Colloidal suspension of gold nanoparticles

    公开(公告)号:US11118108B2

    公开(公告)日:2021-09-14

    申请号:US16222687

    申请日:2018-12-17

    Abstract: Monodisperse carboxylate functionalized gold nanoparticles comprising a capping agent layer of pamoic acid and colloidal suspensions thereof are disclosed. These gold nanoparticles have an average particle size of greater than 15 nm or less than 8 nm and demonstrate significant fluorescent properties. In addition, a method for the size controlled preparation of these monodisperse carboxylate functionalized gold nanoparticles wherein pamoic acid acts as both a reducing and capping agent and wherein the size of the particles can be controlled by the pH of the process is disclosed. In addition, a method for the size controlled preparation of these monodisperse carboxylate functionalized gold nanoparticles utilizing seed mediated growth is disclosed.

    CATALYST SYSTEMS AND METHODS OF USE

    公开(公告)号:US20220266236A1

    公开(公告)日:2022-08-25

    申请号:US17185286

    申请日:2021-02-25

    Abstract: According to embodiments, methods for the production of boron-silicalite-1 are disclosed. In embodiments, the method may include combining a mineralizer agent, a templating agent, water, and boric acid in a first microwave unit; heating the first microwave unit to form a boron-zeolite; calcining the boron-zeolite to form an alkali-zeolite; combining the alkali-zeolite with ammonium nitrate to produce an ion-exchanged zeolite; heating the ion-exchanged zeolite to form a protonated zeolite; and calcining the protonated zeolite to form the boron-silicalite-1. In embodiments, the method may include combining a templating agent, water, and boric acid in a first hydrothermal unit; heating the first microwave unit to form a boron-zeolite; calcining the boron-zeolite to form an alkali-zeolite; combining the alkali-zeolite with ammonium nitrate to produce an ion-exchanged zeolite; heating the ion-exchanged zeolite to form a protonated zeolite; and calcining the protonated zeolite to form the boron-silicalite-1. The boron-silicalite-1 may be microscale or nanoscale.

    COLLOIDAL SUSPENSION OF GOLD NANOPARTICLES
    9.
    发明申请

    公开(公告)号:US20190127632A1

    公开(公告)日:2019-05-02

    申请号:US16222687

    申请日:2018-12-17

    Abstract: Monodisperse carboxylate functionalized gold nanoparticles comprising a capping agent layer of pamoic acid and colloidal suspensions thereof are disclosed. These gold nanoparticles have an average particle size of greater than 15 nm or less than 8 nm and demonstrate significant fluorescent properties. In addition, a method for the size controlled preparation of these monodisperse carboxylate functionalized gold nanoparticles wherein pamoic acid acts as both a reducing and capping agent and wherein the size of the particles can be controlled by the pH of the process is disclosed. In addition, a method for the size controlled preparation of these monodisperse carboxylate functionalized gold nanoparticles utilizing seed mediated growth is disclosed.

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