Process for producing a diaryl carbonate
    1.
    发明授权
    Process for producing a diaryl carbonate 失效
    制备碳酸二芳基酯的方法

    公开(公告)号:US5731453A

    公开(公告)日:1998-03-24

    申请号:US814089

    申请日:1997-03-10

    摘要: A diaryl carbonate with a high degree of purity is produced at a high yield by (A) subjecting (a) a diaryl oxalate and a phenol compound or (b) an alkylaryl oxalate to transesterification reaction in one or two stages in the presence of a catalyst to prepare a diaryl oxalate, while removing a by-product from the reaction system; (B) collecting the diaryl oxalate from the resultant reaction product mixture of the step (A); (C) subjecting the diaryl oxalate to a decarbonylation reaction, preferably in the presence of a phosphorous compound-containing catalyst, to convert the diaryl oxalate to a corresponding diaryl carbonate, while removing a reaction by-product comprising carbon monoxide from the reaction system; and (D) collecting the diaryl carbonate from the reaction product mixture of the step (C).

    摘要翻译: 通过(A)在(a)草酸二芳基酯和酚化合物或(b)草酸烷基芳基酯在一个或两个阶段中存在下进行酯交换反应,以高产率生产具有高纯度的碳酸二芳基酯 催化剂,以制备草酸二芳基酯,同时从反应体系中除去副产物; (B)从所得步骤(A)的反应产物混合物中收集草酸二芳基酯; (C)优选在含磷化合物的催化剂存在下使草酸二芳基酯进行脱羰反应,将草酸二芳基酯转化为相应的碳酸二芳基酯,同时从反应体系中除去包含一氧化碳的反应副产物; 和(D)从步骤(C)的反应产物混合物中收集碳酸二芳基酯。

    Process for producing a diaryl carnonate
    2.
    发明授权
    Process for producing a diaryl carnonate 失效
    生产碳酸二芳酯的方法

    公开(公告)号:US5811573A

    公开(公告)日:1998-09-22

    申请号:US988759

    申请日:1997-12-11

    摘要: A diaryl carbonate with a high degree of purity is produced at a high yield by (A) subjecting (a) a diaryl oxalate and a phenol compound or (b) an alkylaryl oxalate to transesterification reaction in one or two stages in the presence of a catalyst to prepare a diaryl oxalate, while removing a by-product from the reaction system; (B) collecting the diaryl oxalate from the resultant reaction product mixture of the step (A); (C) subjecting the diaryl oxalate to a decarbonylation reaction, preferably in the presence of a phosphorous compound-containing catalyst, to convert the diaryl oxalate to a corresponding diaryl carbonate, while removing a reaction by-product comprising carbon monoxide from the reaction system; and (D) collecting the diaryl carbonate from the reaction product mixture of the step (C).

    摘要翻译: 通过(A)在(a)草酸二芳基酯和酚化合物或(b)草酸烷基芳基酯在一个或两个阶段中存在下进行酯交换反应,以高产率生产具有高纯度的碳酸二芳基酯 催化剂,以制备草酸二芳基酯,同时从反应体系中除去副产物; (B)从所得步骤(A)的反应产物混合物中收集草酸二芳基酯; (C)优选在含磷化合物的催化剂存在下使草酸二芳基酯进行脱羰反应,将草酸二芳基酯转化为相应的碳酸二芳基酯,同时从反应体系中除去包含一氧化碳的反应副产物; 和(D)从步骤(C)的反应产物混合物中收集碳酸二芳基酯。

    Diphenyl oxalate-phenol adduct, process for producing the adduct and
method of producing diphenyl oxalate from the adduct
    3.
    发明授权
    Diphenyl oxalate-phenol adduct, process for producing the adduct and method of producing diphenyl oxalate from the adduct 失效
    草酸二苯酚 - 苯酚加合物,加合物的制备方法和从加合物生产草酸二苯酯的方法

    公开(公告)号:US5705677A

    公开(公告)日:1998-01-06

    申请号:US757070

    申请日:1996-11-26

    IPC分类号: C07C69/017 C07C69/36

    CPC分类号: C07C69/017 C07C69/36

    摘要: A novel crystalline adduct of diphenyl oxalate and phenol in a molar ratio of 1:2 and having a high purity is produced by melting a mixture containing diphenyl oxalate and phenol at a temperature of 100.degree. C. or more; cooling the melt to a temperature of less than 100.degree. C. to allow a resultant adduct of diphenyl oxalate and phenol in a molar ratio of 1:2 to crystallize and deposit from the melt; and collecting the crystalline adduct. Diphenyl oxalate with a high purity is produced by melting the crystalline adduct to dissociate it into diphenyl oxalate and phenol, and evaporating away the dissociated phenol from the melt to collect the dissociated diphenyl oxalate.

