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    METHOD FOR PRODUCING ORGANIC PHOSPHOROUS COMPOUNDS CONTAINING HALOGENE
    1.
    发明申请
    METHOD FOR PRODUCING ORGANIC PHOSPHOROUS COMPOUNDS CONTAINING HALOGENE 有权
    用于生产含有卤素的有机磷化合物的方法

    公开(公告)号：US20090281356A1

    公开(公告)日：2009-11-12

    申请号：US12373336

    申请日：2007-07-03

    申请人： Robert Baumann ,  Tobias Aechtner ,  Wolfgang Siegel ,  Hermann Luyken ,  Peter Pfab ,  Jens Scheidel ,  Andreas Leitner ,  Andreas Glass

    发明人： Robert Baumann ,  Tobias Aechtner ,  Wolfgang Siegel ,  Hermann Luyken ,  Peter Pfab ,  Jens Scheidel ,  Andreas Leitner ,  Andreas Glass

    IPC分类号： C07F9/48

    CPC分类号： C07F9/4891 ,  C07F9/4875

    摘要： Method of producing compounds of the general formula XPR2(OR1)  I a where X is chlorine, bromine or iodine and R1 is an organic radical, by reacting compounds of the general formula X2PR2  II, in which X has the meaning given above and R2 is an organic radical, with compounds of the general formula R1OH  III, in which R1 has the meaning given above, to give a mixture IV, in that a) the postreaction is carried out at a temperature of from 50 to 240° C. and a pressure of from 0.001 to 0.9 bar, b) from the mixture IV the compounds I a are separated off from the compounds PR2(OR1)2  I b and, if appropriate, the compounds II and c) compounds I b and, if appropriate, unreacted compounds II are returned to the synthesis stage.

    摘要翻译： 通过使通式X 2 PR 2 II的化合物（其中X具有上面给出的含义，R 2）是通过使通式XPR2（OR1）Ia的化合物的制备方法，其中X是氯，溴或碘，R 1是有机基团 具有通式R 1 OH III的化合物的化合物，其中R 1具有上述含义，得到混合物IV，其中a）反应在50-240℃的温度和 压力为0.001至0.9巴，b）从混合物IV中，化合物I a与化合物PR2（OR1）2 I b分离，如果合适，分离出化合物II和c）化合物I b，如果合适， 未反应的化合物II返回到合成阶段。

    Method for producing organic phosphorous compounds containing halogens
    2.
    发明授权
    Method for producing organic phosphorous compounds containing halogens 有权
    制备含有卤素的有机磷化合物的方法

    公开(公告)号：US07851656B2

    公开(公告)日：2010-12-14

    申请号：US12373336

    申请日：2007-07-03

    申请人： Robert Baumann ,  Tobias Aechtner ,  Wolfgang Siegel ,  Hermann Luyken ,  Peter Pfab ,  Jens Scheidel ,  Andreas Leitner ,  Andreas Glass

    发明人： Robert Baumann ,  Tobias Aechtner ,  Wolfgang Siegel ,  Hermann Luyken ,  Peter Pfab ,  Jens Scheidel ,  Andreas Leitner ,  Andreas Glass

    IPC分类号： C07F9/02

    CPC分类号： C07F9/4891 ,  C07F9/4875

    摘要： Method of producing compounds of the general formula XPR2(OR1)  Ia where X is chlorine, bromine or iodine and R1 is an organic radical, by reacting compounds of the general formula X2PR2  II, in which X has the meaning given above and R2 is an organic radical, with compounds of the general formula R1OH  III, in which R1 has the meaning given above, to give a mixture IV, in that a) the postreaction is carried out at a temperature of from 50 to 240° C. and a pressure of from 0.001 to 0.9 bar, b) from the mixture IV the compounds Ia are separated off from the compounds PR2(OR1)2  Ib and, if appropriate, the compounds II and c) compounds Ib and, if appropriate, unreacted compounds II are returned to the synthesis stage.

