公开(公告)号：US20080217232A1

公开(公告)日：2008-09-11

申请号：US12044306

申请日：2008-03-07

申请人： Gerard HOTIER ,  Philibert Leflaive ,  Sylvain Louret ,  Frederic Augier

发明人： Gerard HOTIER ,  Philibert Leflaive ,  Sylvain Louret ,  Frederic Augier

IPC分类号： B01D15/08

CPC分类号： B01D15/1842 ,  C07C7/12 ,  C07C15/08 ,  C07C9/00

摘要： The invention concerns a simulated moving bed adsorption separation device comprising a limited number of large diameter valves. According to the invention, the device comprises a column with a plurality of sectors Sk with 2 superimposed plates Pi with a single distribution network, each sector Sk comprising an external principal bypass line Lk connected to each plate Pi of Sk via a large diameter plate valve Vi and an external secondary bypass line Mk comprising a small diameter valve VMk connected to the adjacent sector Sk−1. Each line Lk comprises a flow rate limitation means and is connected to each fluid network via a single large diameter valve. Further, the connectors of lines Lk onto the column are offset by at most 20° inside Sk to limit the volume of lines Lk, and are offset by a mean angle in the range 70° to 110° between two neighbouring sectors Sk and Sk+1 so as not to weaken the column mechanically. The plates preferably comprise panels DMEi,j with parallel segments the direction of which varies from plate to plate or per group of 2 plates.The invention also concerns a separation process using said device.

摘要翻译： 本发明涉及包含有限数量的大直径阀的模拟移动床吸附分离装置。 根据本发明，该装置包括具有多个扇区Sk的列，具有具有单个分配网络的2个叠加板Pi，每个扇区Sk包括通过大直径板阀连接到每个Sk板的Pi的外部主旁路管线Lk Vi和外部辅助旁路管线Mk，其包括连接到相邻扇区Sk-1的小直径阀VMk。 每条线路Lk包括流量限制装置，并通过单个大直径阀连接到每个流体网络。 此外，线路Lk到列上的连接器在Sk内部偏移至多20°以限制线路Lk的体积，并且被两个相邻扇区之间的平均角度偏移在70°至110°之间Sk和Sk + 1，以免机械地削弱色谱柱。 板优选地包括具有平行段的面板DMEi，j，其平行段的方向从板到板或每组2个板变化。 本发明还涉及使用所述装置的分离方法。

公开(公告)号：US20130006031A1

公开(公告)日：2013-01-03

申请号：US13495423

申请日：2012-06-13

申请人： Philibert LEFLAIVE ,  Damien LEINEKUGEL LE COCQ ,  Gerard HOTIER ,  Luc WOLFF

发明人： Philibert LEFLAIVE ,  Damien LEINEKUGEL LE COCQ ,  Gerard HOTIER ,  Luc WOLFF

IPC分类号： C07C7/12

CPC分类号： B01D15/1821 ,  C07C7/13 ,  C07C15/08

摘要： The present invention describes a novel configuration for simulated moving bed separation processes characterized by using two adsorbers each containing 12 beds, these two adsorbers functioning in parallel. This novel configuration can be used to optimize para-xylene production.

摘要翻译： 本发明描述了一种用于模拟移动床分离方法的新型结构，其特征在于使用两个各自含有12个床的吸附器，这两个吸附器平行起作用。 这种新颖的配置可用于优化对二甲苯生产。

公开(公告)号：US20100048973A1

公开(公告)日：2010-02-25

申请号：US12543091

申请日：2009-08-18

申请人： Xavier DECOODT ,  Gerard HOTIER ,  Philibert LEFLAIVE ,  Damien LEINEKUGEL LE COCQ

发明人： Xavier DECOODT ,  Gerard HOTIER ,  Philibert LEFLAIVE ,  Damien LEINEKUGEL LE COCQ

