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    Thiochromenone derivatives as antidotes, and herbicides containing them
    1.
    发明授权
    Thiochromenone derivatives as antidotes, and herbicides containing them 失效
    硫代苯并醌衍生物作为解毒剂，以及含有它们的除草剂

    公开(公告)号：US5378677A

    公开(公告)日：1995-01-03

    申请号：US5797

    申请日：1993-01-19

    申请人： Helmut Hagen ,  Peter Raatz ,  Helmut Walter ,  Andreas Landes

    发明人： Helmut Hagen ,  Peter Raatz ,  Helmut Walter ,  Andreas Landes

    IPC分类号： A01N25/32 ,  A01N43/18 ,  C07D335/06

    CPC分类号： C07D335/06 ,  A01N25/32 ,  A01N43/18

    摘要： Herbicidal agents containing at least one thiochromenone of the formula I ##STR1## where n is 1, 2, 3 or 4, and the radicals R.sup.3 may have different meanings when n is>1;R.sup.1 is hydrogen; cyano; halogen; substituted or unsubstituted alkyl, aryl or hetaryl;a group --XR.sup.4 or a group --COYR.sup.4, whereX is oxygen, sulfur and NR.sup.5,Y is oxygen and NR.sup.5,R.sup.4 is one of the following groups:hydrogen; formyl; alkyl; cycloalkyl; alkylcarbonyl; cycloalkylcarbonyl; alkylsulfonyl; cycloalkylsulfonyl;substituted or unsubstituted aryl, hetaryl, arylcarbonyl, hetarylcarbonyl, arylsulfonyl or hetarylsulfonyl;andR.sup.5 is hydrogen or substituted or unsubstituted alkyl, aryl or hetaryl;R.sup.2 is hydrogen; cyano; nitroso; nitro; halogen; substituted or unsubstituted alkyl, alkoxy, alkylthio, aryl or hetaryl;a group --NR.sup.4 R.sup.5 or a group --COYR.sup.4, whereY, R.sup.4 and R.sup.5 have the above meanings;R.sup.3 is hydrogen; cyano; halogen; substituted or unsubstituted alkyl, aryl or hetaryl;a group --YR.sup.4, a group --COYR.sup.4, a group --COR.sup.6 or a group --SO.sub.2 R.sup.7, whereY and R.sup.4 have the above meanings;R.sup.6 is one of the following groups:hydrogen; alkyl; cycloalkyl; substituted or unsubstituted aryl or hetaryl;andR.sup.7 is hydrogen; alkyl; cycloalkyl; substituted or unsubstituted aryl or hetaryl;or a group --NR.sup.4 R.sup.5, where R.sup.4 and R.sup.5 have the above meanings,and the plant-tolerated salts of those compounds I in which one or several of the substituents denote an acidic or basic group,and at least one herbicidal active ingredient.

    摘要翻译： 含有至少一种式I的图象的除草剂，其中n是1,2,3或4，当n大于1时，基团R 3可以具有不同的含义; R1是氢; 氰基; 卤素; 取代或未取代的烷基，芳基或杂芳基; 基团-XR4或基团-COYR4，其中X是氧，硫和NR5，Y是氧和NR5，R4是以下基团之一：氢; 甲酰基 烷基; 环烷基 烷基羰基; 环烷基羰基; 烷基磺酰基; 环烷基磺酰基; 取代或未取代的芳基，杂芳基，芳基羰基，杂芳基羰基，芳基磺酰基或杂芳基磺酰基; 和R 5是氢或取代或未取代的烷基，芳基或杂芳基; R2是氢; 氰基; 亚硝基 硝基 卤素; 取代或未取代的烷基，烷氧基，烷硫基，芳基或杂芳基; 基团-NR4R5或-COYR4基团，其中Y，R4和R5具有上述含义; R3是氢; 氰基; 卤素; 取代或未取代的烷基，芳基或杂芳基; 基团-YR4，-COYR4基团，基团-COR6或基团-SO2R7，其中Y和R4具有上述含义; R6是以下组之一：氢; 烷基; 环烷基 取代或未取代的芳基或杂芳基; 和R7是氢; 烷基; 环烷基 取代或未取代的芳基或杂芳基; 或-NR4R5基团，其中R4和R5具有上述含义，以及其中一个或几个取代基表示酸性或碱性基团的那些化合物I的植物耐受性盐和至少一种除草活性成分。

