公开(公告)号：US20160145441A1

公开(公告)日：2016-05-26

申请号：US14951541

申请日：2015-11-25

申请人： PPG INDUSTRIES OHIO, INC.

发明人： SONGWEI LU ,  NOEL VANIER ,  XIANGLING XU ,  SHANTI SWARUP ,  DAVID C. MARTIN ,  KURT G. OLSON ,  Irina Schwendeman

IPC分类号： C09D5/00 ,  C09D183/06 ,  C03C17/30 ,  C09D125/06

摘要： Curable film-forming sol-gel compositions that are essentially free of inorganic oxide particles are provided. The compositions contain: a tetraalkoxysilane; a solvent component; and non-oxide particles, and further contain either i) a mineral acid or ii) an epoxy functional trialkoxysilane and a metal-containing catalyst. Coated articles demonstrating antiglare properties are also provided, comprising: (a) a substrate having at least one surface; and (b) a cured film-forming composition applied thereon, formed from a curable sol-gel composition comprising a silane and non-oxide particles. A method of forming an antiglare coating on a substrate is also provided. The method comprises: (a) applying a curable film-forming sol-gel composition on at least one surface of the substrate to form a coated substrate; and (b) subjecting the coated substrate to thermal conditions for a time sufficient to effect cure of the sol-gel composition and form a coated substrate with a sol-gel network layer having anti-glare properties.

摘要翻译： 提供基本上不含无机氧化物颗粒的可成膜成膜溶胶 - 凝胶组合物。 组合物包含：四烷氧基硅烷; 溶剂组分; 和非氧化物颗粒，并且还包含i）无机酸或ii）环氧官能的三烷氧基硅烷和含金属的催化剂。 还提供了展示抗眩光性能的涂层制品，其包括：（a）具有至少一个表面的基材; 和（b）由包含硅烷和非氧化物颗粒的可固化溶胶 - 凝胶组合物形成的固化膜形成组合物。 还提供了在基板上形成防眩光涂层的方法。 该方法包括：（a）在基材的至少一个表面上涂布可固化的成膜溶胶凝胶组合物以形成涂布的基材; 和（b）使涂覆的基材经受足够长时间以固化溶胶 - 凝胶组合物的热条件，并用具有防眩光性质的溶胶 - 凝胶网络层形成涂布的基材。

公开(公告)号：US20160146975A1

公开(公告)日：2016-05-26

申请号：US14951534

申请日：2015-11-25

申请人： PPG INDUSTRIES OHIO, INC.

发明人： SONGWEI LU

IPC分类号： G02B1/111 ,  B05D3/02 ,  C09D183/04 ,  B05D5/06 ,  G06F3/041 ,  C09D5/00

CPC分类号： C09D5/006 ,  B05D3/0236 ,  B05D3/0272 ,  B05D5/061 ,  C03C17/30 ,  C03C2217/29 ,  C03C2217/732 ,  C03C2218/112 ,  C03C2218/32 ,  C08F257/02 ,  C08G77/02 ,  C08G77/14 ,  C08K3/28 ,  C09D125/06 ,  C09D183/02 ,  C09D183/04 ,  C09D183/06 ,  G02B1/111 ,  G06F3/0412 ,  G06F2203/04103 ,  C08L25/00 ,  C08F212/08 ,  C08F220/34 ,  C08K3/01

摘要： Touch screen displays and other coated articles demonstrating antiglare properties are provided. A method of forming an antiglare coating on a substrate is also provided, and may be used to prepare the coated articles. The method comprises: (a) heating the substrate to a temperature of at least 100° F. (37.8° C.) to form a heated substrate; (b) applying a curable film-forming composition on at least one surface of the heated substrate to form a substrate coated with a sol-gel layer; and (c) subjecting the coated substrate to thermal conditions for a time sufficient to effect cure of the sol-gel layer. The curable film-forming composition comprises: (i) a silane; (ii) a mineral acid; and (iii) a solvent; wherein the weight ratio of mineral acid to silane is greater than 0.008:1 and the curable film-forming composition has a solids content of less than 10 percent by weight.

摘要翻译： 提供触摸屏显示器和其他涂层物品，展示防眩光性能。 还提供了在基材上形成防眩光涂层的方法，并且可以用于制备涂覆制品。 该方法包括：（a）将基底加热到至少100°F（37.8℃）的温度以形成加热的基底; （b）在加热的基板的至少一个表面上涂敷可固化的成膜组合物以形成涂有溶胶 - 凝胶层的基材; 和（c）使涂覆的基材经受热条件足够长的时间以固化溶胶 - 凝胶层。 可固化成膜组合物包括：（i）硅烷; （ii）无机酸; 和（iii）溶剂; 其中无机酸与硅烷的重量比大于0.008:1，并且可固化成膜组合物的固体含量小于10重量％。

公开(公告)号：US20230212421A1

公开(公告)日：2023-07-06

申请号：US18180800

申请日：2023-03-08

申请人： PPG Industries Ohio, Inc.

发明人： SONGWEI LU ,  JIPING SHAO ,  HONGYING ZHOU ,  ZILU LI ,  HIU YAN CHENG

IPC分类号： C09D175/12 ,  C08G18/38 ,  C08G18/34

CPC分类号： C09D175/12 ,  C08G18/3825 ,  C08G18/341

摘要： A substrate at least partially coated with an anti-fingerprint coating is prepared from a coating composition that includes: (a) an organic solvent; and (b) an alkoxysilane functional polymer having at least one ester linkage, at least one urethane linkage, and at least one alkoxysilane functional group. Further, the polymer is prepared from components including: (i) an active hydrogen functional compound having a hydroxyl group, amino group, thiol group, or a combination thereof; (ii) an intramolecular cyclic ester; and (iii) an isocyanate functional compound. The isocyanate functional compound (iii) has one or more alkoxysilane functional groups. Alkoxysilane functional polymers and coating compositions containing the same are also included.