IPC分类号： C07C7/12 ,  B01D15/22

CPC分类号： B01D15/1835 ,  B01D15/1842 ,  C07C7/13 ,  C07C15/08

摘要： Process for separation of a feedstock F by adsorption in a simulated moving bed in an SMB device that comprises a zone 1 for desorption of compounds produced by extraction, a zone 2 for desorption of compounds produced with a raffinate, a zone 3 for adsorption of compounds produced by extraction, and a zone 4 that is located between the draw-off of the raffinate and the supply of the desorbent,whereby the device comprises external bypass lines Li/i+1 directly joining two successive plates Pi, Pi+, that are equipped with non-automated means for adjusting flow rate and closing means, in which the degree of opening of the restriction means of the scavenging flow rate of the bypass lines Li/i+1 is adjusted so as to obtain the best performance of the SMB.

摘要翻译： 在SMB装置的模拟移动床中通过吸附分离原料F的方法，其包括用于解吸由萃取物生产的化合物的区域1，用萃余液生产的化合物解吸区域2，用于吸附化合物的区域3 通过提取产生的区域4和位于萃余液的抽出物和解吸剂的供应之间的区域4，由此该装置包括直接连接两个连续的板Pi，Pi +的外部旁路管线Li / i + 1，其配备 用于调节旁路管线Li / i + 1的清除流量限制装置的开度的调节流量和关闭装置的非自动化装置，以获得SMB的最佳性能。

公开(公告)号：US20080269535A1

公开(公告)日：2008-10-30

申请号：US12109378

申请日：2008-04-25

申请人： Gerard HOTIER ,  Philibert Leflaive ,  Luc Wolff

发明人： Gerard HOTIER ,  Philibert Leflaive ,  Luc Wolff

IPC分类号： C07C5/22

CPC分类号： C07C7/13 ,  C07C7/14 ,  C07C15/08

摘要： The invention concerns a process for producing high purity meta-xylene, comprising a step for separation by simulated moving bed adsorption starting from an aromatic C8 feed delivering a fraction which is rich in meta-xylene and a fraction which is depleted in meta-xylene, and a step for crystallization of the meta-xylene rich fraction. The purity of the meta-xylene produced is at least 99.5%.

摘要翻译： 本发明涉及一种生产高纯度间二甲苯的方法，包括通过模拟移动床吸附分离的步骤，起始于芳烃C8进料，其中馏分富含间二甲苯和部分间二甲苯， 以及富二甲苯富集级分的结晶步骤。 产生的间二甲苯的纯度至少为99.5％。

公开(公告)号：US20110315634A1

公开(公告)日：2011-12-29

申请号：US13025316

申请日：2011-02-11

申请人： Gerard HOTIER ,  Damien Leinekugel Le Cocq

发明人： Gerard HOTIER ,  Damien Leinekugel Le Cocq

IPC分类号： B01D15/14 ,  C07C7/12

CPC分类号： B01D15/1835 ,  C07C7/12 ,  C07C15/08

摘要： A process for separating a feed F by simulated moving bed adsorption in a SMB device comprises external bypass lines Li/i+1 which directly connect two successive plates, Pi, Pi+1, the index “i” being either even or (exclusive of the foregoing) odd, along the whole length of the column, allowing said plates to be flushed, in which each of the bypass lines Li/i+1 comprises automated means for regulating the flow rate in the bypass lines, the bypass lines in certain cases being subject to a flushing flow during injection or withdrawal operations.

摘要翻译： 通过SMB装置中的模拟移动床吸附分离进料F的方法包括直接连接两个连续板Pi，Pi + 1的外部旁路管线Li / i + 1，指数“i”为偶数或（不包括 上述）奇数，沿柱的整个长度，允许所有的板被冲洗，其中每个旁路管线Li / i + 1包括用于调节旁路管线中的流量的自动装置，旁路管线在某些 在注射或抽出操作过程中，这种情况需要冲洗。