Method for manufacturing methyltetrahydrophthalic anhydride

    公开(公告)号:US12116340B2

    公开(公告)日:2024-10-15

    申请号:US18069943

    申请日:2022-12-21

    CPC classification number: C07C51/56 C07D307/89

    Abstract: A method for manufacturing methyltetrahydrophthalic anhydride is provided, which includes steps as follows. Maleic anhydride is added into a reactor. Piperylene is added into the reactor, so that the piperylene and the maleic anhydride undergo a first addition reaction. When a conversion rate of the maleic anhydride is more than 25%, the first addition reaction is completed. Isoprene is added into the reactor, so that the isoprene and the maleic anhydride undergo a second addition reaction to obtain a methyltetrahydrophthalic anhydride product. The methyltetrahydrophthalic anhydride product contains 3-methyltetrahydrophthalic anhydride and 4-methyltetrahydrophthalic anhydride.

    Method for manufacturing nonylcyclohexanol

    公开(公告)号:US11739037B1

    公开(公告)日:2023-08-29

    申请号:US17991816

    申请日:2022-11-21

    CPC classification number: C07C29/20 B01J8/10 B01J23/464 C07C29/20 C07C35/08

    Abstract: A method for manufacturing nonylcyclohexanol is provided. The method includes steps as follows: adding a liquid phase reactant into a reactor, and the liquid phase reactant includes a molten nonylphenol and a catalyst; introducing a gas phase reactant to maintain a pressure of the gas phase reactant to be from 36.5 bar to 70 bar, and the gas phase reactant consists of hydrogen; rotating a hollow stirring shaft of the reactor at a temperature of from 100° C. to 130° C. so that the gas phase reactant is transported through a channel formed in the hollow stirring shaft into the liquid phase reactant for carrying out a reaction; obtaining a product that contains nonylcyclohexanol. A conversion rate of the nonylcyclohexanol is higher than or equal to 99.0%.

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