    摘要翻译： 通过使通式X 2 PR 2 II的化合物（其中X具有上面给出的含义，R 2是一个或多个）来制备通式XPR2（OR1）Ia化合物的方法，其中X是氯，溴或碘，R 1是有机基团 有机基团，具有通式R 1 OH III的化合物，其中R 1具有上述含义，得到混合物IV，其中a）反应在50-240℃的温度和压力 0.001至0.9巴，b）从混合物IV中，化合物Ia从化合物PR2（OR1）IIb中分离出来，如果合适，化合物II和c）化合物Ib和如果合适的话，未反应的化合物II为 回到合成阶段。

    Method for producing linear pentenenitrile
    3.
    发明授权
    Method for producing linear pentenenitrile 有权
    线性戊烯腈的制备方法

    公开(公告)号：US08410299B2

    公开(公告)日：2013-04-02

    申请号：US13361783

    申请日：2012-01-30

    申请人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baβler

    发明人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baβler

    IPC分类号： C07C253/30

    CPC分类号： C07C253/30 ,  C07C253/10 ,  Y02P20/582 ,  C07C255/07

    摘要： A method for producing 3-pentenenitrile is provided that includes: (a) isomerizing an educt stream containing 2-methyl-3-butenenitrile on at least one dissolved or dispersed isomerization catalyst to form a stream (1), which contains the isomerization catalyst(s), 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile; (b) distilling the stream (1) to obtain a stream (2) as the overhead product, which contains 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile and a stream (3) as the bottom product, which contains the isomerization catalyst(s); (c) distilling the stream (2) to obtain a stream (4) as the overhead product, which is enriched with (Z)-2-methyl-2-butenenitrile in comparison to stream (2), and a stream (5) as the bottom product, which is enriched with 3-pentenenitrile and 2-methyl-3-butenenitrile in comparison to stream (2); (d) distilling stream (5) to obtain a stream (6) as the bottom product, which contains 3-pentenenitrile and a stream (7) as the head product containing 2-methyl-3-butenenitrile.

    摘要翻译： 提供了一种制备3-戊烯腈的方法，其包括：（a）在至少一种溶解或分散的异构化催化剂上使含有2-甲基-3-丁烯腈的流出物异构化以形成含有异构化催化剂（ s），2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈; （b）蒸馏物流（1）以获得作为塔顶产物的物流（2），其含有2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈和流（ 3）作为含有异构化催化剂的底部产物; （c）与料流（2）相比，蒸馏物流（2）以获得作为塔顶产物的物流（4），其与（2）相比富含（Z）-2-甲基-2-丁烯腈， 作为与料流（2）相比富含3-戊烯腈和2-甲基-3-丁烯腈的底部产物; （d）蒸馏物流（5），得到作为底物的物流（6），其含有3-戊烯腈和作为含有2-甲基-3-丁烯腈的头部产物的物流（7）。

    METHOD FOR PRODUCING LINEAR PENTENENITRILE
    4.
    发明申请
    METHOD FOR PRODUCING LINEAR PENTENENITRILE 有权
    生产线性胆固醇的方法

    公开(公告)号：US20120178958A1

    公开(公告)日：2012-07-12

    申请号：US13361783

    申请日：2012-01-30

    申请人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baßler

    发明人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baßler

    IPC分类号： C07C253/30

    CPC分类号： C07C253/30 ,  C07C253/10 ,  Y02P20/582 ,  C07C255/07

    摘要： A method for producing 3-pentenenitrile is provided that includes: (a) isomerizing an educt stream containing 2-methyl-3-butenenitrile on at least one dissolved or dispersed isomerisation catalyst to form a stream (1), which contains the isomerisation catalyst(s), 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile; (b) distilling the stream (1) to obtain a stream (2) as the overhead product, which contains 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile and a stream (3) as the bottom product, which contains the isomerisation catalyst(s); (c) distilling the stream (2) to obtain a stream (4) as the overhead product, which is enriched with (Z)-2-methyl-2-butenenitrile in comparison to stream (2), and a stream (5) as the bottom product, which is enriched with 3-pentenenitrile and 2-methyl-3-butenenitrile in comparison to stream (2); (d) distilling stream (5) to obtain a stream (6) as the bottom product, which contains 3-pentenenitrile and a stream (7) as the head product containing 2-methyl-3-butenenitrile.

