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公开(公告)号：US20060112852A1
公开(公告)日：2006-06-01
申请号：US10534298
申请日：2003-11-28
IPC分类号： C09D11/00
CPC分类号： C09D11/03 , C08K9/08 , C08K2201/014 , C09B67/0034 , C09B67/006 , C09B67/0092 , C09D7/41 , C09D17/003
摘要： Solid pigment preparations containing the following ingredients as substantial components: (A) 60-85 wt. % of at least one organic pigment, (B) 0.1-15 wt. % of at least one pigment derivative of general formula I wherein the variables have the following meanings: P is the radical of the parent substance of an organic pigment; T1, T2 independently represent a chemical bond, —CONR1— or —SO2NR1—; B1, B2 independently represent a chemical bond, C1-C8-alkylene or phenylene;X, Y independently represent similar or different groups —SO3— Ka+ or —COO— Ka+; m, n represent a rational number from 0 to 3, whereby 1=m+n=4; Ka+ H+, Li+, Na+, K+, N+R2R3 R4 R5 or a mixture of said cations; R1 represents hydrogen; C1-C4-alkyl; phenyl or naphthyl which can be respectively substituted by C1-C18-alkyl; R2, R3, R4, R5 independently represent hydrogen; C1-C30-alkyl; C3-C30-alkenyl; C5-C6-cycloalkyl which can be substituted by C1-C24-alkyl; phenyl or naphthyl which can be respectively substituted by C1-C24-alkyl or C2-C24-alkenyl; a radical of formula —[CHR6—CHR7—O]x—R8, wherein the repeating units —[CHR6—CHR7—O] for x>1 can vary; R6, R7, R8 independently represent hydrogen or C1-C6-alkyl; x is a whole number=1, and (C) 14.9 39.9 wt. % of at least one surface active additive from the group of non-ionic polyethers containing no primary amino groups, the acidic phosphoric acid esters,phosphonic acid esters, sulphuric acid esters and/or sulfonic acid esters thereof, the salts thereof and the condensation produces thereof with formaldehyde.
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公开(公告)号：US07198667B2
公开(公告)日：2007-04-03
申请号：US10534298
申请日：2003-11-28
CPC分类号： C09D11/03 , C08K9/08 , C08K2201/014 , C09B67/0034 , C09B67/006 , C09B67/0092 , C09D7/41 , C09D17/003
摘要： Solid pigment preparations containing the following ingredients as substantial components: (A) 60–85 wt. % of at least one organic pigment, (B) 0.1–15 wt. % of at least one pigment derivative of general formula I wherein the variables have the following meanings: P is the radical of the parent substance of an organic pigment; T1, T2 independently represent a chemical bond, —CONR1— or —SO2NR1—; B1, B2 independently represent a chemical bond, C1–C8-alkylene or phenylene; X, Y independently represent similar or different groups —SO3— Ka+ or —COO— Ka+; m, n represent a rational number from 0 to 3, whereby 1=m+n=4; Ka+ H+, Li+, Na+, K+, N+R2R3 R4 R5 or a mixture of said cations; R1 represents hydrogen; C1–C4-alkyl; phenyl or naphthyl which can be respectively substituted by C1–C18-alkyl; R2, R3, R4, R5 independently represent hydrogen; C1–C30-alkyl; C3–C30-alkenyl; C5–C6-cycloalkyl which can be substituted by C1–C24-alkyl; phenyl or naphthyl which can be respectively substituted by C1–C24-alkyl or C2–C24-alkenyl; a radical of formula —[CHR6—CHR7—O]x—R8, wherein the repeating units —[CHR6—CHR7—O] for x >1 can vary; R6, R7, R8 independently represent hydrogen or C1–C6-alkyl; x is a whole number =1, and (C) 14.9 39.9 wt. % of at least one surface active additive from the group of non-ionic polyethers containing no primary amino groups, the acidic phosphoric acid esters, phosphonic acid esters, sulphuric acid esters and/or sulfonic acid esters thereof, the salts thereof and the condensation produces thereof with formaldehyde.
