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    Process for making 3,4,5,6-tetrahydrophthalimide derivatives
    1.
    发明授权
    Process for making 3,4,5,6-tetrahydrophthalimide derivatives 失效
    制备3,4,5,6-四氢邻苯二甲酰亚胺衍生物的方法

    公开(公告)号：US5324843A

    公开(公告)日：1994-06-28

    申请号：US39497

    申请日：1993-04-29

    申请人： Lothar Rueb ,  Karl Eicken ,  Bernd Schaefer ,  Gernot Reissenweber ,  Peter Schaefer

    发明人： Lothar Rueb ,  Karl Eicken ,  Bernd Schaefer ,  Gernot Reissenweber ,  Peter Schaefer

    IPC分类号： C07C205/56 ,  C07C229/40 ,  C07D209/48

    CPC分类号： C07D209/48

    摘要： 3-(3,4,5,6-tetrahydrophthalimido)cinnamic esters I ##STR1## (R.sup.1 =H, halogen; R.sup.2, R.sup.3 =halogen; R.sup.4 =C-organic radical, R.sup.5 =H, CH.sub.3) are prepared by reducing 3-nitrocinnamic esters II ##STR2## with hydrogen in the presence of a catalyst and condensing the resulting 3-aminocinnamic esters III ##STR3## with a 3,4,5,6-tetrahydrophthalic anhydride IV ##STR4## and are valuable active ingredients in crop protection.

    摘要翻译： PCT No.PCT / EP91 / 02166 Sec。 371日期：1993年4月29日 102（e）日期1993年4月29日PCT 1991年11月16日PCT PCT。 出版物WO92 / 09575 日期：1992年6月11日3 - （3,4,5,6-四氢邻苯二甲酰亚氨基）肉桂酸酯I（R1 = H，卤素; R2，R3 =卤素; R4 = C-有机基团，R5 = H，CH3 ）通过还原3-硝基鸟氨酸酯II和将所得的3-氨基鸟氨酸酯III III与3,4,5,6-四氢邻苯二甲酸酐IV IV缩合制备，并且是作物中有价值的活性成分 保护。

    N-aryltetrahydrophthalimides and herbicidal compositions thereof
    3.
    发明授权
    N-aryltetrahydrophthalimides and herbicidal compositions thereof 失效
    N-三氟甲磺酰嘧啶及其除草剂组合物

    公开(公告)号：US5133799A

    公开(公告)日：1992-07-28

    申请号：US697036

    申请日：1991-05-08

    申请人： Rainer Seele ,  Lothar Rueb ,  Reiner Kober ,  Karl Eicken ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Rainer Seele ,  Lothar Rueb ,  Reiner Kober ,  Karl Eicken ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： A01N43/50 ,  A01N43/56 ,  A01N43/653 ,  C07D403/10 ,  C07D403/14 ,  C07D521/00

    CPC分类号： C07D231/12 ,  A01N43/50 ,  A01N43/56 ,  A01N43/653 ,  C07D233/56 ,  C07D249/08 ,  C07D403/10 ,  C07D403/14

    摘要： R.sup.1 is C.sub.1 -C.sub.4 -alkyl which may carry from one to five halogen atoms or one of the groups stated for X;R.sup.2 is a heteroaromatic structure bonded via a nitrogen atom, which has a 5-membered ring and contains, in addition to carbon ring members, from one to three nitrogen atoms, andR.sup.3 is halogen, C.sub.1 -C.sub.4 -alkylthio, one of the groups stated for R.sup.2 or phenylthio which in turn may carry from one to three of the following radicals: halogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -haloalkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -haloalkoxy or C.sub.1 -C.sub.4 -alkylthio, and where the phenylthio group may also carry halogen atoms such that the total number of radicals is 4 or 5,and salts thereof which can be used in agriculture, are suitable as herbicides. 2