    摘要翻译： 提供了一种制备3-戊烯腈的方法，其包括：（a）在至少一种溶解或分散的异构化催化剂上异构化含有2-甲基-3-丁烯腈的流出物流以形成含有异构化催化剂（ s），2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈; （b）蒸馏物流（1）以获得作为塔顶产物的物流（2），其含有2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈和流（ 3）作为含有异构化催化剂的底部产物; （c）与料流（2）相比，蒸馏物流（2）以获得作为塔顶产物的物流（4），其与（2）相比富含（Z）-2-甲基-2-丁烯腈， 作为与料流（2）相比富含3-戊烯腈和2-甲基-3-丁烯腈的底部产物; （d）蒸馏物流（5），得到作为底物的物流（6），其含有3-戊烯腈和作为含有2-甲基-3-丁烯腈的头部产物的物流（7）。

    Method for Producing Linear Pentenenitrile
    5.
    发明申请
    Method for Producing Linear Pentenenitrile 审中-公开
    生产线性戊烯腈的方法

    公开(公告)号：US20080281120A1

    公开(公告)日：2008-11-13

    申请号：US10586470

    申请日：2005-01-27

    申请人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Bassler

    发明人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Bassler

    IPC分类号： C07C255/00

    CPC分类号： C07C253/30 ,  C07C253/10 ,  Y02P20/582 ,  C07C255/07

    摘要： A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) isomerizing a reactant stream which comprises 2-methyl-3-butenenitrile over at least one dissolved or dispersed isomerization catalyst to give a stream 1 which comprises the at least one isomerization catalyst, 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile, (b) distilling stream 1 to obtain a stream 2 as the top product which comprises 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile, and a stream 3 as the bottom product which comprises the at least one isomerization catalyst, (c) distilling stream 2 to obtain a stream 4 as the top product which, compared to stream 2, is enriched in (Z)-2-methyl-2-butenenitrile, based on the sum of all pentenenitriles in stream 2, and a stream 5 as the bottom product which, compared to stream 2, is enriched in 3-pentenenitrile and 2-methyl-3-butenenitrile, based on the sum of all pentenenitriles in stream 2, (d) distilling stream 5 to obtain a stream 6 as the bottom product which comprises 3-pentenenitrile and a stream 7 as the top product which comprises 2-methyl-3-butenenitrile.

    摘要翻译： 描述了制备3-戊烯腈的方法，其特征在于以下方法步骤：（a）在至少一种溶解或分散的异构化催化剂上异构化包含2-甲基-3-丁烯腈的反应物流，得到流1，其包含 至少一种异构化催化剂，2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈，（b）蒸馏物流1，得到作为顶部产物的物流2，其包含2-甲基 -3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈，以及作为底部产物的料流3，其包含至少一种异构化催化剂，（c）蒸馏物流2以获得物流4， 与流2相比，基于流2中的所有五烯丙烯的总和和作为底部产物的流5，与流2相比富含（Z）-2-甲基-2-丁烯腈的顶部产物与流2相比较 ，富含3-戊烯腈和2-甲基-3-丁烯腈，基于所有pentenenit （d）蒸馏流5以获得作为底部产物的料流6，其包含3-戊烯腈和作为顶部产物的料流7，其包含2-甲基-3-丁烯腈。

    Separation of Nickel(0) Complexes and Phosphorus-Containing Ligands from Nitrile Mixtures
    6.
    发明申请
    Separation of Nickel(0) Complexes and Phosphorus-Containing Ligands from Nitrile Mixtures 审中-公开
    从腈混合物中分离镍（0）络合物和含磷配体

    公开(公告)号：US20080281119A1

    公开(公告)日：2008-11-13

    申请号：US10586493

    申请日：2005-01-27

    申请人： Jens Scheidel ,  Tim Jungkamp ,  Michael Bartsch ,  Gerd Haderlein ,  Robert Baumann ,  Hermann Luyken ,  Petra Deckert ,  Peter Pfab ,  Wolfgang Siegel ,  Tobias Aechtner

