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6 条记录 (耗时 0.016 秒)

    Itaconamide compounds and method of preparation
    1.
    发明授权
    Itaconamide compounds and method of preparation 失效
    赖氨酰胺化合物及其制备方法

    公开(公告)号：US4480125A

    公开(公告)日：1984-10-30

    申请号：US322066

    申请日：1981-11-16

    申请人： Howard C. Haas ,  Stanley J. Jasne ,  Robert D. Moreau

    发明人： Howard C. Haas ,  Stanley J. Jasne ,  Robert D. Moreau

    IPC分类号： C08F22/38 ,  C07C102/00

    CPC分类号： C08F22/38

    摘要： The present invention relates to itaconamide compounds of the formula ##STR1## wherein R is hydrogen, alkyl, aryl, alkaryl, or aralkyl and to a method of preparing the subject compounds which comprises preparing a mixed anhydride of 2-methylenesuccinamic acid and reacting the mixed anhydride with a compound of the formula RNH.sub.2, wherein R is as previously defined, to provide the corresponding itaconamide compound.

    摘要翻译： 本发明涉及式IMAMA的其他酰胺化合物，其中R是氢，烷基，芳基，烷芳基或芳烷基，以及制备本发明化合物的方法，包括制备2-甲基琥珀酰胺酸的混合酸酐，并使混合 酸酐与式RNH2的化合物反应，其中R如前所定义，以提供相应的itaconamide化合物。

    Process for preparing polyfunctional compounds
    2.
    发明授权
    Process for preparing polyfunctional compounds 失效
    制备多官能化合物的方法

    公开(公告)号：US4227013A

    公开(公告)日：1980-10-07

    申请号：US35705

    申请日：1979-05-03

    申请人： Howard C. Haas ,  Robert D. Moreau

    发明人： Howard C. Haas ,  Robert D. Moreau

    IPC分类号： C07C317/04 ,  C07C69/34 ,  C07C102/00 ,  C07C147/14

    CPC分类号： C07C317/04

    摘要： A process for preparing polyfunctional methylene-bridged compounds is disclosed. A difunctional methylene-bridged compound having acidic protons and having the formula X--CH.sub.2 --X is reacted with an alkali metal in the presence of a disubstituted formamide to provide a methylene-bridged polyfunctional compound having the formula ##STR1## wherein X is an electron-withdrawing group such as --CONH.sub.2, --COOR or --SO.sub.2 R where R is alkyl. The polyfunctional compounds prepared by the process of the present invention are useful in the production of metal complexing or sequestering agents, acidulents, cross-linking agents for polymeric reactions and in applications where a polyfunctional compound is desirably employed.

    摘要翻译： 公开了制备多官能亚甲基桥接化合物的方法。 具有酸性质子且具有式X-CH 2 -X的双官能亚甲基桥接化合物在二取代甲酰胺存在下与碱金属反应，得到具有下式的亚甲基桥连多官能化合物，其中X是电子 - 取代基如-CONH 2，-COOR或-SO 2 R，其中R是烷基。 通过本发明的方法制备的多官能化合物可用于生产金属络合剂或螯合剂，酸性剂，聚合反应的交联剂和期望使用多官能化合物的应用。

    Preparation of 2-Methylene-1,3-propanediamide
    3.
    发明授权
    Preparation of 2-Methylene-1,3-propanediamide 失效
    2-亚甲基-1,3-丙二酰胺的制备

    公开(公告)号：US4278803A

    公开(公告)日：1981-07-14

    申请号：US109811

    申请日：1980-01-07

    申请人： Howard C. Haas ,  Stanley J. Jasne ,  Robert D. Moreau

    发明人： Howard C. Haas ,  Stanley J. Jasne ,  Robert D. Moreau

    IPC分类号： C07F7/08 ,  C07C102/00

    CPC分类号： C07F7/0818

    摘要： A process for preparing 2-methylene-1,3-propanediamide is disclosed which comprises providing a solution of a novel compound of the formula ##STR1## wherein R.sub.1, R.sub.2, and R.sub.3 can each independently be lower alkyl of from 1 to 10 carbon atoms, aryl, alkaryl, aralkyl, or halogen and X is an electron-accepting leaving group, in an inert, aprotic organic solvent, and subjecting the compound in solution to .beta.-elimination reaction conditions effective to eliminate the silyl group ##STR2## and the electron-accepting leaving group--Xfrom the compound to form a double bond between those carbon atoms to which the silyl group and the electron-accepting leaving group were bonded, thereby forming 2-methylene-1,3-propanediamide. 2-Methylene-1,3-propanediamide is useful in preparing polymers which can be used in preparing coating compositions, films, and filaments.

    摘要翻译： 公开了一种制备2-亚甲基-1,3-丙二酰胺的方法，其包括提供下式的新化合物的溶液：其中R 1，R 2和R 3可各自独立地为具有1至10个碳原子的低级烷基 ，芳基，烷芳基，芳烷基或卤素，X是电子接受离去基团，在惰性的非质子有机溶剂中，并使化合物在溶液中经受有效消除甲硅烷基的β-烯化反应条件和 电子接受离子基团-X从化合物形成在与甲硅烷基和受电子离子基团结合的那些碳原子之间的双键，从而形成2-亚甲基-1,3-丙二酰胺。 2-亚甲基-1,3-丙二酰胺可用于制备可用于制备涂料组合物，薄膜和长丝的聚合物。

    Polymerization processes and polymer compositions
    5.
    发明授权
    Polymerization processes and polymer compositions 失效
    聚合方法和聚合物组合物

    公开(公告)号：US4377654A

    公开(公告)日：1983-03-22

    申请号：US322065

    申请日：1981-11-16

    申请人： Howard C. Haas ,  Robert D. Moreau

    发明人： Howard C. Haas ,  Robert D. Moreau

    IPC分类号： C08F2/06 ,  C08K5/19 ,  C08K5/17 ,  C08L89/00 ,  C09D3/04

    CPC分类号： C08F2/06 ,  C08K5/19

    摘要： Alkyl ammonium nitrate fused salts of the formula ##STR1## wherein R.sup.1 is a substituted or unsubstituted alkyl group and R.sup.2 and R.sup.3 are each independently hydrogen or a substituted or unsubstituted alkyl group, which fused salts have melting points of up to about 125.degree. C., are disclosed for use as solvents or swelling agents for polymers and as polymerization media for the conduct of polymerization reactions.

    摘要翻译： 其中R 1是取代或未取代的烷基，R 2和R 3各自独立地为氢或取代或未取代的烷基，所述稠合盐的熔点高达约125℃。 被公开用作聚合物的溶剂或溶胀剂以及用于进行聚合反应的聚合介质。