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公开(公告)号：US4510040A
公开(公告)日：1985-04-09
申请号：US549694
申请日：1983-11-07
申请人： Ronald W. Skinner , John C. Tao , Samuel Znaimer
发明人： Ronald W. Skinner , John C. Tao , Samuel Znaimer
CPC分类号： C10G1/002
摘要： This invention relates to an improved process for the production of liquid carbonaceous fuels and solvents from carbonaceous solid fuels, especially coal.The claimed improved process includes the hydrocracking of the light SRC mixed with a suitable hydrocracker solvent. The recycle of the resulting hydrocracked product, after separation and distillation, is used to produce a solvent for the hydrocracking of the light solvent refined coal.
摘要翻译： 本发明涉及一种用于从碳质固体燃料，特别是煤生产液体碳质燃料和溶剂的改进方法。 所要求改进的方法包括与合适的加氢裂化器溶剂混合的光SRC的加氢裂化。 在分离和蒸馏之后，所得加氢裂化产物的再循环用于生产用于轻质溶剂精炼煤的加氢裂化的溶剂。
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公开(公告)号：US4491511A
公开(公告)日：1985-01-01
申请号：US549693
申请日：1983-11-07
申请人： Ronald W. Skinner , John C. Tao , Samuel Znaimer
发明人： Ronald W. Skinner , John C. Tao , Samuel Znaimer
摘要： An improved SRC-I two-stage coal liquefaction process which improves the product slate is provided. Substantially all of the net yield of 650.degree.-850.degree. F. heavy distillate from the LC-Finer is combined with the SRC process solvent, substantially all of the net 400.degree.-650.degree. F. middle distillate from the SRC section is combined with the hydrocracker solvent in the LC-Finer, and the initial boiling point of the SRC process solvent is increased sufficiently high to produce a net yield of 650.degree.-850.degree. F. heavy distillate of zero for the two-stage liquefaction process.
摘要翻译： 提供了改进产品板岩的改进的SRC-I两级煤液化工艺。 基本上所有的净收率为650°-850°F。来自LC-Finer的重质馏出物与SRC工艺溶剂相结合，基本上所有的来自SRC段的400°-650°F净中间馏分与 LC-Finer中的加氢裂化器溶剂和SRC工艺溶剂的初始沸点增加到足够高，以产生650--850°F的净产率，用于两级液化过程的零馏分。
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公开(公告)号：US4536275A
公开(公告)日：1985-08-20
申请号：US586937
申请日：1984-03-07
CPC分类号： C10G1/002
摘要： This invention relates to an improved two-stage process for the production of liquid carbonaceous fuels and solvents from carbonaceous solid fuels, especially coal.
摘要翻译： 本发明涉及用于从含碳固体燃料，特别是煤生产液体碳质燃料和溶剂的改进的两阶段方法。
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公开(公告)号：US4336238A
公开(公告)日：1982-06-22
申请号：US195828
申请日：1980-10-10
IPC分类号： B01J23/00 , C01B15/029 , C01B15/02
CPC分类号： C01B15/029
摘要： An improvement in a process for producing hydrogen peroxide by contacting a mixture of hydrogen and oxygen with a palladium on carbon catalyst in the presence of an acidic aqueous liquid capable of inhibiting decomposition of hydrogen peroxide comprises prolonging the useful life of the catalyst by continuous removal of palladium salts produced by solubilization of the catalyst from the acidic aqueous liquid.
摘要翻译： 通过在能够抑制过氧化氢分解的酸性含水液体的存在下，使氢和氧的混合物与钯/碳催化剂接触来制造过氧化氢的方法的改进包括通过连续除去催化剂的使用寿命来延长催化剂的使用寿命 通过从酸性含水液体中溶解催化剂而产生的钯盐。
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5.发明授权
公开(公告)号：US4329321A
公开(公告)日：1982-05-11
申请号：US195972
申请日：1980-10-10
CPC分类号： C22B11/04 , C01G55/001 , C22B3/24 , Y02P10/234
摘要： Salts of Group VIII noble metals are recovered from neutral or acidic solutions by admixing with the solution up to 10% by weight of hydrogen peroxide, adsorbing the salt of the Group VIII noble metal from the peroxide-containing solution on activated carbon and separating activated carbon containing the adsorbed Group VIII noble metal salts from solution diminished in concentration thereof.
摘要翻译： 将VIII族贵金属的盐从中性或酸性溶液中回收，与溶液最多混合10％（重量）的过氧化氢，将含有过氧化物的溶液中的第Ⅷ族贵金属的盐吸附在活性炭上并分离活性炭 含有来自溶液的吸附的VIII族贵金属盐的浓度降低。
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公开(公告)号：US4389390A
公开(公告)日：1983-06-21
申请号：US344235
申请日：1982-01-29
IPC分类号： C01B15/029 , C01B15/02
CPC分类号： C01B15/029
摘要： An improvement in a process for producing hydrogen peroxide by contacting a mixture of hydrogen and oxygen with a palladium on carbon catalyst in the presence of an acidic liquid capable of inhibiting decomposition of thus-produced hydrogen peroxide comprises prolonging the useful life of the catalyst by continuous removal of palladium salts produced by solubilization of the catalyst from the acidic liquid, preferably by employing high surface activated carbon as the catalyst support and adsorbent for palladium salts.