    摘要翻译: 通过在100℃或更高的温度下熔化含有草酸二苯酯和苯酚的混合物,产生摩尔比为1:2且具有高纯度的草酸二苯酯和苯酚的新型结晶加合物; 将熔体冷却至低于100℃的温度,使所得到的草酸二苯酯和苯酚的摩尔比为1:2的加合物从熔体中结晶和沉积; 并收集结晶加合物。 通过熔化结晶加合物将其分解成草酸二苯酯和苯酚,并将离解的苯酚从熔体中蒸发掉以收集离解的草酸二苯酯,从而产生高纯度的二苯基草酸盐。

    Process for producing a diaryl oxalate
    4.
    发明授权
    Process for producing a diaryl oxalate 失效
    制备草酸二芳基酯的方法

    公开(公告)号:US6018072A

    公开(公告)日:2000-01-25

    申请号:US875823

    申请日:1997-08-07

    IPC分类号: C07C67/02 C07C69/34

    CPC分类号: C07C67/02

    摘要: The present invention relates to a process for producing a diaryl oxalate, characterized in that an alkylaryl oxalate is subjected to a disproportionation reaction in the presence of a disproportionation catalyst, thereby to produce a diaryl oxalate while removing a by-product comprising a dialkyl oxalate.The production process of the present invention is advantageous in that the kinds of the by-products are fewer than that in conventional production process for diaryl oxalate, and thus can be practically utilized in industry, and the diaryl oxalates such as diphenyl oxalate, produced by the production process of the present invention are very important industrial materials for producing chemical products such as carbamates.

    摘要翻译: PCT No.PCT / JP96 / 03636 Sec。 371日期1997年8月7日 102(e)日期1997年8月7日PCT 1996年12月12日PCT PCT。 公开号WO97 / 21660 日期:1997年6月19日本发明涉及草酸二芳基酯的制备方法,其特征在于草酸烷基芳基酯在歧化催化剂存在下进行歧化反应,从而产生草酸二芳基酯,同时除去副产物 包括草酸二烷基酯。 本发明的制造方法的优点在于副产物的种类比常规的草酸二芳基酯的制备方法少,因此可以实际应用于工业中,草酸二芳基酯如草酸二苯酯,由 本发明的生产方法是用于生产化学产品如氨基甲酸酯的非常重要的工业材料。

    Method of producing an ester compound
    6.
    发明授权
    Method of producing an ester compound 失效
    酯化合物的制备方法

    公开(公告)号:US5869729A

    公开(公告)日:1999-02-09

    申请号:US670552

    申请日:1996-06-27

    IPC分类号: C07C68/00 C07C69/96

    CPC分类号: C07C68/00

    摘要: An ester compound, for example, carbonic acid ester or succinic acid ester, is produced by catalytically reacting, in gas phase, carbon monoxide with a nitrous acid ester and optionally an olefin in the presence of a catalyst and in the presence of a chlorine-containing substance, bringing the reaction product-containing mixed gas into contact with a solid catalyst such as activated carbon or inorganic oxide to reduce the content of the chlorine-containing substance, cool-condensing the resultant mixed gas, and collecting the target ester compound from the condensed liquid.

    摘要翻译: 酯化合物,例如碳酸酯或琥珀酸酯,是通过在催化剂存在下,在氯气存在下,在气相中,一氧化碳与一种亚硝酸酯和任选的一种烯烃进行催化反应, 使含有反应产物的混合气体与固体催化剂如活性炭或无机氧化物接触以降低含氯物质的含量,冷凝所得混合气体,并将目标酯化合物从 冷凝液体。

    Document generation method, document generation system, and printing system
    7.
    发明申请
    Document generation method, document generation system, and printing system 审中-公开
    文件生成方法,文件生成系统和打印系统

