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    POROSITY CONTROL WITH POLYHEDRAL OLIGOMERIC SILSESQUIOXANES
    4.
    发明申请
    POROSITY CONTROL WITH POLYHEDRAL OLIGOMERIC SILSESQUIOXANES 审中-公开
    多孔低密度硅藻土的多孔性控制

    公开(公告)号：US20100137464A1

    公开(公告)日：2010-06-03

    申请号：US12698931

    申请日：2010-02-02

    申请人： Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Jack Sammons

    发明人： Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Jack Sammons

    IPC分类号： C08J9/40

    CPC分类号： C08J3/203 ,  B82Y30/00 ,  C08J5/005 ,  C08J2201/038 ,  C08K5/549 ,  Y10T428/2995 ,  Y10T428/31663

    摘要： The use of nanostructured chemicals based on polyhedral oligomeric silsesquioxanes (POSS) and polyhedral oligomeric silicates (POS) are used to control porosity in organic and inorganic media. The precisely defined nanoscopic dimensions of this class of chemicals enables porosity to be both created (increased) or reduced (decreased) as desired. The thermal and chemical stability of the POSS/POS nanostructures and the ability of these nano-building blocks to be selectively placed or rationally assembled with both inorganic and organic material mediums allow tailoring of porosity.

    摘要翻译： 使用基于多面体低聚倍半硅氧烷（POSS）和多面体低聚硅酸盐（POS）的纳米结构化学品用于控制有机和无机介质中的孔隙率。 这类化学品的精确定义的纳米尺寸尺寸可以根据需要产生（增加）或减少（减少）孔隙度。 POSS / POS纳米结构的热和化学稳定性以及这些纳米结构单元与无机和有机材料介质选择性地放置或合理组装的能力允许调整孔隙度。

    BIOMIMETIC MATERIALS COMPRISING POLYHEDRAL OLIGOMERIC SILSESQUIOXANES
    5.
    发明申请
    BIOMIMETIC MATERIALS COMPRISING POLYHEDRAL OLIGOMERIC SILSESQUIOXANES 失效
    包含聚合物低聚硅氧烷的生物材料

    公开(公告)号：US20090176006A1

    公开(公告)日：2009-07-09

    申请号：US11379993

    申请日：2006-04-24

    申请人： Jason T. Flodin ,  Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Xuan Fu ,  Zachary Kemp

    发明人： Jason T. Flodin ,  Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Xuan Fu ,  Zachary Kemp

    IPC分类号： B05D3/00

    CPC分类号： A61L27/18 ,  A61L2400/12 ,  C08L83/04

    摘要： Nanostructured chemicals such as polyhedral oligomeric silsesquioxanes, polyhedral oligomeric silicates, and polyhedral oligomeric metallasesquioxanes are attached to living and nonliving systems as biomaterials to provide a nanoscopic topology that favors biomimetic function and cellular modulation. The resulting surface is nanoscopically thin, nanoscopically dispersed, provides systematic chemistry, surface area, surface volume, surface topology, and is essentially free of impurities, and has controllable properties through selection of composition, R groups, nanostructure size and topology. Highly shape specific and chemically tailorable nanostructured molecules are sized to biological material dimensions and are compatible with all sterilization methods.

    摘要翻译： 纳米结构化学物质​​如多面体低聚倍半硅氧烷，多面体低聚硅酸盐和多面体低聚金属氧化物倍半硅氧烷作为生物材料连接到生物和非活性体系上，以提供有利于仿生功能和细胞调节的纳米视觉拓扑结构。 所得表面纳米级薄，纳米级分散，提供系统化学，表面积，表面体积，表面拓扑，基本上不含杂质，通过选择组成，R基团，纳米结构尺寸和拓扑结构具有可控性。 高度形状的特定和化学可裁剪的纳米结构分子的大小适合生物材料尺寸，并与所有灭菌方法兼容。

    Process for the functionalization of polyhedral oligomeric silsesquioxanes
    7.
    发明授权
    Process for the functionalization of polyhedral oligomeric silsesquioxanes 失效

    公开(公告)号：US06927270B2

    公开(公告)日：2005-08-09

    申请号：US10186318

    申请日：2002-06-27

    申请人： Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Qibo Liu ,  Timothy S. Haddad

    发明人： Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Qibo Liu ,  Timothy S. Haddad

