPC分类号: G01N33/582 , Y10T436/17 , Y10T436/201666
摘要: A method of detecting unreacted termini within a dendritic structure is achieved by exposing a dendrimer to a single generating compound capable of bonding to and tagging a deprotected but uncoupled termini. A signal generated by the signal generating compound to an otherwise uncoupled termini provides detection of the unreacted termini.
摘要翻译: 通过将树状聚合物暴露于能够结合去标记但未偶联的末端的单一生成化合物,可以检测树突状结构内未反应的末端的方法。 由信号产生化合物产生的信号到另一个非耦合终端的信号提供对未反应末端的检测。
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公开(公告)号:US20050101744A1
公开(公告)日:2005-05-12
申请号:US10462397
申请日:2003-06-16
IPC分类号: C07C205/51 , C07C229/24 , C07C233/63 , C07C237/22 , C08G83/00 , C08L77/00
CPC分类号: C08G83/003 , C07C201/12 , C07C205/51 , C07C227/04 , C07C229/24 , C07C231/02 , C07C233/63 , C07C237/22 , C07C237/24 , C07C2603/74
摘要: A method for forming cascade polymers specifically utilizing the amine monomer of the formula The monomer is made by initially reacting nitromethane and CH2═CHCO2-TBu by nucleophilic addition to form the triester nitrotrialkanoate of the formula and then reducing the nitrosubstituent to afford the said amine monomer.
摘要翻译: 用于形成特别利用下式的胺单体的级联聚合物的方法单体通过首先通过亲核加成使硝基甲烷和CH 2 -CHCO 2 -TBu反应形成 然后将亚硝基取代基还原,得到所述胺单体。
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公开(公告)号:US20070142663A1
公开(公告)日:2007-06-21
申请号:US11698422
申请日:2007-01-26
IPC分类号: C07C227/18
CPC分类号: C08G83/003 , C07C201/12 , C07C205/51 , C07C227/04 , C07C229/24 , C07C231/02 , C07C233/63 , C07C237/22 , C07C237/24 , C07C2603/74
摘要: A method for forming cascade polymers specifically utilizing the amine monomer of the formula The monomer is made by initially reacting nitromethane and CH2═CHCO2-TBu by nucleophilic addition to form the triester nitrotrialkanoate of the formula and then reducing the nitrosubstituent to afford the said amine monomer.
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公开(公告)号:US20050106068A1
公开(公告)日:2005-05-19
申请号:US10716310
申请日:2003-11-18
申请人: Abdul Malik , Abuzar Kabir , George Newkome , Kyung Yoo
发明人: Abdul Malik , Abuzar Kabir , George Newkome , Kyung Yoo
IPC分类号: B01J20/286 , B01J20/291 , G01N30/02
CPC分类号: B01J20/28047 , B01J20/286 , B01J20/291 , B01J20/3261 , B01J20/3272 , B01J2220/54 , B01J2220/84 , B01J2220/86
摘要: The present invention provides for a capillary column including a tube structure having an inner surface and a sol-gel substrate bonded to a dendrimer substrate to form a sol-gel dendrimer matrix that bonds to a portion of the inner surface of the tube structure to form a surface-bonded stationary phase coating thereon. The present invention additionally provides for a capillary column including a tube structure having an inner surface, a stationary phase coating attached to a portion of the inner surface, and a dendrimer moiety bonded to the stationary phase coating. Further, a sol-gel dendrimer coated apparatus including a structure having a surface and a sol-gel substrate bonded to a dendrimer substrate to form a sol-gel dendrimer matrix coating the surface thereon is provided. The present invention also provides for a one-step method for making and preparing a column and a method of making the sol-gel and dendrimer solution.
摘要翻译: 本发明提供了一种毛细管柱,其包括具有内表面的管结构和与树枝状聚合物基底结合的溶胶 - 凝胶基质,以形成结合到管结构的内表面的一部分的溶胶 - 凝胶树状聚合物基质以形成 表面粘结固定相涂层。 本发明另外提供了一种毛细管柱,其包括具有内表面的管结构,附着到内表面的一部分的固定相涂层和结合到固定相涂层的树枝状聚合物部分。 此外,提供了一种溶胶 - 凝胶树状聚合物涂覆设备,其包括具有表面的结构和与树枝状聚合物基底结合的溶胶 - 凝胶基质,以形成涂覆其表面的溶胶 - 凝胶树枝状大分子基质。 本发明还提供制备和制备柱的一步法和制备溶胶 - 凝胶和树枝状大分子溶液的方法。
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