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3.发明授权Solid pigment preparations containing anionic and non-ionic surface-active additives 有权含有阴离子和非离子表面活性添加剂的固体颜料制剂公开(公告)号：US07384473B2
公开(公告)日：2008-06-10
申请号：US10515345
申请日：2003-06-18
CPC分类号： C09D17/00 , C09B67/006 , C09B67/0063 , C09B67/0085 , C09B67/0092
摘要： Solid pigment preparations comprising as essential constituents (A) from 60% to 10% to 40% by weight of at least one anionic surface-active additive based on acid phosphoric, phosphonic, sulfuric and/or sulfonic esters of polyalkylene oxides or of reaction products of alkylene oxides with aliphatic alcohols, with phenol or naphthol, which may each be alkyl substituted if desired, with aliphatic or aromatic amines or with aliphatic carboxylic acids or carboxamides or on salts thereof, the fraction of the phosphorus-containing additive in a mixture of phosphorus- and sulfur-containing additives being not less than 50% by weight, and (C) from 0% to
摘要翻译： 含有60％至90％重量的至少一种颜料，（B）> 10％至40％重量的至少一种基于酸性磷酸的阴离子表面活性添加剂的必要组分（A）的固体颜料制剂， 聚氧化烯的膦酸，硫酸和/或磺酸酯或烯化氧与脂族醇的反应产物与苯酚或萘酚，如果需要，它们各自可以被烷基取代，与脂族或芳族胺或与脂族羧酸或羧酰胺或与 其含磷添加剂在含磷和硫的添加剂的混合物中的分数不小于50重量％，（C）0重量％至30重量％的至少一种非离子表面 活性添加剂，前提条件是当组分（C）的份数为0重量％时，组分（B）是磷酸和/或膦酸酯，并用于着色大分子有机和无机材料。
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4.发明申请Solid pigment preparations containing anionic and non-ionic surface-active additives 有权含有阴离子和非离子表面活性添加剂的固体颜料制剂公开(公告)号：US20050235876A1
公开(公告)日：2005-10-27
申请号：US10515345
申请日：2003-06-18
申请人： Hansulrich Reisacher , Andreas Stohr , Ingo Klopp , Juan Gomez
发明人： Hansulrich Reisacher , Andreas Stohr , Ingo Klopp , Juan Gomez
IPC分类号： C08K9/04 , A61K8/04 , A61K8/46 , A61K8/55 , A61K8/90 , A61Q1/02 , C08L101/00 , C09B67/00 , C09B67/20 , C09B67/46 , C09D7/12 , C09D11/00 , C09D17/00 , C09D201/00 , C08K5/00
CPC分类号： C09D17/00 , C09B67/006 , C09B67/0063 , C09B67/0085 , C09B67/0092
摘要： Solid pigment preparations comprising as essential constituents (A) from 60% to 10% to 40% by weight of at least one anionic surface-active additive based on acid phosphoric, phosphonic, sulfuric and/or sulfonic esters of polyalkylene oxides or of reaction products of alkylene oxides with aliphatic alcohols, with phenol or naphthol, which may each be alkyl substituted if desired, with aliphatic or aromatic amines or with aliphatic carboxylic acids or carboxamides or on salts thereof, the fraction of the phosphorus-containing additive in a mixture of phosphorus- and sulfur-containing additives being not less than 50% by weight, and (C) from 0% to
摘要翻译： 含有60％至90％重量的至少一种颜料，（B）> 10％至40％重量的至少一种基于酸性磷酸的阴离子表面活性添加剂的必要组分（A）的固体颜料制剂， 聚氧化烯的膦酸，硫酸和/或磺酸酯或烯化氧与脂族醇的反应产物与苯酚或萘酚，如果需要，它们各自可以被烷基取代，与脂族或芳族胺或与脂族羧酸或羧酰胺或与 其含磷添加剂在含磷和硫的添加剂的混合物中的分数不小于50重量％，（C）0重量％至30重量％的至少一种非离子表面 活性添加剂，前提条件是当组分（C）的份数为0重量％时，组分（B）是磷酸和/或膦酸酯，并用于着色大分子有机和无机材料。
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5.发明授权Solid pigment preparations containing water-soluble anionic surface-active additives that comprise carboxylate groups 有权含有包含羧酸酯基团的水溶性阴离子表面活性添加剂的固体颜料制剂公开(公告)号：US08124672B2
公开(公告)日：2012-02-28
申请号：US10531586
申请日：2003-11-11
CPC分类号： C09B67/0063
摘要： Disclosed are solid pigment preparations containing (A) 60 to 95 per weight of at least one pigment, (B) 5 to 40 percent by weight of at least one water-soluble anionic surface-active additive from the group of the homopolymers and copolymers of ethylenically unsaturated monocarboxylic acids and/or ethylenically unsaturated dicarboxylic acids which can additionally contain monopolymerized vinyl monomers having no acid function, the alkoxylation products of said homopolymers and copolymers, and the salts of said homopolymers and copolymers and the alkoxylation products thereof, and (C) 0 to 20 percent by weight of at least one nonionic surface-active polyether-based additive as essential components. Also disclosed are a method for the production thereof and methods for dyeing macromolecular organic and inorganic materials.
