Process for the preparation of alkali metal salts of
2-phosphonobutane-1,2,4-tricarboxylic acid
    3.
    发明授权
    Process for the preparation of alkali metal salts of 2-phosphonobutane-1,2,4-tricarboxylic acid 失效
    制备2-膦酰基-1,2,4-三羧酸的碱金属盐的方法

    公开(公告)号:US5233088A

    公开(公告)日:1993-08-03

    申请号:US746841

    申请日:1991-08-19

    IPC分类号: C07F9/38

    CPC分类号: C07F9/3808

    摘要: The present invention relates to a process for the preparation of alkali metal salts of 2-phosphonobutane-1,2,4-tricarboxylic acid, characterized in that 2-phosphonobutane-1,2,4-tricarboxylic acid penta-alkyl esters or partial esters are reacted with an aqueous alkali metal hydroxide solution in a ratio of from 0.5 to 0.76 mol, preferably from 0.6 to 0.7 mol of alkali metal hydroxide per mol of ester function at temperatures from 20.degree. to 200.degree. C. in a one-shot process.

    摘要翻译: 本发明涉及2-膦酰基丁烷-1,2,4-三羧酸的碱金属盐的制备方法,其特征在于2-膦酰基丁烷-1,2,4-三羧酸五烷基酯或偏酯 在一步法中在20℃至200℃的温度下,每摩尔酯官能团与碱金属氢氧化物水溶液的比例为0.5至0.76摩尔,优选0.6至0.7摩尔碱金属氢氧化物。 。