    摘要翻译： 其中X是氢或卤素; R 1是可以携带1至5个卤素原子的C1-C4-烷基或为X表示的基团之一; R2是通过氮原子键合的杂芳族结构，其具有5元环，并且除了碳环成员之外还含有一个至三个氮原子，并且R 3是卤素，C 1 -C 4 - 烷硫基，其中一个基团 对于R2或苯硫基，其又可以携带1-3个以下基团：卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基，C 1 -C 4 - 卤代烷氧基或C 1 -C 4 - 烷硫基 并且苯硫基也可以携带卤素原子使得基团的总数为4或5，并且其可用于农业的盐适用作除草剂。

    Tetrahydroindazoles with a phenyl ether structure, compositions and use
    4.
    发明授权
    Tetrahydroindazoles with a phenyl ether structure, compositions and use 失效
    具有苯乙烯结构的组合物和用途的四氢呋喃

    公开(公告)号：US5112383A

    公开(公告)日：1992-05-12

    申请号：US749352

    申请日：1991-08-23

    申请人： Lothar Rueb ,  Karl Eicken ,  Peter Plath ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Lothar Rueb ,  Karl Eicken ,  Peter Plath ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： A01N43/56 ,  C07D231/56 ,  C07D405/12 ,  C07D409/12

    CPC分类号： C07D231/56 ,  C07D405/12 ,  C07D409/12

    摘要： N-(Phenyl)-tetrahydroindazole derivatives of the general formula 1a and 1b ##STR1## where R.sup.1 is halogen;R.sup.2 is C.sub.1 -C.sub.6 -alkoxycarbonyl-C.sub.3 -C.sub.5 -alkenyl or C.sub.1 -C.sub.3 -alkyl which is substituted in the 1- or 2-position by C.sub.1 -C.sub.6 -alkoxycarbonyl or a 5- or 6-membered saturated or monounsaturated heterocycle which contains one oxygen or sulfur as heteroatom and can be substituted by from one to four C.sub.1 -C.sub.4 -alkyls, andR.sup.3 is C.sub.2 -C.sub.7 -alkyl, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.6 -alkynyl, C.sub.1 -C.sub.6 -alkoxycarbonyl-C.sub.3 -C.sub.5 -alkenyl or C.sub.1 -C.sub.3 -alkyl which is substituted in the 1- or 2-position by C.sub.1 -C.sub.6 -alkoxycarbonyl or a 5- or 6-membered saturated or monounsaturated heterocycle which contains one oxygen or sulfur as heteroatom and can be substituted by from one to four C.sub.1 -C.sub.4 -alkyls, their manufacture and their herbicidal use.

    N-phenyltetrahydroindazole derivatives herbicidal compositions and use
    5.
    发明授权
    N-phenyltetrahydroindazole derivatives herbicidal compositions and use 失效
    N-苯基四氢吲唑衍生物除草组合物及用途

    公开(公告)号：US4990174A

    公开(公告)日：1991-02-05

    申请号：US462704

    申请日：1990-01-09

    申请人： Lothar Rueb ,  Karl Eicken ,  Peter Plath ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Lothar Rueb ,  Karl Eicken ,  Peter Plath ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： C07D231/54 ,  A01N43/56 ,  C07D231/56

    CPC分类号： C07D231/56

    摘要： R.sup.2 is halogen,R.sup.3 is hydrogen, halogen or a C.sub.1 -C.sub.4 -alkyl,R.sup.4, R.sup.5 are hydrogen, C.sub.1 -C.sub.8 -alkyl, C.sub.2 -C.sub.4 -alkyl which carries a hydroxyl, C.sub.1 -C.sub.4 -alkoxy or C.sub.1 -C.sub.4 -alkylthio radical, C.sub.1 -C.sub.6 -alkoxy, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.6 -alkynyl, C.sub.3 -C.sub.6 -alkenyloxy and/or C.sub.3 -C.sub.6 -alkynyloxy, or together with the nitorgen atom form a 5- or 6-membered aliphatic ring in which a methylene group may be replaced by an oxygen atom, andR.sup.6 is hydrogen, C.sub.1 -C.sub.6 -alkyl which is unsubstituted or substituted by one or two C.sub.1 -C.sub.4 -alkoxy groups, or is C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.6 -alkynyl or benzyl,processes for their manufacture, and their herbicidal use.