    IPC分类号： C07F7/07 ,  C08G20060101 ,  C08G77/00 ,  C08G77/06

    CPC分类号： C08G77/04 ,  C08G77/24 ,  C08G77/38

    摘要： Efficient processes have been developed for the cost effective functionalization of polyhedral oligomeric silsesquioxane-silanols (POSS-Silanols) and for the manufacture of polyfunctional polyhedral oligomeric silsesquioxanes. The processes utilize the action of bases or acids on silane coupling agents. The preferred process utilizes base to promote the silylation of POSS-Silanols of the formula [(RSiO1.5)n(R(HO)SiO1.0)m]Σ# with silane coupling agents to form POSS species with functionalized incompletely condensed nanostructures [(RSiO1.5)n(R(YSiR2O)SiO1.0)m]Σ# or functionalized completely condensed nanostructures [(RSiO1.5)n(YSiO1.5)1]Σ#. The process can alternately be conducted with acids. A second process utilizes base to alkylate POSS-Silanols with functionalized alkyl halides. A third related process utilizes base to react with silane coupling agents to form polyfunctional, fully condensed POSS species of formula [(YSiO1.5)n]Σ#. This process can also alternately be conducted under acidic conditions. Each of the processes result in new POSS compositions that can undergo additional desirable chemical reactions or which are directly suitable for polymerization or grafting into polymeric materials. POSS frameworks containing silanol and other reactive functionalities suitable for polymerizations have previously been described as valuable co-monomers in polymerizations and as feed-stocks for the preparation of a diverse number of chemical agents that are useful in polymeric materials in biological applications, and for the modification of surfaces.

    Biomimetic materials comprising polyhedral oligomeric silsesquioxanes
    8.
    发明授权
    Biomimetic materials comprising polyhedral oligomeric silsesquioxanes 失效
    包含多面体低聚倍半硅氧烷的仿生材料

    公开(公告)号：US07572872B2

    公开(公告)日：2009-08-11

    申请号：US11379993

    申请日：2006-04-24

    申请人： Jason T. Flodin ,  Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Xuan Fu ,  Zachary Kemp

    发明人： Jason T. Flodin ,  Joseph D. Lichtenhan ,  Joseph J. Schwab ,  Yi-Zhong An ,  Xuan Fu ,  Zachary Kemp

    IPC分类号： C08F30/08

    CPC分类号： A61L27/18 ,  A61L2400/12 ,  C08L83/04

    摘要： Nanostructured chemicals such as polyhedral oligomeric silsesquioxanes, polyhedral oligomeric silicates, and polyhedral oligomeric metallasesquioxanes are attached to living and nonliving systems as biomaterials to provide a nanoscopic topology that favors biomimetic function and cellular modulation. The resulting surface is nanoscopically thin, nanoscopically dispersed, provides systematic chemistry, surface area, surface volume, surface topology, and is essentially free of impurities, and has controllable properties through selection of composition, R groups, nanostructure size and topology. Highly shape specific and chemically tailorable nanostructured molecules are sized to biological material dimensions and are compatible with all sterilization methods.

    摘要翻译： 纳米结构化学物质​​如多面体低聚倍半硅氧烷，多面体低聚硅酸盐和多面体低聚金属氧化物倍半硅氧烷作为生物材料连接到生物和非活性体系上，以提供有利于仿生功能和细胞调节的纳米视觉拓扑结构。 所得表面纳米级薄，纳米级分散，提供系统化学，表面积，表面体积，表面拓扑，基本上不含杂质，通过选择组成，R基团，纳米结构尺寸和拓扑结构具有可控性。 高度形状的特定和化学可裁剪的纳米结构分子的大小适合生物材料尺寸，并与所有灭菌方法兼容。

    Process for assembly of POSS monomers
    9.
    发明授权
    Process for assembly of POSS monomers 有权
    POSS单体装配工艺

    公开(公告)号：US07485692B2

    公开(公告)日：2009-02-03

    申请号：US11371195

    申请日：2006-03-07

    申请人： Joseph J. Schwab ,  Yi-Zhong An

    发明人： Joseph J. Schwab ,  Yi-Zhong An

    IPC分类号： C08G77/08

    CPC分类号： C07F7/21

    摘要： A synthesis process for polyhedral oligomeric silsesquioxanes using phosphazene superbases to produce in high yield a low resin content, solvent free, and trace metal free monomer suitable for use in microelectronic, biological, and medical applications involving polymerization, grafting, and alloying.

    摘要翻译： 多面体低聚倍半硅氧烷的合成方法，其使用磷腈超级酶以高产率生产低树脂含量，无溶剂和不含痕量金属的单体，适用于涉及聚合，接枝和合金化的微电子，生物和医学应用。