公开(公告)号：US20110303599A1

公开(公告)日：2011-12-15

申请号：US13202722

申请日：2010-03-10

申请人： Norimasa Minamoto ,  Masahito Ito ,  Kisaburo Deguchi ,  Hiroyuki Tanai ,  Kiyotoshi Mori

发明人： Norimasa Minamoto ,  Masahito Ito ,  Kisaburo Deguchi ,  Hiroyuki Tanai ,  Kiyotoshi Mori

IPC分类号： B01D15/08 ,  B01D39/10

CPC分类号： G01N30/603

摘要： In a liquid chromatograph, the disulfide adsorption of iron atoms in a filter for a column is avoided and thus peak tailing in a chromatogram is prevented to thereby prevent a lowering in the sample recovery rate. A liquid chromatograph column comprising a hollow tubular column body, a bead-shaped packing material which is packed in the hollow part of the column body, a filter provided with a mesh which has a mesh size smaller than the particle diameter of the packing material, and a cap which presses the filter against the packing material to thereby enclose the packing material within the column body, characterized in that the main component of the filter is nickel or hastelloy.

摘要翻译： 在液相色谱仪中，避免了用于柱的过滤器中的铁原子的二硫键吸附，因此防止了色谱图中的峰值拖尾，从而防止了样品回收率的降低。 一种液相色谱柱，包括中空管状柱体，填充在柱体中空部分中的珠状包装材料，具有筛网尺寸小于包装材料粒径的筛网的过滤器， 以及将过滤器压靠在包装材料上的盖子，从而将包装材料包围在柱体内，其特征在于，过滤器的主要部件是镍或哈氏合金。

公开(公告)号：US09110073B2

公开(公告)日：2015-08-18

申请号：US13202722

申请日：2010-03-10

申请人： Norimasa Minamoto ,  Masahito Ito ,  Kisaburo Deguchi ,  Hiroyuki Tanai ,  Kiyotoshi Mori

发明人： Norimasa Minamoto ,  Masahito Ito ,  Kisaburo Deguchi ,  Hiroyuki Tanai ,  Kiyotoshi Mori

IPC分类号： G01N30/60

CPC分类号： G01N30/603

摘要： In a liquid chromatograph, the disulfide adsorption of iron atoms in a filter for a column is avoided and thus peak tailing in a chromatogram is prevented to thereby prevent a lowering in the sample recovery rate. A liquid chromatograph column comprising a hollow tubular column body, a bead-shaped packing material which is packed in the hollow part of the column body, a filter provided with a mesh which has a mesh size smaller than the particle diameter of the packing material, and a cap which presses the filter against the packing material to thereby enclose the packing material within the column body, characterized in that the main component of the filter is nickel or hastelloy.

摘要翻译： 在液相色谱仪中，避免了用于柱的过滤器中的铁原子的二硫键吸附，因此防止了色谱图中的峰值拖尾，从而防止了样品回收率的降低。 一种液相色谱柱，包括中空管状柱体，填充在柱体中空部分中的珠状包装材料，具有筛网尺寸小于包装材料粒径的筛网的过滤器， 以及将过滤器压靠在包装材料上的盖子，从而将包装材料包围在柱体内，其特征在于，过滤器的主要部件是镍或哈氏合金。

公开(公告)号：US20130145828A1

公开(公告)日：2013-06-13

申请号：US13818035

申请日：2011-08-26

申请人： Masako Kawarai ,  Masahito Ito ,  Norimasa Minamoto

发明人： Masako Kawarai ,  Masahito Ito ,  Norimasa Minamoto

IPC分类号： B01J39/26 ,  G01N30/50

CPC分类号： B01J39/26 ,  B01J20/286 ,  B01J20/321 ,  B01J20/327 ,  B01J20/328 ,  B01J20/3282 ,  B01J20/3293 ,  B01J39/20 ,  B01J2220/54 ,  G01N30/50 ,  G01N2030/525 ,  G01N2030/567

摘要： To provide a column packing, a separation column, an analysis device, and an analysis method to reduce the analysis time without deteriorating the separation of multi-component amino acids. Disclosed are a column packing comprising a core portion made of a styrene-di-vinylbenzene copolymer having a cross-linkage degree of 50% or more and a shell portion made of a styrene-di-vinylbenzene copolymer having a cross-linkage degree of 20% or less; a separation column using the column packing; and a high-speed liquid chromatography analysis device and a analysis method using the separation column.

摘要翻译： 提供柱填充，分离柱，分析装置和分析方法，以减少分析时间，而不会降低多组分氨基酸的分离。 公开了一种柱填料，其包含由交联度为50％以上的苯乙烯 - 二乙烯基苯共聚物制成的核心部分和由交联度为20的苯乙烯 - 二乙烯基苯共聚物制成的壳部分 ％ 或更少; 使用柱填料的分离柱; 和高速液相色谱分析装置以及使用分离塔的分析方法。