    摘要翻译： 其中R 1是氢或氟，R 2是卤素，R 3是氢，卤素或C 1 -C 4烷基，R 4，R 5是氢，C 1 -C 8 - 烷基，C 2 -C 4烷基， 含有羟基，C 1 -C 4 - 烷氧基或C 1 -C 4 - 烷硫基，C 1 -C 6 - 烷氧基，C 3 -C 6 - 烯基，C 3 -C 6炔基，C 3 -C 6 - 烯氧基和/或C 3 -C 6 - 炔氧基，或 与维生素原子一起形成5-或6-元脂族环，其中亚甲基可以被氧原子取代，R6是氢，未被取代或被一个或两个C1-C4取代的C1-C6-烷基 - 烷氧基，或为C 3 -C 6 - 烯基，C 3 -C 6 - 炔基或苄基，其制备方法及其除草用途。

    Herbicidal thiadiazabicyclononane derivatives
    8.
    发明授权
    Herbicidal thiadiazabicyclononane derivatives 失效
    除草剂三氮杂环戊二烯衍生物

    公开(公告)号：US5106408A

    公开(公告)日：1992-04-21

    申请号：US561813

    申请日：1990-08-02

    申请人： Lothar Rueb ,  Karl Eicken ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Lothar Rueb ,  Karl Eicken ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： C07D417/12 ,  A01N43/90 ,  C07D513/04

    CPC分类号： C07D513/04 ,  A01N43/90

    摘要： Thiadiazabicyclononane derivatives of the formula I ##STR1## (R.sup.1 =H, F; R.sup.2 =halogen; R.sup.3 =H, C.sub.1 -C.sub.4 -alkyl; R.sup.4 =H, C.sub.1 -C.sub.8 -alkoxycarbonyl, C.sub.3 -C.sub.6 -alkenyloxycarbonyl or C.sub.3 -C.sub.5 -alkynyloxycarbonyl, and these 3 groups may additionally bear C.sub.1 -C.sub.4 -alkoxy; X, Y, Z=O,= S; a=C.sub.2 -C.sub.3 -alkylene chain which in addition to R.sup.4 may bear up to 3 identical or different radicals R.sup.5 : OH, COOH, C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.6 -alkoxycarbonyl, and the last two radicals may in turn bear up to 5 halogen atoms or one of the following substituents; OH, CN, SH, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.6 -alkylthio, C.sub.3 -C.sub.6 -alkenyloxy, C.sub.3 -C.sub.6 -alkenylthio, C.sub.3 -C.sub.6 -alkynyloxy, C.sub.3 -C.sub.6 -alkynylthio, C.sub.1 -C.sub.6 -alkylcarbonyloxy, C.sub.1 -C.sub.6 -alkoxycarbonyl, C.sub.1 -C.sub.6 -alkoxycarbonyl-C.sub.1 -C.sub.4 -alkoxy or C.sub.1 -C.sub.6 -alkoxycarbonyl-C.sub.1 -C.sub.4 -alkylthio).These thiadiazabicyclononane derivatives are suitable for use as herbicides.

