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    Device for determining the composition of a fluid mixture
    5.
    发明申请
    Device for determining the composition of a fluid mixture 有权
    用于确定流体混合物的组成的装置

    公开(公告)号：US20050264302A1

    公开(公告)日：2005-12-01

    申请号：US11119556

    申请日：2005-05-02

    申请人： Kim Mohajer ,  Edward Browne ,  Abbas Khajeh

    发明人： Kim Mohajer ,  Edward Browne ,  Abbas Khajeh

    IPC分类号： G01N22/00 ,  G01N30/62 ,  G01N30/95 ,  G01N33/20 ,  G01N33/28 ,  G01N37/00 ,  G01R27/08 ,  G01R27/22 ,  G01R27/26 ,  G01R27/32

    CPC分类号： G01N22/00 ,  G01N33/2847 ,  G01R27/22

    摘要： A method and apparatus are disclosed for determining the concentration of individual components within a fluid mixture by determining the permittivity of the individual components. The method and apparatus use a reference sensor and at least one measurement sensor positioned inside the same sensor device that is immersed in the fluid mixture to be measured. Signals, such as radio frequency or microwave, are sequentially transmitted at multiple, known, constant frequencies to and reflected from both the reference and measurement sensor(s). Permittivities of the individual components are determined from these transmitted and reflected signals and information about the concentration of the individual fluids and other compounds within the fluid mixture and the density of the fluid mixture are produced. Repetitive sampling and processing of these signals allow determination and real-time monitoring of the concentration of individual components within a mixture of fluids. The present invention provides self-calibration, accurate frequency maintenance and self-selection of an operating frequency range.

    摘要翻译： 公开了一种用于通过确定各个部件的介电常数来确定流体混合物内各个部件的浓度的方法和装置。 该方法和装置使用参考传感器和位于同一传感器装置内部的至少一个测量传感器，该传感器装置浸没在要测量的流体混合物中。 诸如射频或微波之类的信号以多个已知的恒定频率被顺序传送到参考和测量传感器两者并从其反射。 根据这些透射和反射的信号以及关于流体混合物内的各种流体和其它化合物的浓度的信息以及流体混合物的密度产生单个组分的介电常数。 重复采样和处理这些信号可以确定和实时监测流体混合物内各个组分的浓度。 本发明提供工作频率范围的自校准，精确的频率维持和自选。

    Water-miscible metal working fluids with reduced aerosol inhalation toxicity
    6.
    发明申请
    Water-miscible metal working fluids with reduced aerosol inhalation toxicity 审中-公开
    水溶性金属工作液，具有降低的气溶胶吸入毒性

    公开(公告)号：US20070167335A1

    公开(公告)日：2007-07-19

    申请号：US11332071

    申请日：2006-01-13

    申请人： George Combs ,  Edward Browne

    发明人： George Combs ,  Edward Browne

    IPC分类号： C10M171/00

    CPC分类号： C10M173/02 ,  C10M2209/104 ,  C10M2209/105 ,  C10M2209/108 ,  C10N2230/64 ,  C10N2240/401

    摘要： The present invention provides a process for producing a water-miscible metalworking fluid by combining water, and additives chosen from plasticizers, chelating agents, biocides, surfactants, dispersants, dyes, odorants, extreme pressure agents, anti-oxidants and corrosion inhibitors with a polyether polyol produced by mixing an active hydrogen compound with a double metal cyanide (DMC) catalyst in a reactor vessel, charging to the reactor vessel a mixture containing two or more alkylene oxides to activate the catalyst and continuously feeding one or more alkylene oxides to produce the polyether polyol, wherein a 1% solution in water of the polyether polyol has a cloud point of greater than about 32° C., the equivalent weight of the polyether polyol is greater than about 1,000 Da, and a four-hour aerosol inhalation exposure to the polyether polyol has a LC50 of greater than about 0.50 mg/L. The water-miscible metalworking fluid produced by the inventive process may find use in cooling and/or lubricating metal surfaces during one or more of grinding, cutting, boring, drilling and turning of metal parts.

    摘要翻译： 本发明提供了一种通过将水和选自增塑剂，螯合剂，杀生物剂，表面活性剂，分散剂，染料，气味剂，极压剂，抗氧化剂和腐蚀抑制剂的添加剂与聚醚结合来生产水混溶性金属加工液的方法 通过在反应器容器中将活性氢化合物与双金属氰化物（DMC）催化剂混合而制备的多元醇，向反应器容器中加入含有两种或更多种环氧烷烃的混合物以活化催化剂并连续供给一种或多种烯化氧以产生 聚醚多元醇，其中聚醚多元醇的1％水溶液的浊点大于约32℃，聚醚多元醇的当量大于约1,000Da，并且四小时气溶胶吸入暴露于 聚醚多元醇具有大于约0.50mg / L的LC 50。 由本发明方法生产的与水可混溶的金属加工流体可用于在金属部件的研磨，切割，钻孔，钻孔和车削期间的一个或多个过程中冷却和/或润滑金属表面。

    Starter feed stream acidification in DMC-catalyzed process
    7.
    发明授权
    Starter feed stream acidification in DMC-catalyzed process 有权
    起动器进料流酸化DMC催化过程

    公开(公告)号：US07919575B2

    公开(公告)日：2011-04-05

    申请号：US12786628

    申请日：2010-05-25

    申请人： Edward Browne

    发明人： Edward Browne

    IPC分类号： C08G65/34 ,  C07C43/00

    CPC分类号： C08G65/2696 ,  B01J27/26 ,  C08G65/2663

    摘要： The process of the present invention provides for the manufacture of lower molecular weight DMC-catalyzed polyols than is possible using non-acidified continuous addition of starter (CAOS) feeds, by adding excess acid to a starter feed stream over that required for mere neutralization of the basicity of the starter. The benefits of the invention also extend to starters which do not contain basicity. Polyether polyols made by the inventive process may be used to produce improved polyurethane products such as coatings, adhesives, sealants, elastomers, foams and the like.

