Method of maintaining particle size
    1.
    发明授权
    Method of maintaining particle size 有权
    保持粒径的方法

    公开(公告)号:US07608158B2

    公开(公告)日:2009-10-27

    申请号:US11374633

    申请日:2006-03-13

    Applicant: J. Ping Liu

    Inventor: J. Ping Liu

    Abstract: The present invention includes particle compositions and methods of fabrication that prevent agglomeration, thereby maintaining particle size and/or shape. Particles of the present invention were prepared after embedding chemically disordered metal-containing particles in at least one salt to form a dispersion. The dispersion of particles in salt was treated to temperatures of at least about 500 degrees Centigrade for several hours. Particles were easily recovered from the dispersion and did not agglomerate. The particles were also absent contaminating salts after performing simple washing and/or rinsing steps. Structural, compositional and/or magnetic characterizations of the metal-containing particles confirmed that they had not agglomerated. When particles with an fcc structure formed a dispersion with at least one salt, the method yielded the formation of particles having an fct structure with high magnetic anisotropy and without a substantial change in size and/or shape. When desired, however, particles shape and/or size may be changed.

    Abstract translation: 本发明包括防止附聚的颗粒组合物和制造方法,从而保持颗粒尺寸和/或形状。 在将化学无序的含金属颗粒包埋在至少一种盐中以形成分散体之后制备本发明的颗粒。 将颗粒在盐中的分散体处理至少约500摄氏度的温度数小时。 颗粒容易从分散体中回收并且不附聚。 在执行简单的洗涤和/或漂洗步骤之后,颗粒也不存在污染盐。 含金属颗粒的结构,组成和/或磁性表征证实它们没有凝聚。 当具有fcc结构的颗粒形成具有至少一种盐的分散体时,该方法产生具有高磁各向异性的fct结构并且没有大小和/或形状的实质变化的颗粒的形成。 然而,当需要时,颗粒的形状和/或尺寸可以改变。

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