    摘要翻译： 式I的噻二唑二环壬烷衍生物（R1 = H，F; R2 =卤素; R3 = H，C1-C4-烷基; R4 = H，C1-C8-烷氧基羰基，C3-C6-烯氧基羰基或C3-C5 - 炔基氧基羰基，并且这3个基团可以另外具有C 1 -C 4 - 烷氧基; X，Y，Z = O，= S; a = C 2 -C 3 - 亚烷基链，除了R 4之外，还可以具有3个相同或不同的基团R 5 ：OH，COOH，C 1 -C 4 - 烷基或C 1 -C 6 - 烷氧基羰基，最后两个基团又可以承载多达5个卤素原子或以下取代基之一：OH，CN，SH，C 1 -C 4 - 烷氧基， C 1 -C 6 - 烷硫基，C 3 -C 6 - 烯氧基，C 3 -C 6 - 烯硫基，C 3 -C 6 - 炔氧基，C 3 -C 6炔硫基，C 1 -C 6烷基羰氧基，C 1 -C 6烷氧基羰基，C 1 -C 6烷氧羰基-C 1 - C 1 -C 6 - 烷氧基羰基-C 1 -C 4 - 烷硫基）。 这些噻二氮二环壬烷衍生物适合用作除草剂。

    5-(N-3,4,5,6-tetrahydrophthalimido)cinnamic acid derivatives
    10.
    发明授权
    5-(N-3,4,5,6-tetrahydrophthalimido)cinnamic acid derivatives 失效
    5-（N-3,4,5,6-四氢邻苯二甲酰亚氨基）肉桂酸衍生物

    公开(公告)号：US5009701A

    公开(公告)日：1991-04-23

    申请号：US403382

    申请日：1989-09-06

    申请人： Peter Plath ,  Karl Eicken ,  Lothar Rueb ,  Barbara Schwalge ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    发明人： Peter Plath ,  Karl Eicken ,  Lothar Rueb ,  Barbara Schwalge ,  Karl-Otto Westphalen ,  Bruno Wuerzer

    IPC分类号： A01N37/46 ,  A01N43/38 ,  C07D209/48

    CPC分类号： C07D209/48 ,  A01N37/46

    摘要： 5-(N-3,4,5,6-Tetrahydrophthalimido)-cinnamic acid derivatives of the formula Ib ##STR1## where the substituents have the following meanings: Y is chlorine, bromine or C.sub.1 -C.sub.4 -alkyl;R.sup.1 is hydrogen, C.sub.1 -C.sub.8 -alkyl, substituted or unsubstituted C.sub.2 -C.sub.4 alkyl, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.6 -alkynyl, or substituted or unsubstituted phenyl or benzyl,R.sup.2 is C.sub.5 -C.sub.8 -alkyl, substituted or unsubstituted C.sub.2 -C.sub.4 -alkyl, C.sub.1 -C.sub.6 -alkoxy, C.sub.3 -C.sub.6 -alkenyl, C.sub.3 -C.sub.6 -alkenyloxy, C.sub.3 -C.sub.6 -alkynyl, C.sub.3 -C.sub.6 -alkynyloxy, or substituted or unsubstituted phenyl, phenoxy, benzyl or benzyloxy,R.sub.3 C.sub.1 -C.sub.6 -alkyl, or substituted or unsubstituted C.sub.2 -C.sub.6 -alkyl,methods of manufacturing these compounds, and their use as herbicides.

    摘要翻译： 式Ib Ib的5-（N-3,4,5,6-四氢邻苯二甲酰亚氨基） - 肉桂酸衍生物，其中取代基具有以下含义：Y是氯，溴或C 1 -C 4 - 烷基; R 1是氢，C 1 -C 8 - 烷基，取代或未取代的C 2 -C 4烷基，C 3 -C 6 - 烯基，C 3 -C 6炔基或取代或未取代的苯基或苄基，R 2是C 5 -C 8 - 烷基，取代或未取代的C 2- C 1 -C 6 - 烷基，C 1 -C 6 - 烷氧基，C 3 -C 6 - 烯基，C 3 -C 6 - 烯氧基，C 3 -C 6 - 炔基，C 3 -C 6 - 炔氧基或取代或未取代的苯基，苯氧基，苄基或苄氧基， - 烷基或取代或未取代的C 2 -C 6 - 烷基，制备这些化合物的方法及其作为除草剂的用途。