    摘要翻译： 本发明的方法提供了比使用非酸化连续添加起动剂（CAOS）进料可能制备低分子量DMC-催化的多元醇，通过向起始物原料流中加入过量的酸，超过纯中和所需的 起始者的基本性。 本发明的优点还扩展到不包含碱性的起动器。 通过本发明方法制备的聚醚多元醇可用于生产改进的聚氨酯产品，例如涂料，粘合剂，密封剂，弹性体，泡沫等。

    Water-miscible metal working fluids with reduced aerosol inhalation toxicity
    8.
    发明申请
    Water-miscible metal working fluids with reduced aerosol inhalation toxicity 审中-公开
    水溶性金属工作液，具有降低的气溶胶吸入毒性

    公开(公告)号：US20070167336A1

    公开(公告)日：2007-07-19

    申请号：US11439576

    申请日：2006-05-24

    申请人： George Combs ,  Edward Browne

    发明人： George Combs ,  Edward Browne

    IPC分类号： C10M171/00 ,  C10L1/18

    CPC分类号： C10M173/02 ,  C08G65/2663 ,  C08L71/02 ,  C10M107/34 ,  C10M177/00 ,  C10M2209/104 ,  C10M2209/105 ,  C10M2209/107 ,  C10M2209/1075 ,  C10N2220/021 ,  C10N2230/00 ,  C10N2230/64 ,  C10N2240/40 ,  C10N2240/401

    摘要： The present invention provides a process for producing a water-miscible metalworking fluid involving combining about 90 wt. % to about 5 wt. %, based on the weight of the fluid, of water and one or more additives chosen from plasticizers, chelating agents, biocides, surfactants, dispersants, dyes, odorants, extreme pressure agents, anti-oxidants and corrosion inhibitors with about 10 wt. % to about 95 wt. %, based on the weight of the fluid, of a polyether polyol produced by mixing an active hydrogen compound with a double metal cyanide (DMC) catalyst in a reactor vessel, charging to the reactor vessel a mixture containing two or more alkylene oxides to activate the catalyst, and continuously feeding one or more alkylene oxides to produce the polyether polyol, wherein a 1% solution in water of the polyether polyol has a cloud point of from greater than about 32° C. to less than about 53° C., the polyether polyol has a number average equivalent weight of from greater than about 1,600 Da to about 10,000 Da, and a four-hour aerosol inhalation exposure to the polyether polyol has a LC50 of greater than about 5 mg/L. The water-miscible metalworking fluid produced by the inventive process may find use in cooling and/or lubricating metal surfaces during one or more of grinding, cutting, boring, drilling and turning of metal parts.

    摘要翻译： 本发明提供了一种生产水混溶性金属加工液的方法，其包括将约90wt。 ％至约5wt。 基于流体重量的水和一种或多种添加剂，其选自增塑剂，螯合剂，杀生物剂，表面活性剂，分散剂，染料，气味剂，极压剂，抗氧化剂和具有约10wt。 ％至约95wt。 基于流体重量的通过在反应器容器中混合活性氢化合物与双金属氰化物（DMC）催化剂而制备的聚醚多元醇，向反应容器中加入含有两种或更多种氧化烯以使其活化的混合物 催化剂，并连续地供给一种或多种烯化氧以制备聚醚多元醇，其中聚醚多元醇的1％水溶液的浊点为大于约32℃至小于约53℃， 聚醚多元醇的数均当量为大于约1,600Da至约10,000Da，并且对聚醚多元醇的四小时气溶胶吸入暴露具有大于约5mg的LC 50 / L。 由本发明方法生产的与水可混溶的金属加工流体可用于在金属部件的研磨，切割，钻孔，钻孔和车削期间的一个或多个过程中冷却和/或润滑金属表面。

    Starter feed stream acidification in DMC-catalyzed process
    9.
    发明申请
    Starter feed stream acidification in DMC-catalyzed process 审中-公开
    起动器进料流酸化DMC催化过程

    公开(公告)号：US20050209438A1

    公开(公告)日：2005-09-22

    申请号：US10804894

    申请日：2004-03-19

    申请人： Edward Browne

    发明人： Edward Browne

    IPC分类号： C08G65/10 ,  B01J27/26 ,  C08G65/26 ,  C08G59/68

    CPC分类号： C08G65/2696 ,  B01J27/26 ,  C08G65/2663

    摘要： The process of the present invention provides for the manufacture of lower molecular weight DMC-catalyzed polyols than is possible using non-acidified continuous addition of starter (CAOS) feeds, by adding excess acid to a starter feed stream over that required for mere neutralization of the basicity of the starter. The benefits of the invention also extend to starters which do not contain basicity. Polyether polyols made by the inventive process may be used to produce improved polyurethane products such as coatings, adhesives, sealants, elastomers, foams and the like.

    摘要翻译： 本发明的方法提供了比使用非酸化连续添加起动剂（CAOS）进料可能制备低分子量DMC-催化的多元醇，通过向起始物原料流中加入过量的酸，超过纯中和所需的 起始者的基本性。 本发明的优点还扩展到不包含碱性的起动器。 通过本发明方法制备的聚醚多元醇可用于生产改进的聚氨酯产品，例如涂料，粘合剂，密封剂，弹性体，泡沫等。