    PROCESS FOR PREPARING TRI-N-PROPYLAMINE (TPA)
    2.
    发明申请
    PROCESS FOR PREPARING TRI-N-PROPYLAMINE (TPA) 失效
    制备三-N-丙酰胺（TPA）的方法

    公开(公告)号：US20120004464A1

    公开(公告)日：2012-01-05

    申请号：US13173437

    申请日：2011-06-30

    申请人： Kevin Huyghe ,  Steven Brughmans ,  Falk Simon ,  Johann-Peter Melder ,  Peter Raatz

    发明人： Kevin Huyghe ,  Steven Brughmans ,  Falk Simon ,  Johann-Peter Melder ,  Peter Raatz

    IPC分类号： C07C211/06 ,  C07C209/60

    CPC分类号： C07C209/64 ,  Y02P20/125 ,  C07C211/06

    摘要： Process for preparing tri-n-propylamine (TPA), wherein di-n-propylamine (DPA) is reacted in the presence of hydrogen and a copper-comprising heterogeneous catalyst.An integrated process for preparing TPA, which comprises the following operations: I) reaction of n-propanol with ammonia in a reactor in the presence of an amination catalyst and optionally hydrogen to form a mixture of mono-n-propylamine, DPA and TPA, II) separation of unreacted ammonia, unreacted n-propanol and possibly hydrogen from the reaction product mixture and recirculation of at least the ammonia and propanol to the reactor in I) and also separation of the n-propylamine mixture by distillation and isolation of the TPA, III) reaction of the DPA obtained in the separation by distillation in II) in a reactor in the presence of hydrogen and a copper-comprising heterogeneous catalyst to form TPA and IV) feeding of the reactor output from III) to operation II).

    摘要翻译： 制备三正丙胺（TPA）的方法，其中二正丙胺（DPA）在氢存在下与含铜的非均相催化剂反应。 一种制备TPA的综合方法，其包括以下操作：I）在胺化催化剂和任选的氢气存在下，反应器中正丙醇与氨的反应，形成单正丙胺，DPA和TPA的混合物， II）从反应产物混合物中分离未反应的氨，未反应的正丙醇和可能的氢，并在I）中将至少氨和丙醇再循环到反应器中，并且还通过蒸馏和分离TPA分离正丙胺混合物 ，III）在反应器中在氢气和含铜的非均相催化剂的存在下在II）中在蒸馏分离中获得的DPA的反应，以形成TPA和IV）将反应器输出从III）进料到操作II）。

    Process for preparing tri-n-propylamine (TPA)
    4.
    发明授权
    Process for preparing tri-n-propylamine (TPA) 失效
    制备三正丙胺（TPA）的方法

    公开(公告)号：US08466322B2

    公开(公告)日：2013-06-18

    申请号：US13173437

    申请日：2011-06-30

    申请人： Kevin Huyghe ,  Steven Brughmans ,  Falk Simon ,  Johann-Peter Melder ,  Peter Raatz

    发明人： Kevin Huyghe ,  Steven Brughmans ,  Falk Simon ,  Johann-Peter Melder ,  Peter Raatz

    IPC分类号： C07C209/64

    CPC分类号： C07C209/64 ,  Y02P20/125 ,  C07C211/06

    摘要： Process for preparing tri-n-propylamine (TPA), wherein di-n-propylamine (DPA) is reacted in the presence of hydrogen and a copper-comprising heterogeneous catalyst. An integrated process for preparing TPA, which comprises the following operations: I) reaction of n-propanol with ammonia in a reactor in the presence of an amination catalyst and optionally hydrogen to form a mixture of mono-n-propylamine, DPA and TPA, II) separation of unreacted ammonia, unreacted n-propanol and possibly hydrogen from the reaction product mixture and recirculation of at least the ammonia and propanol to the reactor in I) and also separation of the n-propylamine mixture by distillation and isolation of the TPA, III) reaction of the DPA obtained in the separation by distillation in II) in a reactor in the presence of hydrogen and a copper-comprising heterogeneous catalyst to form TPA and IV) feeding of the reactor output from III) to operation II).