    发明人： Jens Scheidel ,  Tim Jungkamp ,  Michael Bartsch ,  Gerd Haderlein ,  Robert Baumann ,  Hermann Luyken ,  Petra Deckert ,  Peter Pfab ,  Wolfgang Siegel ,  Tobias Aechtner

    IPC分类号： C07C253/34

    CPC分类号： C07C253/34 ,  C07C255/04

    摘要： A process for extractively removing nickel(0) complexes having phosphorus ligands and/or free phosphorus ligands from a reaction effluent of a hydrocyanation of unsaturated mononitriles to dinitriles by extraction by means of a hydrocarbon, a phase separation of the hydrocarbon and of the reaction effluent into two phases being effected at a temperature T (in ° C.),wherein the content of nickel(0) complexes having phosphorus ligands and/or free phosphorus ligands in the reaction effluent of the hydrocyanation, depending on the temperature T, is at least y % by weight and, irrespective of the temperature T, is a maximum of 60% by weight, where the numerical value of the minimum content y is given by the equation y=0.5·T+20 and T is to be used in the equation as a dimensionless numerical value.

    摘要翻译： 一种通过烃的提取将含有磷配体和/或游离磷配位体的镍（0）络合物从不饱和单腈的氢化氰化反应流出物萃取到二腈的方法，烃和反应流出物的相分离 在温度T（℃）下进行两相，其中根据温度T，氢氰化反应流出物中具有磷配体和/或游离磷配体的镍（0）络合物的含量在 最小含量y的数值由等式<？in-line-formula description =“在线式 “end =”lead“？> y = 0.5.T + 20 <？in-line-formula description =”In-line Formulas“end =”tail“？>而T在方程中用作无量纲数字 值。

    Process for producing nickel(0)-phosphorus ligand complexes
    10.
    发明授权
    Process for producing nickel(0)-phosphorus ligand complexes 有权
    制备镍（0） - 磷配体络合物的方法

    公开(公告)号：US07705171B2

    公开(公告)日：2010-04-27

    申请号：US12279795

    申请日：2007-02-13

    申请人： Gerd Haderlein ,  Tobias Aechtner ,  Andreas Leitner ,  Peter Pfab ,  Hermann Luyken ,  Jens Scheidel

    发明人： Gerd Haderlein ,  Tobias Aechtner ,  Andreas Leitner ,  Peter Pfab ,  Hermann Luyken ,  Jens Scheidel

    IPC分类号： C07F15/04

    CPC分类号： B01J31/1845 ,  B01J31/24 ,  B01J2231/32 ,  B01J2531/847

    摘要： A process for preparing nickel(0)-phosphorus ligand complexes comprising at least one nickel(0) central atom and at least one phosphorus ligand by reacting a nickel(II) compound with a reducing agent in the presence of the ligand to give a reaction mixture, wherein a) the molar reducing agent:nickel(II) compound ratio in the reaction is from 1:1 to 1000:1, calculated as the molar ratio of the redox equivalents, b) the molar phosphorus ligand:nickel(II) compound ratio in the reaction is not more than 30:1, calculated as the molar P atoms:Ni atoms ratio, c) the nickel(0) content in the resulting reaction mixture is not more than 1.3% by weight and d) the resulting reaction mixture is extracted by adding at least one dinitrile and at least one hydrocarbon to form at least two immiscible phases.

    摘要翻译： 一种通过在配体存在下使镍（II）化合物与还原剂反应而制备包含至少一个镍（O）中心原子和至少一个磷配体的镍（0） - 磷配体络合物的方法，得到反应 混合物，其中a）摩尔还原剂：反应中的镍（II）化合物比例为1:1至1000:1，以氧化还原当量的摩尔比计算，b）磷配体：镍（II） 反应中的化合物比例不超过30:1，以P原子摩尔数计算：Ni原子比，c）所得反应混合物中的镍（0）含量不超过1.3重量％，d）所得的 通过加入至少一种二腈和至少一种烃以形成至少两个不混溶的相来萃取反应混合物。