    公开(公告)号:US20090147274A1

    公开(公告)日:2009-06-11

    申请号:US11901879

    申请日:2007-09-19

    IPC分类号: G06K15/02

    摘要: [Object] To control a protrusion amount which indicates an amount of protrusion of an image protruding to a surrounding portion of a sheet for printing when marginless printing is performed in accordance with the XHTML-print specification.[Solving Means] The UI processor 11 accepts designation of a size of a sheet for printing and designation of an amount of protrusion from the sheet for printing when marginless printing is performed. The XHTML document generation unit 12 generates an XHTML document including a size of an image to be printed which is specified in accordance with a scale factor used when marginless printing is performed in accordance with the XHTML-print specification, a print starting position of the image to be printed which is specified in accordance with the scale factor and the specified amount of protrusion, and designation of marginless printing.

    摘要翻译: 根据XHTML打印规格,当进行无边距打印时,控制指示突出到用于打印的纸张的周围部分的图像的突出量的突出量。 [解决方案]在执行无边距打印时,UI处理器11接受用于打印的片材的尺寸的指定和用于打印的片材的突出量的指定。 XHTML文档生成单元12生成包括根据XHTML打印规格执行无边距打印时所使用的比例因子指定的要打印的图像的大小的XHTML文档,图像的打印开始位置 要根据比例因子和指定的突出量指定打印,并指定无边距打印。

    Oil pump including rotors that change eccentric positional relationship one-to another to adjust a discharge amount
    9.
    发明授权
    Oil pump including rotors that change eccentric positional relationship one-to another to adjust a discharge amount 有权
    油泵包括转子偏心位置关系改变以调节排放量的转子

    公开(公告)号:US09127671B2

    公开(公告)日:2015-09-08

    申请号:US12933912

    申请日:2009-07-22

    摘要: An oil pump includes: an inner rotor rotatable with a drive shaft in a unified manner on a drive-rotation axis; an outer rotor which has inner teeth configured to engage with outer teeth of the inner rotor and is rotatable about a driven axis eccentric to the drive-rotation axis; and an adjustment ring for rotatably supporting the outer rotor. A guide means which allows the adjustment ring to rotate about the driven axis, while allowing the driven axis to revolve about the drive-rotation axis, is formed of: first and second arm portions provided on the adjustment ring; and first and second guide faces with which the first and second arm portions are brought into slidable contact.

    摘要翻译: 油泵包括:内转子,其以驱动轴在驱动旋转轴线上以统一的方式旋转; 外转子,其内齿构造成与内转子的外齿接合,并且能够围绕偏心于驱动旋转轴的从动轴旋转; 以及用于可旋转地支撑外转子的调节环。 引导装置,其允许调节环围绕驱动轴线旋转,同时允许从动轴围绕驱动旋转轴线旋转,由导向装置形成:设置在调节环上的第一和第二臂部分; 以及第一和第二引导面,第一和第二引导面与第一和第二臂部分可滑动接触。

    Valve timing control device
    10.
    发明授权
    Valve timing control device 有权
    气门正时控制装置

    公开(公告)号:US08091524B2

    公开(公告)日:2012-01-10

    申请号:US12508134

    申请日:2009-07-23

    IPC分类号: F01L1/34

    摘要: A valve timing control device includes a driving side rotational member, a driven side rotational member, a fluid pressure chamber, a parting portion dividing the fluid pressure chamber into an advanced angle chamber and a retarded angle chamber, a restriction member, a restriction recessed portion for restricting a displacement of a relative rotational phase within a range between a most advanced angle phase or a most retarded angle phase and a predetermined phase when the restriction member is inserted into the restriction recessed portion, and a restriction cancellation passage, wherein a communication between the accommodation portion and one of the advanced angle chamber and the retarded angle chamber via the cancellation passage is interrupted at least when the restriction member contacts one of end portions of the restriction recessed portion, and the restriction member is restricted so as not to move over the other one of the end portions.

    摘要翻译: 气门正时控制装置包括驱动侧旋转构件,从动侧旋转构件,流体压力室,将流体压力室分割成前进角室和延迟角室的分离部,限制构件,限制凹部 用于限制在所述限制构件插入所述限制凹部中时在最高角度相位或最大延迟角度相位与预定相位之间的范围内的相对旋转相位的位移,以及限制消除通道,其中, 至少当限制构件接触限制凹部的端部之一时,经由消除通道的收纳部分和提前角室和延迟角室中的一个被中断,并且限制构件被限制为不移动 另一个端部。