摘要翻译： 公开了含有（A）60至95重量％的至少一种颜料的固体颜料制剂，（B）5至40重量％的至少一种水溶性阴离子表面活性添加剂，其来自均聚物和共聚物 烯键式不饱和一元羧酸和/或烯属不饱和二羧酸，其可另外含有不具有酸性功能的单聚乙烯基单体，所述均聚物和共聚物的烷氧基化产物，以及所述均聚物和共聚物的盐及其烷氧基化产物，和（C） 0至20重量％的至少一种非离子表面活性聚醚基添加剂作为必需组分。 还公开了其生产方法和染色大分子有机和无机材料的方法。
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6.发明申请Solid pigment preparations containing water-soluble anionic surface-active additives that comprise carboxylate groups 有权含有包含羧酸酯基团的水溶性阴离子表面活性添加剂的固体颜料制剂公开(公告)号：US20060000392A1
公开(公告)日：2006-01-05
申请号：US10531586
申请日：2003-11-11
IPC分类号： C08K5/00
CPC分类号： C09B67/0063
摘要： Disclosed arm solid pigment preparations containing (A) 60 to 95 per weight of at least one pigment, (B) 5 to 40 percent by weight of at least one water-soluble anionic surface-active additive from the group of the homopolymers and copolymers of ethylenically unsaturated monocarboxylic acids and/or ethylenically unsaturated dicarboxylic acids which can additionally contain monopolymerized vinyl monomers having no acid function, the alkoxylation products of said homopolymers and copolymers, and the salts of said homopolymers and copolymers and the alkoxylation products thereof, and (C) 0 to 20 percent by weight of at least one nonionic surface-active polyether-based additive as essential components. Also disclosed are a method for the production thereof and methods for dyeing macromolecular organic and inorganic materials.
摘要翻译： 公开的臂固体颜料制剂，其包含（A）60至95重量％的至少一种颜料，（B）5至40重量％的至少一种水溶性阴离子表面活性添加剂，来自均聚物和共聚物 烯键式不饱和一元羧酸和/或烯属不饱和二羧酸，其可另外含有不具有酸性功能的单聚乙烯基单体，所述均聚物和共聚物的烷氧基化产物，以及所述均聚物和共聚物的盐及其烷氧基化产物，和（C） 0至20重量％的至少一种非离子表面活性聚醚基添加剂作为必需组分。 还公开了其生产方法和染色大分子有机和无机材料的方法。
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7.发明申请公开(公告)号：US20070232795A1
公开(公告)日：2007-10-04
申请号：US11569263
申请日：2005-05-18
申请人： Gunter-Rudolf Schroder , Jurgen Decker , Helmut Reichelt , Ingo Klopp , Armin Diefenbacher , Hartwig Voss
发明人： Gunter-Rudolf Schroder , Jurgen Decker , Helmut Reichelt , Ingo Klopp , Armin Diefenbacher , Hartwig Voss
IPC分类号： C07C309/13
CPC分类号： C09B67/0073 , C09B35/38 , C09B35/42 , C09B35/52 , C09B37/00 , C09B67/0096
摘要： A process for producing a liquid formulation of salts of sulfonated azo dyes by coupling an at least equimolar amount of diazotized aminoarylsulfonic acids I H2N—Ar—SO3H (I), where Ar is phenylene (which may be monosubstituted by sulfo) or naphthylene (which may be mono- or disubstituted by sulfo and/or monosubstituted by hydroxyl) onto the coupling product of an unsubstituted or methyl-substituted phenylenediamine with itself comprises dissolving the azo dye in a basic medium and then subjecting the solution to a nanofiltration.
