Process for the preparation of poly-dodecalactam with high molecular weight
    3.
    发明授权
    Process for the preparation of poly-dodecalactam with high molecular weight 失效
    制备具有高分子量的聚二酯的方法

    公开(公告)号:US3564599A

    公开(公告)日:1971-02-16

    申请号:US33960164

    申请日:1964-01-23

    Applicant: INVENTA AG

    CPC classification number: C08G69/16

    Abstract: 1. A PROCESS FOR PREPARING A HIGH MOLECULAR WEIGHT POLYAMIDE CAPABLE OF AFTER-POLYMERIZATION IN AN INERT GAS ATMOSPHERE AT TEMPERTURES BELOW ITS MELTING POINT, WHICH COMPRISES POLYMERIZING W-DODECALACTAM BY HEATING UNDER EXCLUSION OF WATER AT TEMPERATURE ABOVE 300*C. IN THE PRESENCE OF A PHOSPHONIC ACID IN THE AMOUNT OF 0.05-1% BY WEIGHT CALCULATED ON THE W-DODECALACTAM.

    Continuous manufacture of fiber-forming polyesters
    4.
    发明授权
    Continuous manufacture of fiber-forming polyesters 失效
    连续制造纤维成型聚酯

    公开(公告)号:US3644483A

    公开(公告)日:1972-02-22

    申请号:US3644483D

    申请日:1967-09-12

    Applicant: INVENTA AG

    CPC classification number: C08G63/785

    Abstract: A PROCESS FOR THE CONTINOUS MANUFACTURE OF FIBERFORMING POLYESTER OF COPOLYESTER FROM DICARBOXYLIC ACIDS AND GLYCOLS WHEREIN THE FORMATION OF UNDESIRABLE DIGLYCOLS IS SUPPRESSED. THE MATERIAL ARE DIRECTLY ESTERIFIED BY INTRODUCING THEM INTO A TUBULAR REACTION CONE AT 150-250* WHEREIN A CONSIDERABLE PORTION ESTERIFIES. THE PRODUCT THEN IS INTGRODUCED INTO A PRECONDENSATE OF THE SAME INGREVACUUM OR 25-100 TORR. THE WATER OF EACTION AND FREE GLYCOL IMMEDIATELY EVAPORATE UNDER THE INFLUENCE OF THE VACUUM. AS SOON AS THIS REACTION PRODUCT ATTAINS A DEGREE OF POLYCONDENSATION FO 2-6, A PORTION THEREOF CONTINUOUSLY IS WITHDRAWN IN PROPORTION TO NEW ACID INTRODUCED. THE CONDENSATE WITHDRAWN THEN POLYCONDENSED IN THE CONVENTIONAL MANNER TO A FIBER-FORMING POLYESTER. IN A PREFERRED EMBODIMENT, A PART OF THE GLYCOL IS WITHHELD AND SUBJECTED TO A GLYCOLYSIS WITH THE PRECONDENSATE PRIOR TO ITS ENTRY INTO THE REACTION.

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