公开(公告)号：US20190256720A1

公开(公告)日：2019-08-22

申请号：US15902656

申请日：2018-02-22

申请人： PPG INDUSTRIES OHIO, INC.

发明人： SONGWEI LU ,  JIPING SHAO

IPC分类号： C09D5/16 ,  C09D183/04 ,  C09D183/02 ,  C08L83/08 ,  C09J183/04 ,  C01F7/02 ,  C07F7/08

摘要： Coated articles demonstrating anti-fouling properties are provided, comprising: (a) a substrate comprising sapphire; (b) an adhesion promoting layer applied to the substrate; and (c) a top layer comprising at least an anti-fouling coating applied to the adhesion promoting layer. The adhesion promoting layer is formed from a curable sol-gel composition and has a dry film thickness less than 1000 nm after curing. The present invention also provides a method of forming a coated article comprising: (a) applying a curable film-forming sol-gel composition on a sapphire substrate, to form a coated substrate with a sol-gel adhesion promoting layer having a dry film thickness less than 1000 nm after curing; (b) subjecting the coated substrate to a temperature of at least 500° C. to effect cure of the sol-gel composition; and (c) applying at least an anti-fouling coating on the adhesion promoting layer to form a multi-layer, coated article.

公开(公告)号：US20220064353A1

公开(公告)日：2022-03-03

申请号：US17524013

申请日：2021-11-11

申请人： PPG INDUSTRIES OHIO, INC.

发明人： SONGWEI LU

IPC分类号： C08F257/02 ,  C09D5/00 ,  C09D125/06 ,  C09D183/06 ,  C03C17/30 ,  C09D183/02 ,  B05D3/02 ,  B05D5/06 ,  C09D183/04 ,  G02B1/111 ,  G06F3/041

摘要： Touch screen displays and other coated articles demonstrating antiglare properties are provided. A method of forming an antiglare coating on a substrate is also provided, and may be used to prepare the coated articles. The method comprises: (a) heating the substrate to a temperature of at least 100° F. (37.8° C.) to form a heated substrate; (b) applying a curable film-forming composition on at least one surface of the heated substrate to form a substrate coated with a sol-gel layer; and (c) subjecting the coated substrate to thermal conditions for a time sufficient to effect cure of the sol-gel layer. The curable film-forming composition comprises: (i) a silane; (ii) a mineral acid; and (iii) a solvent; wherein the weight ratio of mineral acid to silane is greater than 0.008:1 and the curable film-forming composition has a solids content of less than 10 percent by weight.

公开(公告)号：US20190033491A1

公开(公告)日：2019-01-31

申请号：US15662894

申请日：2017-07-28

申请人： PPG INDUSTRIES OHIO, INC.

发明人： SONGWEI LU ,  JIPING SHAO ,  ZILU LI

IPC分类号： G02B1/115 ,  C03C17/34 ,  C23C14/06 ,  C23C14/10 ,  G02B1/18 ,  G06F3/041

摘要： Coated articles demonstrating antireflective properties are provided. Exemplary coated articles comprise a substrate and two or three coating layers applied to at least one surface of the substrate; the coatings are deposited from sol-gel compositions comprising a silane. Each adjacent coating layer demonstrates a different refractive index. The coated article further comprises an outermost anti-fouling coating layer applied to at least one surface of a coating layer. Processes for forming the coated articles are also provided.

公开(公告)号：US20160038972A1

公开(公告)日：2016-02-11

申请号：US14818359

申请日：2015-08-05

申请人： PPG INDUSTRIES OHIO, INC.

发明人： SONGWEI LU

IPC分类号： B05D5/06 ,  G02B1/111 ,  C09D183/06 ,  B05D1/02 ,  B05D3/00

CPC分类号： B05D5/06 ,  B05D1/02 ,  B05D3/002 ,  C08G77/045 ,  C08G77/14 ,  C09D4/00 ,  C09D183/06 ,  G02B1/111 ,  C08L83/00 ,  C08K5/0091 ,  C08K2003/2227 ,  C08K5/5435 ,  C08K5/5415

摘要： A method of forming an anti-glare coating on a substrate is provided. The method comprises: (a) heating the substrate to a temperature of at least 100° F. (37.8° C.) to form a heated substrate; (b) applying a curable film-forming sol-gel composition on at least one surface of the heated substrate, to form a coated substrate with a sol-gel network layer having a surface roughness; and (c) subjecting the coated substrate to conditions for a time sufficient to effect cure of the sol-gel layer and form an anti-glare, coated article. The sol-gel network layer is essentially free of inorganic oxide particles and comprises: (i) a tetraalkoxysilane; (ii) an epoxy functional trialkoxysilane; (iii) a metal-containing catalyst; and (iv) a solvent component. Coated articles prepared by the method above and demonstrating anti-glare properties are also provided.

摘要翻译： 提供了在基板上形成防眩涂层的方法。 该方法包括：（a）将基底加热到至少100°F（37.8℃）的温度以形成加热的基底; （b）在加热的基材的至少一个表面上施加可固化的成膜溶胶 - 凝胶组合物，以形成具有表面粗糙度的溶胶 - 凝胶网络层的涂布基材; 和（c）使涂覆的基材经历足以实现溶胶 - 凝胶层固化的时间并形成防眩涂层制品。 溶胶 - 凝胶网络层基本上不含无机氧化物颗粒，包括：（i）四烷氧基硅烷; （ii）环氧官能的三烷氧基硅烷; （iii）含金属的催化剂; 和（iv）溶剂组分。 还提供了通过上述方法制备并显示抗眩光性质的涂层制品。