摘要翻译： 通过偶联至少等摩尔量的重氮化氨基芳基磺酸I <βin-line-formula description =“In-Line Formulas”end =“lead”→> H
2 N-Ar-SO 3 H（I），<β在线公式描述=“在线式”末端=“尾”→其中Ar是亚苯基 （其可以被磺基单取代）或亚萘基（其可以被磺基和/或被羟基单取代单取代或被二取代）到未取代或甲基取代的苯二胺与其本身的偶联产物上，包括将偶氮染料溶解在碱性介质 然后对该溶液进行纳滤。 -
公开(公告)号：US07074953B2
公开(公告)日：2006-07-11
申请号：US10497519
申请日：2002-12-03
申请人： Ingo Klopp , Thomas Bogenstätter , Dirk Franke
发明人： Ingo Klopp , Thomas Bogenstätter , Dirk Franke
IPC分类号： C07C63/00
CPC分类号： C07C51/412 , C07C63/08
摘要： A process is described for preparing ammonium salts of aromatic carboxylic acids by reacting an aromatic carboxylic acid with ammonia in an aprotic solvent, which comprises carrying out the reaction in a closed vessel by continuously introducing a solution of the aromatic carboxylic acid in the aprotic solvent and passing in gaseous ammonia so that an ammonia partial pressure in the range from 0.1 to 3 bar is maintained in the gas space of the vessel, and discharging a suspension of the ammonium salt in the aprotic solvent. The process allows the preparation of ammonium salts of defined crystal size having a narrow size distribution.
摘要翻译： 描述了通过在非质子溶剂中使芳族羧酸与氨反应制备芳族羧酸的铵盐的方法，该方法包括通过在芳烃羧酸在非质子传递溶剂中连续引入溶液并在密闭容器中进行反应，以及 通过气态氨，使得在容器的气体空间中保持0.1-3巴范围内的氨分压，并将铵盐的悬浮液排出在非质子传递溶剂中。 该方法允许制备具有窄尺寸分布的限定晶体尺寸的铵盐。
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公开(公告)号：US20060042028A1
公开(公告)日：2006-03-02
申请号：US11200109
申请日：2005-08-10
IPC分类号： D06P1/00
CPC分类号： C09B67/0073 , C09B67/0046 , C09B67/0055 , D21H21/28
摘要： The present invention relates to an aqueous liquid formulation comprising 5-25% by weightof a dye composition comprising 20-100% by weightof Direct Yellow 11 or of a dye obtainable by reduction or thermal treatment of Direct Yellow 11 0-30% by weightof a blue direct dye, 0-30% by weightof a red direct dye, and 0-60% by weightof a brown direct dye all based on the dye composition, and 1-25% by weightof poly-N-vinylformamide and/or of a polymer obtained by polymerization of a mixture of one or more ethylenically unsaturated monomers and >50% by weight of N-vinylformamide based on total monomers, based on the total weight of the aqueous liquid formulation.
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公开(公告)号：US07511170B2
公开(公告)日：2009-03-31
申请号：US10487214
申请日：2002-08-29
IPC分类号： C07C63/06
CPC分类号： C07F9/1417 , B01J8/006 , B01J8/007 , B01J8/008 , B01J8/06 , B01J8/20 , B01J2208/00548 , B01J2208/0069 , B01J2219/00164 , B01J2219/00189 , C07F9/3813
摘要： A process for carrying out a liquid/solid reaction comprises a) preparing a reaction suspension in which a first reactant is present in suspended form and a second reactant is present in dissolved form in a suspension medium, where one of the reaction products is insoluble in the suspension medium, b) passing the reaction suspension through an elongated reaction zone so that the Reynolds number of the stream is less than 20,000 and c) separating off the insoluble reaction product formed. The process has the advantage that the insoluble reaction product is obtained in a readily filterable form.
摘要翻译： 进行液/固反应的方法包括：a）制备其中第一反应物以悬浮形式存在的反应悬浮液，第二反应物以溶解形式存在于悬浮介质中，其中一种反应产物不溶于 悬浮介质，b）使反应悬浮液通过细长的反应区，使得流的雷诺数小于20,000，和c）分离形成的不溶性反应产物。 该方法具有以易于过滤的形式获得不溶性反应产物的优点。
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