摘要翻译： 在能够抑制由此产生的过氧化氢分解的酸性液体的存在下，通过使氢和氧的混合物与钯/碳催化剂接触来制备过氧化氢的方法的改进包括通过连续地延长催化剂的使用寿命 通过优选通过使用高表面活性炭作为催化剂载体和钯盐的吸附剂来除去由酸性液体溶解催化剂而产生的钯盐。
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公开(公告)号：US4313806A
公开(公告)日：1982-02-02
申请号：US195815
申请日：1980-10-10
CPC分类号： C23F13/02
摘要： Dissolution of Group VIII supported metal catalysts from semi-conductive or conductive carriers in liquid media containing a strong inorganic acid is stopped by making the Group VIII noble metal cathodic with respect to an anode placed in the reactor. A representative embodiment is in processes for synthesis of hydrogen peroxide from its elements.
摘要翻译： 通过使VIII族贵金属相对于放置在反应器中的阳极阴极化而停止将来自半导体或导电载体的VIII族负载金属催化剂溶解在含有强无机酸的液体介质中。 代表性的实施方案是从其元素合成过氧化氢的方法。
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公开(公告)号：US4421630A
公开(公告)日：1983-12-20
申请号：US308639
申请日：1981-10-05
IPC分类号： C10G1/00
CPC分类号： C10G1/006
摘要： There is described an improved liquefaction process by which coal is converted to a low ash and low sulfur carbonaceous material that can be used as a fuel in an environmentally acceptable manner without costly gas scrubbing equipment. In the process, coal is slurried with a pasting oil, passed through a preheater and at least two dissolvers in series in the presence of hydrogen-rich gases at elevated temperatures and pressures. Solids, including mineral ash and unconverted coal macerals, are separated from the condensed reactor effluent. In accordance with the improved process, the first dissolver is operated at a higher temperature than the second dissolver. This temperature sequence produces improved product selectivity and permits the incorporation of sufficient hydrogen in the solvent for adequate recycle operations.
摘要翻译： 描述了一种改进的液化过程，其中煤转化为低灰分和低硫碳质材料，其可以以环境可接受的方式用作燃料，而不需要昂贵的气体洗涤设备。 在此过程中，煤用粘贴的油浆化，在富含氢气的气体存在下，在升高的温度和压力下，通过预热器和至少两个溶解器串联。 固体，包括矿物灰和未转化的煤矿，与冷凝的反应器流出物分离。 根据改进的方法，第一溶解器在比第二溶解器更高的温度下操作。 该温度序列产生改善的产物选择性，并允许在溶剂中引入足够的氢以进行充分的循环操作。
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公开(公告)号：US4336239A
公开(公告)日：1982-06-22
申请号：US219402
申请日：1980-12-22
IPC分类号： C01B15/029 , C01B15/02
CPC分类号： C01B15/029
摘要： This invention relates to an improvement in hydrogen peroxide synthesis from hydrogen and oxygen, in an acidic medium containing an oxygenated or nitrogenous organic compound using a supported Group VIII noble metal catalyst. The improvement comprises using an oxygen/hydrogen ratio higher than about 3.4 and a catalyst level above 30 mg. per 100 ml. of medium.
摘要翻译： 本发明涉及使用负载的第VIII族贵金属催化剂，在含有含氧有机化合物的酸性介质中由氢和氧合成过氧化氢的改进。 该改进包括使用高于约3.4的氧/氢比和高于30mg的催化剂水平。 每100毫升 的中等。
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公开(公告)号：US4379778A
公开(公告)日：1983-04-12
申请号：US195829
申请日：1980-10-10
IPC分类号： B01J23/00 , C01B15/029 , C01B15/02
CPC分类号： C01B15/029
摘要： This invention relates to improvements in palladium-carbon catalysts for the production of hydrogen peroxide from a mixture of hydrogen and oxygen in the presence of an aqueous liquid capable of inhibiting the decomposition of hydrogen peroxide. The improvement comprises pretreating the catalyst with an aldehyde or ketone, and, preferably, also pretreating the catalyst with a dilute solution of hydrochloric acid. Improved catalysts are obtained by reducing a soluble palladium compound deposited on a high surface area non-graphitic carbon base, in the form of a dried powder, with hydrogen at 27.degree.-200.degree. C.
摘要翻译： 本发明涉及在能够抑制过氧化氢分解的含水液体存在下从氢和氧的混合物中生产过氧化氢的钯 - 碳催化剂的改进。 改进包括用醛或酮预处理催化剂，并且优选还用稀盐酸溶液预处理催化剂。 改进的催化剂是通过将沉积在高表面积非石墨碳底物上的可溶性钯化合物以干燥粉末形式，在27℃-200℃下用氢气还原来获得的。
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