Desublimator for isolating sublimation products from reaction gases
    1.
    发明授权
    Desublimator for isolating sublimation products from reaction gases 失效
    用于将升华产物从反应气体中分离出来的分离器

    公开(公告)号:US4489775A

    公开(公告)日:1984-12-25

    申请号:US287783

    申请日:1981-07-28

    CPC分类号: F28F9/0138 B01D7/02

    摘要: Desublimator for isolating sublimation products from reaction gases, which consists of a closed housing and a plurality of rows of finned tubes accommodated horizontally and superposedly therein, successive superposed finned tubes being supported, and mutually spaced, with limited adjustability, by means of cage-like perforated sliding shoes surrounding them in a box-like manner, the sliding shoes of the individual finned tubes being directly stacked one above the other and resting loosely on common supporting girders anchored to the housing, and the supporting girders having, in cross-section, the outline of a triangle with its apex pointing downward.

    摘要翻译: 用于将升华产物与反应气体隔离的分离器,其由封闭的壳体和水平和重叠地容纳在其中的多排翅片管组成,连续的叠置的翅片管通过笼状支撑并相互间隔开,具有有限的可调节性 以盒状方式围绕它们的穿孔滑动鞋,各个翅片管的滑靴直接彼此堆叠堆叠并松动地搁置在锚固到壳体上的共同的支撑梁上,并且支撑梁的横截面, 三角形的轮廓,其顶点指向下方。

    Manufacture of phthalic anhydride from o-xylene or naphthalene
    7.
    发明授权
    Manufacture of phthalic anhydride from o-xylene or naphthalene 失效
    从邻二甲苯或萘制造邻苯二甲酸酐

    公开(公告)号:US4077984A

    公开(公告)日:1978-03-07

    申请号:US731005

    申请日:1976-10-08

    CPC分类号: C07C51/265 C07C51/313

    摘要: A process for the manufacture of phthalic anhydride by oxidizing o-xylene and/or naphthalene over a supported catalyst containing vanadium pentoxide and titanium dioxide, at from 350.degree. to 500.degree. C, in which the o-xylene or naphthalene is passed, with an oxygen-containing carrier gas, over the catalyst, and in which the catalyst in the first 25-50 per cent by volume of the total catalyst volume, in the direction of flow of the mixture of o-xylene or naphthalene and carrier gas, contains from 0.01 to 0.3 per cent by weight, based on titanium dioxide, of rubidium, but no phosphorus, in the active composition, while the remainder of the catalyst contains from 0.02 to 0.8 per cent by weight, based on titanium dioxide, of phosphorus, but no rubidium, in the active composition.

    摘要翻译: 一种通过在含有五氧化二钒和二氧化钛的负载型催化剂上氧化邻二甲苯和/或萘来制备邻苯二甲酸酐的方法,其中350℃至500℃,其中邻二甲苯或萘通过, 含氧载体气体在催化剂上,其中在邻二甲苯或萘和载气的混合物流动方向上,催化剂在总催化剂体积的最初25-50体积%中含有 在活性组合物中为0.01〜0.3重量%,基于二氧化钛,铷,但不含磷,而其余的催化剂含有0.02〜0.8重量%,以二氧化钛为基准的磷, 但没有铷,在活性组合物中。