摘要:
A process for the recovery by distillation of tributyl phosphate (TBPO) from spent hydraulic oils, which are employed particularly in aircraft used for civilian air traffic.
摘要:
This invention relates to an improved process for the production of 2-phosphono-butane-1,2,4-tricarboxylic acid (PBTC) and the alkali metal salts thereof, in which process dialkyl phosphite, preferably dimethyl or diethyl phosphite, and ethene-1,2-dicarboxylic acid dialkyl ester, in particular the dimethyl or diethyl ester of maleic acid and/or fumaric acid, are initially reacted in the presence of a basic catalyst to yield a phosphonosuccinic acid tetraalkyl ester, the resultant ester is thereupon reacted without further working up with acrylic acid alkyl ester, preferably methyl or ethyl acrylate, in the presence of an alkaline catalyst and the reaction product obtained in this manner is saponified without further working up to yield PBTC or the alkali metal salts thereof. The product when mixed with bleaching lye exhibits reduced chlorine depletion.
摘要:
In the preparation of dimethylamine-borane by reacting an alkali metal or alkaline earth metal borohydride with a dimethylammonium salt, the improvement which comprises effecting the reaction in a liquid mixture comprising dimethylamine as a solvent and an additional organic solvent.
摘要:
A process is provided for the preparation of aqueous silica sols having a particle size of 27 to 72 nm. by adding fresh acidic silica sol into the reactors of a multi stage cascade reactor wherein the reactors contain aqueous solution of colloidal silica sol of a pH of 8 or above. Each successive stage of the cascade reactor is supplied with overflow from the preceding stage. Alkaline compounds, such as alkaline sodium silicate solution, alkaline potassium silicate solution, sodium hydroxide solution or potassium hydroxide solution, are introduced into the first reactor or first reactors so that a pH value in the range of 8 to 12.5 is established in the reactors.
摘要:
Process for the production and concentration of alkaline silica sols containing nonaggregated, spherical SiO.sub.2 particles with a diameter of .gtoreq.1 nm starting with SiO.sub.2 concentrations of 4-8% by weight, using microporous membrane filters.
摘要:
A process for the removal of organic impurities and dissolved salts from hydrazine hydrate and aqueous solutions thereof by distillation of the hydrazine hydrate under reduced pressure, passing the hydrazine hydrate vapor through an adsorbent, and condensing the vapor.
摘要:
The present invention relates to fluorinated carboxylic acid esters of phosphono- and phosphinocarboxylic acids containing hydroxyl and/or mercapto groups, their use as waterproofing and/or oil-repellency agents, and a method for their preparation.
摘要:
A method for manufacturing alkali chromates by the reacting of chromium ore with alkali compounds and oxidation in an atmosphere containing at least 50% oxygen is described, in which the mixture consisting of chromium ore, alkali compound and optionally leaning materials is heated in a first stage in an atmosphere containing not more than 5 vol. % oxygen to a temperature between 1000.degree. and 1 400.degree. C., and in a second stage is oxidized at a lower temperature of 900.degree. to 1 070.degree. C. with supply of an atmosphere containing at least 50% oxygen.
摘要:
The present invention relates to fluorinated carboxylic acid esters of phosphonocarboxylic acids containing acrylate and/or methacrylate groups, their use as waterproofing or oil-repellency agents, and a method for their preparation.