    摘要翻译： 制备三正丙胺（TPA）的方法，其中二正丙胺（DPA）在氢存在下与含铜的非均相催化剂反应。 一种制备TPA的综合方法，其包括以下操作：I）在胺化催化剂和任选的氢气存在下，反应器中正丙醇与氨的反应，形成单正丙胺，DPA和TPA的混合物， II）从反应产物混合物中分离未反应的氨，未反应的正丙醇和可能的氢，并在I）中将至少氨和丙醇再循环到反应器中，并且还通过蒸馏和分离TPA分离正丙胺混合物 ，III）在反应器中在氢气和含铜的非均相催化剂的存在下在II）中在蒸馏分离中获得的DPA的反应，以形成TPA和IV）将反应器输出从III）进料到操作II）。

    Ethylene urea displaying lasting powder flow
    7.
    发明授权
    Ethylene urea displaying lasting powder flow 有权
    乙烯尿素显示持久的粉末流动

    公开(公告)号：US08303872B2

    公开(公告)日：2012-11-06

    申请号：US12747313

    申请日：2008-12-10

    申请人： Henry Szafranski ,  Stefanie Werland ,  Peter Raatz ,  Joachim Simon

    发明人： Henry Szafranski ,  Stefanie Werland ,  Peter Raatz ,  Joachim Simon

    IPC分类号： B29B9/00 ,  C07D233/34

    CPC分类号： C07D233/34 ,  Y10T428/2982

    摘要： The present invention relates to a process for preparing ethylene urea in solid form, in which a water-comprising product melt of ethylene urea is cooled on a breaking-up apparatus and the water content of the solid obtained is from 5 to 15% by weight. Furthermore, the invention relates to ethylene urea as solid prepared by a process according to the invention, wherein the water content of the solid is from 5 to 15% by weight and the solid displays lasting powder flow.

    摘要翻译： 本发明涉及一种制备固体形式的亚乙基脲的方法，其中将乙烯脲的含水产物熔体在破碎装置上冷却，所得固体的水含量为5至15重量％ 。 此外，本发明涉及通过根据本发明的方法制备的固体的乙烯脲，其中固体的水含量为5至15重量％，并且固体显示持续的粉末流动。

    ETHYLENE UREA DISPLAYING LASTING POWDER FLOW
    8.
    发明申请
    ETHYLENE UREA DISPLAYING LASTING POWDER FLOW 有权
    乙烯尿素显示激光粉

    公开(公告)号：US20100261015A1

    公开(公告)日：2010-10-14

    申请号：US12747313

    申请日：2008-12-10

    申请人： Henry Szafranski ,  Stefanie Werland ,  Peter Raatz ,  Joachim Simon

    发明人： Henry Szafranski ,  Stefanie Werland ,  Peter Raatz ,  Joachim Simon

    IPC分类号： B32B5/16 ,  C07C273/00 ,  C07C275/20

    CPC分类号： C07D233/34 ,  Y10T428/2982

    摘要： The present invention relates to a process for preparing ethylene urea in solid form, in which a water-comprising product melt of ethylene urea is cooled on a breaking-up apparatus and the water content of the solid obtained is from 5 to 15% by weight. Furthermore, the invention relates to ethylene urea as solid prepared by a process according to the invention, wherein the water content of the solid is from 5 to 15% by weight and the solid displays lasting powder flow.

    摘要翻译： 本发明涉及一种制备固体形式的亚乙基脲的方法，其中将乙烯脲的含水产物熔体在破碎装置上冷却，所得固体的水含量为5至15重量％ 。 此外，本发明涉及通过根据本发明的方法制备的固体的乙烯脲，其中固体的水含量为5至15重量％，并且固体显示持续的粉末流动。